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1. 发明授权

US4909942A Process for removing pyrogens 失效
标题翻译：去除热原的方法
公开(公告)号：US4909942A
公开(公告)日：1990-03-20
申请号：US256729
申请日：1988-10-12
申请人： Tadashi Sato , Taizo Watanabe , Satoshi Minobe , Takashi Nishimura , Masahiro Kagotani , Tomonobu Ase , Zenjiro Honda , Shinji Nagamatsu
发明人： Tadashi Sato , Taizo Watanabe , Satoshi Minobe , Takashi Nishimura , Masahiro Kagotani , Tomonobu Ase , Zenjiro Honda , Shinji Nagamatsu
IPC分类号： A61K9/08 , A61L2/02 , B01D15/00 , B01D61/14 , B01D61/58 , C02F1/28 , C02F1/44
CPC分类号： B01D61/145 , A61L2/022 , B01D15/00 , C02F1/444
摘要： Pyrogens are removed out of a solution thereof by (1) treating the solution with a membrane and then (2) treating the resulting solution with a pyrogen adsorbent. The obtained solution is useful in pharmaceutical fields.

2. 发明授权

US4537997A Process for treating hydroformylation catalyst 失效
标题翻译：处理加氢甲酰化催化剂的方法
公开(公告)号：US4537997A
公开(公告)日：1985-08-27
申请号：US557763
申请日：1983-12-02
申请人： Hidetaka Kojima , Takeshi Horikawa , Masahiro Kagotani
发明人： Hidetaka Kojima , Takeshi Horikawa , Masahiro Kagotani
IPC分类号： C07C45/50 , B01J31/40 , B01J38/48 , C07B61/00 , C07C45/00 , C07C45/49 , C07C45/80 , C07C47/02 , C07C67/00
CPC分类号： B01J31/24 , B01J31/2404 , B01J31/4046 , C07C45/49 , C07C45/80 , B01J2231/321 , B01J2531/822 , Y02P20/584
摘要： In a process for producing an aldehyde by hydroformylating allyl alcohol with carbon monoxide and hydrogen gas in the presence of a catalyst comprising a rhodium compound and a tertiary phosphine in an organic solvent and separating the resulting aldehyde with water extraction from the reaction mixture, the catalyst is maintained and recovered in the activity by treating the catalyst-containing solution in the organic solvent with a gaseous mixture of carbon monoxide and hydrogen gas after the water extraction step.
摘要翻译：在通过在一种有机溶剂中包含铑化合物和叔膦的催化剂存在下，用一氧化碳和氢气将烯丙醇加氢甲酰化制备醛的方法中，用反应混合物中的水提取将得到的醛分离出来，通过在水提取步骤之后用一氧化碳和氢气的气体混合物处理有机溶剂中的含催化剂的溶液来维持和回收活性。

3. 发明授权

US5653853A Method of removing iodine compounds from crude acetic anhydride 失效
标题翻译：从粗乙酸酐中除去碘化合物的方法
公开(公告)号：US5653853A
公开(公告)日：1997-08-05
申请号：US657427
申请日：1996-06-03
申请人： Masahiro Kagotani , Yasuo Tsuji
发明人： Masahiro Kagotani , Yasuo Tsuji
IPC分类号： C07B61/00 , C07C51/12 , C07C51/44 , C07C51/54 , C07C51/573 , C07C53/08 , C07C53/12 , B01D3/06 , B01D3/34
CPC分类号： C07C51/573 , Y10S203/20
摘要： A process by which iodine compounds contained in crude acetic anhydride or a mixture of crude acetic anhydride and crude acetic acid can be converted into methyl iodide having a low boiling point and which can be separated by distillation and efficiently removed by the combination of the conversion step with the heat treatment step and distillation step. The process includes the steps of heat-treating the crude acetic anhydride or the mixture of crude acetic anhydride and crude acetic acid in the presence of methanol and/or methyl acetate in a treatment tank and distilling the heat-treated crude acetic anhydride or the heat-treated mixture of crude acetic anhydride and crude acetic acid, in the presence of an alkali metal salt and/or an alkaline earth metal salt if necessary.
摘要翻译：将粗制乙酸酐或粗乙酸酐与粗乙酸的混合物中含有的碘化合物转化成沸点低的甲基碘，通过蒸馏分离并通过转化步骤的组合有效除去的方法用热处理步骤和蒸馏步骤。该方法包括在处理槽中在甲醇和/或乙酸甲酯的存在下，将粗乙酸酐或粗乙酸酐与粗乙酸的混合物进行热处理并蒸馏经热处理的粗乙酸酐或热如果需要，在碱金属盐和/或碱土金属盐的存在下，将粗乙酸酐和粗乙酸的混合物混合。

4. 发明授权

US5625095A Process for producing high purity acetic acid 失效
标题翻译：生产高纯度乙酸的方法
公开(公告)号：US5625095A
公开(公告)日：1997-04-29
申请号：US458348
申请日：1995-06-02
申请人： Hiroyuki Miura , Masahiko Shimizu , Takashi Sato , Yoshiaki Morimoto , Masahiro Kagotani
发明人： Hiroyuki Miura , Masahiko Shimizu , Takashi Sato , Yoshiaki Morimoto , Masahiro Kagotani
IPC分类号： C07C51/12 , C07C51/44
CPC分类号： C07C51/12 , C07C51/44
摘要： A high purity acetic acid is prepared by reacting methanol with carbon monoxide in the presence of a rhodium catalyst, iodide salts, and methyl iodide, wherein an acetaldehyde concentration in the reaction liquid is maintained at 400 ppm or lower. This may be attained by contacting the liquid containing carbonyl impurities with water to separate and remove the carbonyl impurities. After that, the liquid can be returned to the reactor.
摘要翻译：在铑催化剂，碘化物盐和碘甲烷的存在下，使甲醇与一氧化碳反应制备高纯度乙酸，其中反应液中的乙醛浓度保持在400ppm以下。这可以通过使含有羰基杂质的液体与水接触以分离和除去羰基杂质来实现。之后，液体可以返回到反应器。

5. 发明授权

US5981425A Photocatalyst-containing coating composition 有权
标题翻译：含光催化剂的涂料组合物
公开(公告)号：US5981425A
公开(公告)日：1999-11-09
申请号：US285056
申请日：1999-04-02
申请人： Hiroshi Taoda , Toru Nonami , Takaaki Fujiwa , Masahiro Kagotani
发明人： Hiroshi Taoda , Toru Nonami , Takaaki Fujiwa , Masahiro Kagotani
IPC分类号： B01J35/00 , B01J27/14 , B01J21/06 , B01J27/182
CPC分类号： B01J35/004 , B01J35/002
摘要： A coating composition which is excellent in water resistance, weatherability and durability and can maintain its appearance for a prolonged period of time can be provided. A coating composition comprising a coating component and a photocatalyst containing calcium phosphate and titanium oxide is disclosed. As the photocatalyst, use is made of titanium oxide particles partially covered thereon with calcium phosphate, or porous body coated thereon with a film of titanium oxide, the film of titanium oxide being further covered partially thereon with calcium phosphate. The crystal form of titanium oxide is preferably anatase. The organic coating includes vinyl-type synthetic resin emulsions, and the inorganic coating is e.g. a solution containing a metal alkoxide for forming a film by a sol-gel method.
摘要翻译：可以提供耐水性，耐气候性和耐久性优异并能够长时间保持其外观的涂料组合物。公开了一种包含涂料组分和含有磷酸钙和氧化钛的光催化剂的涂料组合物。作为光催化剂，使用部分被磷酸钙覆盖的氧化钛粒子或其上涂覆有氧化钛膜的多孔体，二氧化钛膜还被磷酸钙部分地覆盖。氧化钛的晶体形式优选为锐钛矿型。有机涂层包括乙烯基型合成树脂乳液，无机涂层是例如。含有通过溶胶 - 凝胶法形成膜的金属醇盐的溶液。

6. 发明授权

US5672744A Process for the preparation of acetic acid 失效
标题翻译：乙酸的制备方法
公开(公告)号：US5672744A
公开(公告)日：1997-09-30
申请号：US459161
申请日：1995-06-02
申请人： Masahiro Kagotani , Yasuteru Kajikawa
发明人： Masahiro Kagotani , Yasuteru Kajikawa
IPC分类号： B01J31/26 , C07B61/00 , C07C51/12 , C07C53/08
CPC分类号： C07C51/12
摘要： By employing a process for the preparation of acetic acid which comprises carbonylating methanol with carbon monoxide in a first reactor in the presence of a reaction fluid comprising a rhodium catalyst, methyl iodide, an iodide salt, methyl acetate and water, while continuously withdrawing the reaction fluid from the first reactor and introducing it into a flash zone to separate it into an evaporated part and an unevaporated part, characterized in that second reactor is provided between the first reactor and the flash zone and methanol is carbonylated with the carbon monoxide contained in the reaction fluid in a state in which it is dissolved therein in the second reactor with a residence time of 7 to 60 seconds at 150.degree. to 220.degree. C., the carbon monoxide contained in the reaction fluid withdrawn from the first reactor in a state in which it is dissolved therein can be converted into acetic acid in the second reactor through the same carbonylation as that occurring in the first reactor, which enables effective use and high recovery of carbon monoxide.
摘要翻译：通过采用一种制备乙酸的方法，该方法包括在包含铑催化剂，甲基碘，碘化物盐，乙酸甲酯和水的反应流体存在下，在第一反应器中用一氧化碳羰基化甲醇，同时连续地抽出反应流体从第一反应器并将其引入闪蒸区以将其分离成蒸发部分和未蒸发部分，其特征在于，在第一反应器和闪蒸区之间提供第二反应器，并且甲醇与包含在第一反应器中的一氧化碳羰基化在第二反应器中以150℃至220℃停留时间为7至60秒的状态将反应流体以第一反应器中的状态从第一反应器中排出的一氧化碳其溶解在其中可以通过与在第一反应器中发生的相同的羰基化在第二反应器中转化为乙酸可以有效利用和高回收一氧化碳。

7. 发明授权

US4937081A Process for producing porous, spherical particles 失效
标题翻译：生产多孔，球形颗粒的方法
公开(公告)号：US4937081A
公开(公告)日：1990-06-26
申请号：US144042
申请日：1988-01-14
申请人： Masahiro Kagotani
发明人： Masahiro Kagotani
IPC分类号： A61K9/16 , C08J3/14
CPC分类号： C08J3/14 , A61K9/1652 , C08J2301/10
摘要： A process for producing porous, spherical particles of cellulose fatty acid esters which comprises dissolving a cellulose fatty acid ester and a gelling agent therefor in an organic solvent, adding the solution thus obtained to an aqueous medium with stirring to form droplets, converting said droplets to gel particles of cellulose fatty acid ester in the presence or absence of a gelation accelerator, and separating porous, spherical particles of cellulose fatty acid ester.
摘要翻译：一种生产纤维素脂肪酸酯的多孔，球形颗粒的方法，其包括将纤维素脂肪酸酯和其胶凝剂溶于有机溶剂中，将所得溶液在搅拌下加入到水性介质中以形成液滴，将所述液滴转化为在存在或不存在凝胶促进剂的情况下，将纤维素脂肪酸酯的凝胶颗粒分离，并分离出纤维素脂肪酸酯的多孔，球形颗粒。

8. 发明授权

US4764605A Process for selectively deacetylating acetyl derivatives of saccharides 失效
标题翻译：选择性脱乙酰化糖类的乙酰衍生物的方法
公开(公告)号：US4764605A
公开(公告)日：1988-08-16
申请号：US809970
申请日：1985-12-17
申请人： Stephen Hanessian , Masahiro Kagotani
发明人： Stephen Hanessian , Masahiro Kagotani
IPC分类号： C07H1/00 , C07H13/04 , C07H15/04 , C07G3/00 , C07G17/00 , C07H15/00
CPC分类号： C07H13/04 , C07H1/00 , C07H15/04
摘要： A process for selectively deacetylating an acetyl derivative of a saccharide is described, comprising treating an acetyl derivative of a monosaccharide or oligosaccharide using a mixture of an aqueous solution of alkali metal hydroxide/aqueous hydrogen peroxide/organic solvent to selectively hydrolyze acetate bonds at specific positions in the molecule, and thereby obtain a partially hydrolyzed acetyl derivative of a saccharide.
摘要翻译：描述了选择性脱乙酰化糖类的乙酰衍生物的方法，包括使用碱金属氢氧化物水溶液/过氧化氢水溶液/有机溶剂的混合物处理单糖或寡糖的乙酰衍生物，以选择性地水解特定位置的乙酸根在分子中，从而得到部分水解的糖的乙酰衍生物。

9. 发明授权

US4603020A Preparation of acetyl compounds 失效
标题翻译：乙酰化合物的制备
公开(公告)号：US4603020A
公开(公告)日：1986-07-29
申请号：US624635
申请日：1984-06-26
申请人： Hidetaka Kojima , Masahiro Kagotani
发明人： Hidetaka Kojima , Masahiro Kagotani
IPC分类号： C07C53/12 , B01J31/00 , B01J31/20 , B01J31/28 , C07B61/00 , C07C27/00 , C07C51/00 , C07C51/56 , C07C53/122 , C07C67/00 , C07C51/54
CPC分类号： C07C51/56
摘要： An O-acetyl compound, such as acetic anhydride, is prepared by carbonylating the corresponding O-methyl compound, such as methyl acetate, by heating the latter at 130.degree. to 250.degree. C. with carbon monoxide of a partial pressure of 1 to 100 kg/cm.sup.2 G in the presence of a rhodium catalyst and a iodine compound, whereby the reaction is caused to take place in a reaction solution containing a carboxylic acid in the presence of an aluminum accelerator and a rhodium catalyst treated with hydrogen.
摘要翻译：通过将相应的O-甲基化合物如乙酸甲酯羰基化，通过将其在130-250℃下加热，分压为1至100的一氧化碳来制备O-乙酰基化合物，例如乙酸酐 kg / cm 2，在铑催化剂和碘化合物的存在下，在铝加速剂和用氢处理的铑催化剂的存在下，在含有羧酸的反应溶液中进行反应。

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