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1. 发明授权

US5925184A Cement composition 失效
标题翻译：水泥组成
公开(公告)号：US5925184A
公开(公告)日：1999-07-20
申请号：US803759
申请日：1997-02-21
申请人： Tsuyoshi Hirata , Tsutomu Yuasa , Toru Uno , Koichiro Nagare , Hideyuki Tahara , Shogo Iwai
发明人： Tsuyoshi Hirata , Tsutomu Yuasa , Toru Uno , Koichiro Nagare , Hideyuki Tahara , Shogo Iwai
IPC分类号： C04B24/26 , C04B24/32 , C04B28/02 , C04B24/04
CPC分类号： C04B28/02 , C04B24/2647 , C04B24/2694 , C04B2103/308
摘要： A cement composition excelling in the slump retaining property which comprises at least cement admixture comprising as a main ingredient thereof (I) a copolymer (A) of short-chain polyalkylene glycol (meth)acrylate (a), a long-chain polyalkylene glycol (meth)acrylate (b), a carboxylic acid monomer (c), and a monomer copolymerizable with the monomers mentioned above or a salt of the copolymer (B), (II) a copolymer (A.sub.1) of the monomers (a), (c), and (d) mentioned above or a salt thereof, (III) a mixture of a copolymer (A.sub.1) of the monomers (a), (c), and (d) mentioned above or a salt (B.sub.1) of thereof with a known cement admixture, or (IV) a polycarboxylic acid based polymer (A.sub.3) manifesting to a calcium sulfoaluminate based expansive additive an adsorption ratio of not less than 90% in 5 minutes at room temperature when added in an amount of 0.1% by weight as solids or a salt (B.sub.3) thereof, or (V) a mixture of said polycarboxylic acid polymer with a known cement dispersant; cement; and water.
摘要翻译：坍落度保持性优异的水泥组合物至少包括水泥混合物，其包含主要成分（I）短链聚亚烷基二醇（甲基）丙烯酸酯（a）的共聚物（A），长链聚亚烷基二醇（甲基丙烯酸酯（b），羧酸单体（c）和可与上述单体共聚的单体或共聚物（B），（II）的单体（a）的共聚物（A1） c）和（d）或其盐，（III）上述单体（a），（c）和（d）的共聚物（A1）或其盐（B1）的混合物使用已知的水泥混合物，或（IV）表示基于硫铝酸钙的膨胀性添加剂的多元羧酸系聚合物（A3），当以0.1％的量加入时，在室温下5分钟内吸附率不小于90％重量为固体或其盐（B3），或（V）所述多元羧酸聚合物与已知的水泥分散剂的混合物; 水泥; 和水。

2. 发明授权

US06174980B1 Cement dispersant, method for producing polycarboxylic acid for cement dispersant and cement composition 失效
标题翻译：水泥分散剂，用于水泥分散剂和水泥组合物的多元羧酸的制备方法
公开(公告)号：US06174980B1
公开(公告)日：2001-01-16
申请号：US08991285
申请日：1997-12-16
申请人： Tsuyoshi Hirata , Tsutomu Yuasa , Katsuhisa Shiote , Koichiro Nagare , Syogo Iwai
发明人： Tsuyoshi Hirata , Tsutomu Yuasa , Katsuhisa Shiote , Koichiro Nagare , Syogo Iwai
IPC分类号： C08F22210
CPC分类号： C04B24/267 , C04B24/2647 , C04B2103/302 , C04B2103/408 , C08F290/062 , C08G65/2609 , C08G65/3322 , C08L71/02 , Y10S526/932 , C08L2666/04
摘要： The present invention provides a method for producing a cement dispersant having high percentage in water reduction-rate and appropriate air-entraining property. This method for producing a polycarboxylic acid for a cement dispersant is characterized in that alkylene oxide is added at a specific temperature range.
摘要翻译：本发明提供一种水分散剂的制造方法，该水泥分散剂具有高的降水率和合适的加气性能。该水泥分散剂用多元羧酸的制造方法的特征在于，在特定的温度范围加入环氧烷烃。

3. 发明授权

US06545083B1 Cement additive 失效
标题翻译：水泥添加剂
公开(公告)号：US06545083B1
公开(公告)日：2003-04-08
申请号：US09522300
申请日：2000-03-09
申请人： Tsuyoshi Hirata , Tsutomu Yuasa , Koichiro Nagare , Hirokatsu Kawakami
发明人： Tsuyoshi Hirata , Tsutomu Yuasa , Koichiro Nagare , Hirokatsu Kawakami
IPC分类号： C08L3302
CPC分类号： C04B24/2647 , C04B28/02 , C08F220/28 , C08F290/062 , C08F2220/286 , C08F2220/287 , C08F2220/288 , C04B2103/304 , C08F220/06 , C08F212/08 , C08F216/18 , C08F220/14
摘要： The present invention is thus directed to a cement additive which comprises a copolymer (A) obtained by polymerizing a monomer mixture (K), wherein; said monomer mixture (K) comprises a polyalkylene glycol ester monomer (I) represented by the general formula (1): a polyalkylene glycol ester monomer (II) represented by the general formula (2): and a carboxylic acid monomer (III) represented by the general formula (3):
摘要翻译：因此，本发明涉及一种水泥添加剂，其包含通过聚合单体混合物（K）获得的共聚物（A），其中所述单体混合物（K）包含由通式（I）表示的聚亚烷基二醇酯单体（I） 1）：由通式（2）表示的聚亚烷基二醇酯单体（II）和由通式（3）表示的羧酸单体（III）：

4. 发明授权

US06388038B1 Method for producing polycarboxylic acid for cement dispersant and cement composition 有权
标题翻译：用于水泥分散剂和水泥组合物的多元羧酸的制备方法
公开(公告)号：US06388038B1
公开(公告)日：2002-05-14
申请号：US09724009
申请日：2000-11-28
申请人： Tsuyoshi Hirata , Tsutomu Yuasa , Katsuhisa Shiote , Koichiro Nagare , Syogo Iwai
发明人： Tsuyoshi Hirata , Tsutomu Yuasa , Katsuhisa Shiote , Koichiro Nagare , Syogo Iwai
IPC分类号： C08F22210
CPC分类号： C04B24/267 , C04B24/2647 , C04B2103/302 , C04B2103/408 , C08F290/062 , C08G65/2609 , C08G65/3322 , C08L71/02 , Y10S526/932 , C08L2666/04
摘要： The present invention provides a method for producing a cement dispersant having high percentage in water reduction rate and appropriate air-entraining property. This method for producing a polycarboxylic acid for a cement dispersant is characterized in that alkylene oxide is added at a specific temperature range.
摘要翻译：本发明提供一种水分散剂的制造方法，该水泥分散剂具有高的降水率和合适的加气性能。该水泥分散剂用多元羧酸的制造方法的特征在于，在特定的温度范围加入环氧烷烃。

5. 发明授权

US6166112A Cement admixture and cement composition 失效
标题翻译：水泥外加剂和水泥组成
公开(公告)号：US6166112A
公开(公告)日：2000-12-26
申请号：US82835
申请日：1998-05-21
申请人： Tsuyoshi Hirata , Tsutomu Yuasa , Koichiro Nagare
发明人： Tsuyoshi Hirata , Tsutomu Yuasa , Koichiro Nagare
IPC分类号： C04B24/26 , C04B24/32 , C08F220/06 , C08F222/10 , C08F283/01 , C08F290/06 , C08F290/14 , C08G65/332 , C08L71/02 , C08K3/00
CPC分类号： C08G65/3322 , C04B24/2641 , C04B24/2647 , C04B24/32 , C08F220/06 , C08F222/1006 , C08F283/01 , C08F290/06 , C08F290/061 , C08F290/14 , C08F290/142 , C08L71/02 , C08L2205/05 , C08L2666/04
摘要： The invention provides: a cement admixture which has excellent cement dispersibility and can afford high slump retainability; and a cement composition which has excellent cement dispersibility and high slump retainability. The cement admixture comprises a polycarboxylic acid as an effective component, wherein the polycarboxylic acid is obtained by a process including the steps of: charging "a" parts by weight of a polyalkylene glycol (A) and "b" parts by weight of a (meth)acrylic acid monomer (B) into a reactor in the range of {(a/n.sup.1/2)/b}.times.100.ltoreq.200, wherein n is an average molar number of the added oxyalkylene groups in the polyalkylene glycol (A) and is a number of 1 to 300; carrying out an esterification reaction of the resultant mixture in the reactor, thus obtaining a polyalkylene glycol (meth)acrylate (C); and copolymerizing the resultant polyalkylene glycol (meth)acrylate (C) and the (meth)acrylic acid monomer (B), thus obtaining the polycarboxylic acid.
摘要翻译：本发明提供：具有优异的水泥分散性并能提供高坍落度保持性的水泥混合物; 和具有优异的水泥分散性和高坍落度保持性的水泥组合物。所述水泥混合物包含多元羧酸作为有效成分，其中所述多元羧酸通过包括以下步骤的方法获得：将“a”重量份的聚亚烷基二醇（A）和“b”份重量的（甲基）丙烯酸单体（B）加入到{（a / n + E，fra 1/2 + EE）/ b}×100≤200的范围内的反应器中，其中n是加入的氧化烯的平均摩尔数聚亚烷基二醇（A）中的基团数为1〜300; 在反应器中进行所得混合物的酯化反应，得到聚亚烷基二醇（甲基）丙烯酸酯（C）; 并使得到的聚亚烷基二醇（甲基）丙烯酸酯（C）和（甲基）丙烯酸单体（B）共聚，得到多元羧酸。

6. 发明授权

US6048916A Method for dispersion of cement 失效
标题翻译：水泥分散方法
公开(公告)号：US6048916A
公开(公告)日：2000-04-11
申请号：US831199
申请日：1997-04-02
申请人： Tsuyoshi Hirata , Tsutomu Yuasa , Katsuhisa Shiote , Shogo Iwai , Koichiro Nagare , Hideyuki Tahara
发明人： Tsuyoshi Hirata , Tsutomu Yuasa , Katsuhisa Shiote , Shogo Iwai , Koichiro Nagare , Hideyuki Tahara
IPC分类号： C04B24/26 , C04B24/32 , C07C67/08 , C08K3/00
CPC分类号： C04B24/2647 , C07C67/08 , C04B2103/408
摘要： A method for the dispersion of cement, which comprises incorporating in a cement composition consisting at least of cement and water a cement dispersing agent formed of a polymer obtained by polymerizing a monomer component containing an alkoxy polyalkylene glycol mono(meth)acrylic ester monomer produced by the interesterification of an alkoxy polyalkylene glycol and a (meth)acrylic ester. A cement composition comprising the cement dispersing agent, cement and water.
摘要翻译：一种用于水泥分散的方法，其包括将至少由水泥和水组成的水泥组合物掺入由通过聚合含有由烷氧基聚亚烷基二醇单（甲基）丙烯酸酯单体组成的单体组分而获得的聚合物形成的水泥分散剂，所述单体组分含有由烷氧基聚亚烷基二醇和（甲基）丙烯酸酯的酯交换。一种水泥组合物，包括水泥分散剂，水泥和水。

7. 发明授权

US5912284A Cement additive, its production process and use 失效
标题翻译：水泥添加剂，其生产工艺和用途
公开(公告)号：US5912284A
公开(公告)日：1999-06-15
申请号：US992328
申请日：1997-12-17
申请人： Tsuyoshi Hirata , Tsutomu Yuasa , Katsuhisa Shiote , Syogo Iwai , Koichiro Nagare
发明人： Tsuyoshi Hirata , Tsutomu Yuasa , Katsuhisa Shiote , Syogo Iwai , Koichiro Nagare
IPC分类号： C04B24/26 , C04B24/32 , C04B40/00 , C08F216/14 , C08F290/06 , C08L71/02 , C08K3/00
CPC分类号： C04B24/267 , C04B40/0039 , C08F216/1416 , C08F290/062 , C08L71/02 , C04B2103/308
摘要： The present invention provides a cement additive its production process and cement composition achieving excellent slump loss prevention capability. As a cement additive, there can be a copolymer (A-1) comprising an unsaturated polyalkylene glycol ether-based monomer (I), maleic acid-based monomer (II) and other monomer (III) copolymerizable with these monomers, the monomer (I)/monomer (II)/monomer (III) weight ratio being 50-99/50-1/0-49 and the weight average molecular weight of the copolymer (A) being 10,000 to 100,000 in terms of polyethylene glycol measured by gel permeation chromatography, or a copolymer (A) with an antifoaming agent (B), wherein the copolymer (A) comprises polyalkylene glycol ether-based units and dicarboxylic acid-based units as repeating units.
摘要翻译：本发明提供一种水泥添加剂，其生产工艺和水泥组合物具有优异的坍落度损失防止能力。作为水泥添加剂，可以使用与这些单体共聚的不饱和聚亚烷基二醇醚系单体（I），马来酸系单体（II）和其它单体（III）的共聚物（A-1），单体（ I）/单体（II）/单体（III）的重量比为50-99 / 50-1 / 0-49，共聚物（A）的重均分子量以聚乙二醇换算为10,000至100,000 渗透色谱法或与消泡剂（B）的共聚物（A），其中共聚物（A）包含聚亚烷基二醇醚基单元和二羧酸基单元作为重复单元。

8. 发明授权

US06384141B2 Anti-shrinkage agent for hydraulic material 失效
标题翻译：液压材料抗收缩剂
公开(公告)号：US06384141B2
公开(公告)日：2002-05-07
申请号：US09749619
申请日：2000-12-28
申请人： Tsuyoshi Hirata , Koichiro Nagare
发明人： Tsuyoshi Hirata , Koichiro Nagare
IPC分类号： C08L7102
CPC分类号： C04B24/2647 , C04B24/267 , C04B24/2694 , C04B2111/34
摘要： The present invention is related to a shrinkage reducing agent for hydraulic materials which comprises at least one polymer selected from the group consisting of (a) a polymer having a structure derived from the residue of a compound containing 2 to 30 carbon atoms and one active hydrogen atom by the binding thereto of one oxyalkylene chain having a carboxyl-containing side chain, (b) a polymer having a structure derived from the residue of a compound containing 4 to 30 carbon atoms and two active hydrogen atoms by the binding thereto of at least one oxyalkylene chain having a carboxyl-containing side chain, (c) a polymer having a structure derived from the residue of a compound containing 1 to 30 carbon atoms and at least three active hydrogen atoms by the binding thereto of at least one oxyalkylene chain having a carboxyl-containing side chain and (d) a polymer having a structure derived from the residue of an amine by the binding thereto one oxyalkylene chain having a carboxyl-containing side chain.
摘要翻译：本发明涉及用于水硬性材料的减缩剂，其包含至少一种选自以下的聚合物：（a）具有衍生自含有2至30个碳原子的化合物的残基的结构的聚合物和一种活性氢具有含羧基侧链的一个氧化烯链的结合的原子，（b）具有至少与含有羧基侧链结合的含有4至30个碳原子的化合物的残基的结构的聚合物和两个活性氢原子一个具有含羧基的侧链的氧化烯链，（c）具有衍生自含有1至30个碳原子和至少3个活性氢原子的化合物的残基的结构的聚合物与至少一个具有羧基侧链的氧化烯链的结合，含羧基侧链和（d）具有通过与一个具有羧基含量的氧化烯链结合而衍生自胺残基的结构的聚合物 g侧链。

9. 发明授权

US07049462B2 Production process for product of dehydration reaction and apparatus used for the production 失效
标题翻译：脱水反应产物的生产工艺和生产用的设备
公开(公告)号：US07049462B2
公开(公告)日：2006-05-23
申请号：US09993621
申请日：2001-11-27
申请人： Koichiro Nagare , Toru Uno , Yoshiyuki Onda , Tsutomu Yuasa , Masato Nishiue , Hisamoto Kawano
发明人： Koichiro Nagare , Toru Uno , Yoshiyuki Onda , Tsutomu Yuasa , Masato Nishiue , Hisamoto Kawano
IPC分类号： C07C69/52
CPC分类号： B01J19/0073 , B01D5/0012 , B01J19/0053 , B01J19/0066 , B01J19/1881 , B01J2219/00058 , B01J2219/00069 , B01J2219/00074 , B01J2219/00094 , B01J2219/00103 , B01J2219/00182 , B01J2219/00768 , B01J2219/00779 , C07C67/08 , C07C231/02 , F28D7/16 , F28F9/16 , F28F9/18 , Y02P20/149 , C07C69/54 , C07C233/38
摘要： It is an object of the present invention to provide a production method of a dehydration reaction product by which the occurrence of troubles in the production step or the degradation in performance characteristics or quality of various chemical products can be suppressed to a satisfactory extent.A production method of a dehydration reaction product which comprises a dehydration reaction step of subjecting a reaction solution containing a polymerizable compound to the dehydration reaction, said dehydration reaction step comprising using a dehydration reaction apparatus, said dehydration reaction apparatus comprising a reaction vessel, a condenser and a connecting pipe joining said reaction vessel with said condenser and satisfying the requirement: 0.05
摘要翻译：本发明的目的是提供一种脱水反应产物的生产方法，通过该方法可以将生产步骤中的麻烦的发生或各种化学产品的性能特性或质量的劣化抑制到令人满意的程度。脱水反应产物的制备方法包括使含有聚合性化合物的反应溶液进行脱水反应的脱水反应步骤，所述脱水反应步骤包括使用脱水反应装置，所述脱水反应装置包括反应容器，冷凝器以及将所述反应容器与所述冷凝器连接的连接管，并满足以下要求：<？in-line-formula description =“In-line formula”end =“lead”？> 0.05 <（B < / A）<35 <？in-line-formula description =“In-line Formulas”end =“tail”？>其中A是所述反应容器的容量（m 3），B是所述连接管的总长度（m）在水平的基础上。

10. 发明授权

US5834576A Acrylic acid derivatives, method for preparing the acrylic acid derivatives, and acrylic acid polymers 失效
标题翻译：丙烯酸衍生物，丙烯酸衍生物的制备方法和丙烯酸聚合物
公开(公告)号：US5834576A
公开(公告)日：1998-11-10
申请号：US607605
申请日：1996-02-27
申请人： Hideaki Nagano , Koichi Nakagawa , Keiji Yurugi , Mitsuaki Makino , Tsuyoshi Hirata , Koichiro Nagare , Yuichi Kita
发明人： Hideaki Nagano , Koichi Nakagawa , Keiji Yurugi , Mitsuaki Makino , Tsuyoshi Hirata , Koichiro Nagare , Yuichi Kita
IPC分类号： C04B24/26 , C07C59/58 , C07C67/31 , C07C69/734 , C07H15/04 , C08F220/64
CPC分类号： C07H15/04 , C04B24/2641 , C07C59/58 , C07C67/31 , C07C69/734
摘要： A novel acrylic ester which is represented by general formula (2) ##STR1## wherein R.sub.1 and R.sub.2 independently represent a hydrogen atom or an organic residue, R.sub.3 represents an organic residue, n is a positive number among 1 to 3, and m is a positive number among 1 to 100 and which is applicable to various uses, is obtained by reacting an acrylic ester of general formula (3) ##STR2## wherein R.sub.1 represents a hydrogen atom or an organic residue, and R.sub.3 represents an organic residue, with a cyclic ether compound of general formula (4) ##STR3## wherein R.sub.2 represents a hydrogen atom or an organic residue, and n is a positive number among 1 to 3. Moreover, a novel acrylic acid derivative whose use is even wider is obtained by hydrolyzing the acrylic acid derivative.
摘要翻译：一种由通式（2）表示的新型丙烯酸酯其中R1和R2独立地表示氢原子或有机残基，R3表示有机残基，n为1〜3的正数， m为1〜100的正数，适用于各种用途，通过使通式（3）的丙烯酸酯与其中R 1表示氢原子或有机残基反应而得到，其中R 3表示具有通式（4）的环状醚化合物或有机残基的有机残基，n为1〜3的正数。此外，使用更宽的新型丙烯酸衍生物通过水解丙烯酸酸衍生物。

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