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    • 1. 发明授权
    • Apparatus for radiochromatographic analysis of mixture of substances
containing components tagged by radioactive isotopes
    • 含放射性同位素标记物质混合物的放射色谱分析装置
    • US4214161A
    • 1980-07-22
    • US867154
    • 1978-01-05
    • Viktor L. TalrozeVladimir D. GrishinBoris A. Galushkin
    • Viktor L. TalrozeVladimir D. GrishinBoris A. Galushkin
    • G01T7/00G01N30/02G01N30/08G01N30/62G01N30/78G01T1/20G01T1/161
    • G01N30/78G01N30/62G01N2030/77
    • Proposed is a device for radiochromatographic analysis of mixtures of substances containing components tagged by radioactive isotopes, such as soft .beta.-isotopes comprising a chromatographic column, a detector of nuclear radiation and a chromatographic detector connected in series along the flow of the substance being analyzed. The detector of nuclear radiation is provided with a cell made as a tube with a scintillator applied onto its inner surface in the form of a solid layer. The tube is provided with movable means for sequentialy cooling and heating the same and a light detector which is movable along the length of the tube. In operation, upon introduction of the portion of the mixture being analyzed into the column, with the heater interacting with the tube, the heater and cooler are moved so that by the time the last component of the mixture exits from the column, the cooler is in interacting relationship with the tube whereby the components of the mixture are frozen. According to one mode of operation, the light detector is then moved to register the glow of the strips of the radioactive components whereby a radiochromatogram can be derived.
    • 提出了用于放射色谱分析含有由放射性同位素标记的成分的物质的混合物的装置,例如包含色谱柱,核辐射检测器和沿着被分析物质的流动串联连接的色谱检测器的软β-同位素。 核辐射检测器具有制成管的电池,其中闪烁体以固体层的形式施加在其内表面上。 该管设置有用于对其进行连续冷却和加热的可移动装置,以及可沿着管的长度移动的光检测器。 在操作中,当将待分析的混合物的一部分引入柱中时,加热器与管相互作用,使加热器和冷却器移动,使得在混合物的最后一个成分离开塔的时候,冷却器 与管的相互作用关系,由此混合物的组分被冷冻。 根据一种操作模式,然后移动光检测器以记录放射性元件的条带的辉光,由此可以得到放射色谱图。