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1. 发明申请

US20120202144A1 PELLICLE AND MASK ADHESIVE THEREFOR 有权
标题翻译：油漆和面膜粘合剂
公开(公告)号：US20120202144A1
公开(公告)日：2012-08-09
申请号：US13500513
申请日：2010-10-06
申请人： Shuichi Murakami , Takashi Kozeki , Minehiro Mori
发明人： Shuichi Murakami , Takashi Kozeki , Minehiro Mori
IPC分类号： G03F1/62 , C09J123/20
CPC分类号： C09J123/10 , C08L23/10 , C08L23/142 , C08L23/145 , C08L23/18 , C08L2205/02 , C08L2666/06 , C08L2666/08 , C09J153/025 , G03F1/64
摘要： Disclosed is a pellicle having a mask adhesive layer having appropriate softness, having a small adhesive residue after being peeled off from a mask, and having good handling characteristics; and a pellicle for preventing position deviation of patterns, in particular in double patterning. The pellicle of the present invention includes a pellicle frame, a pellicle membrane disposed on one end surface of the pellicle frame, and a mask adhesive layer disposed on other end surface of the pellicle frame; wherein the mask adhesive layer includes 35 to 170 weight parts of a hardness adjuster (B) containing a polypropylene (b1) and a propylene based elastomer (b2) per 100 weight parts of a styrene resin (A); and in an electron microscopic photograph of the mask adhesive layer, a phase-separated structure of a continuous phase of the styrene resin (A) and a discontinuous phase of the hardness adjuster (B) is observed.
摘要翻译：公开了一种具有适当柔软度的掩模粘合剂层的防护薄膜组件，在从掩模剥离之后具有小的粘合剂残留物，并且具有良好的处理特性; 以及用于防止图案的位置偏移的防护薄片，特别是在双重图案化中。本发明的防护薄膜组件包括防护薄膜组件框架，设置在防护膜框架的一个端面上的防护薄膜组件和设置在防护薄膜组件框架的另一个端面上的掩模粘合剂层; 其中，所述掩模粘合剂层每100重量份苯乙烯树脂（A）含有35〜170重量份含有聚丙烯（b1）和丙烯系弹性体（b2）的硬度调节剂（B）并且在掩模粘合剂层的电子显微镜照片中，观察到苯乙烯树脂（A）的连续相的相分离结构和硬度调节剂（B）的不连续相。

2. 发明授权

US08685598B2 Pellicle and mask adhesive therefor 有权
标题翻译：防护薄膜和面膜粘合剂
公开(公告)号：US08685598B2
公开(公告)日：2014-04-01
申请号：US13500513
申请日：2010-10-06
申请人： Shuichi Murakami , Takashi Kozeki , Minehiro Mori
发明人： Shuichi Murakami , Takashi Kozeki , Minehiro Mori
IPC分类号： G03F1/00 , C08L23/00
CPC分类号： C09J123/10 , C08L23/10 , C08L23/142 , C08L23/145 , C08L23/18 , C08L2205/02 , C08L2666/06 , C08L2666/08 , C09J153/025 , G03F1/64
摘要： Disclosed is a pellicle having a mask adhesive layer having appropriate softness, having a small adhesive residue after being peeled off from a mask, and having good handling characteristics; and a pellicle for preventing position deviation of patterns, in particular in double patterning. The pellicle of the present invention includes a pellicle frame, a pellicle membrane disposed on one end surface of the pellicle frame, and a mask adhesive layer disposed on other end surface of the pellicle frame; wherein the mask adhesive layer includes 35 to 170 weight parts of a hardness adjuster (B) containing a polypropylene (b1) and a propylene based elastomer (b2) per 100 weight parts of a styrene resin (A); and in an electron microscopic photograph of the mask adhesive layer, a phase-separated structure of a continuous phase of the styrene resin (A) and a discontinuous phase of the hardness adjuster (B) is observed.
摘要翻译：公开了一种具有适当柔软度的掩模粘合剂层的防护薄膜组件，在从掩模剥离之后具有小的粘合剂残留物，并且具有良好的处理特性; 以及用于防止图案的位置偏移的防护薄片，特别是在双重图案化中。本发明的防护薄膜组件包括防护薄膜组件框架，设置在防护膜框架的一个端面上的防护薄膜组件和设置在防护薄膜组件框架的另一个端面上的掩模粘合剂层; 其中，所述掩模粘合剂层每100重量份苯乙烯树脂（A）含有35〜170重量份含有聚丙烯（b1）和丙烯系弹性体（b2）的硬度调节剂（B）并且在掩模粘合剂层的电子显微镜照片中，观察到苯乙烯树脂（A）的连续相的相分离结构和硬度调节剂（B）的不连续相。

3. 发明申请

US20050165196A1 Adhesive resin and film adhesive made by using the same 审中-公开
标题翻译：粘合树脂和使用该胶粘剂制成的胶粘剂
公开(公告)号：US20050165196A1
公开(公告)日：2005-07-28
申请号：US10512064
申请日：2003-05-29
申请人： Jin Kinoshita , Moritsugu Morita , Minehiro Mori , Yoichi Kodama
发明人： Jin Kinoshita , Moritsugu Morita , Minehiro Mori , Yoichi Kodama
IPC分类号： C08G73/10 , C08L63/00 , C09J7/00 , C09J179/08 , H01L21/58 , C08G77/26
CPC分类号： C09J179/08 , C08G73/1042 , C08G73/105 , C08G73/106 , C08L63/00 , C08L2666/22 , C09J7/10 , C09J2203/326 , C09J2479/08 , H01L24/83 , H01L2224/8385 , H01L2924/09701 , H01L2924/10253 , H01L2924/14 , H01L2924/3512 , H01L2924/00
摘要： The adhesive resin of the invention comprises a polyimide resin obtained by reacting a diamine component containing the compound (1) as an essential component with a tetracarboxylic dianhydride component. The diamine component contains a silicone diamine having a specific structure and/or the tetracarboxylic dianhydride component contains a silicone acid dianhydride having a specific structure. Film adhesives made by using the adhesive resin preferably together with a thermosetting resin, and, if necessary, an inorganic filler are excellent in low-temperature adhesion, resistance to moisture absorption, heat resistance, and workability in adhesive adhering and are favorably usable as semiconductor-mounting materials for adhering semiconductor elements to substrates.
摘要翻译：本发明的粘合树脂包括通过使含有作为必需成分的化合物（1）的二胺成分与四羧酸二酐成分反应得到的聚酰亚胺树脂。二胺组分含有具有特定结构的硅氧烷二胺和/或四羧酸二酐组分含有具有特定结构的硅酸二酐。通过使用粘合剂树脂优选与热固性树脂一起制成的胶粘剂，并且如果需要，可以根据需要使用无机填料，粘合剂粘合性低，耐吸湿性，耐热性，加工性优异，有利于半导体 - 用于将半导体元件粘附到基板的安装材料。

4. 发明授权

US07223480B2 Metal laminate and etching method therefor 失效
标题翻译：金属层压板及其蚀刻方法
公开(公告)号：US07223480B2
公开(公告)日：2007-05-29
申请号：US10500846
申请日：2003-07-28
申请人： Koji Hirota , Masanao Kobayashi , Minehiro Mori , Naoki Nakazawa
发明人： Koji Hirota , Masanao Kobayashi , Minehiro Mori , Naoki Nakazawa
IPC分类号： B32B15/08 , B32B15/18 , G11B5/00 , G11B21/00 , H01B13/00
CPC分类号： H05K3/002 , G11B5/4833 , H05K1/0346 , H05K1/056 , H05K3/0041 , H05K3/385 , H05K2201/0154 , H05K2203/0315 , H05K2203/163 , Y10T428/12951 , Y10T428/265 , Y10T428/31681
摘要： The present invention relates to a metal laminate which is broadly used for a flexible wiring board or the like and an etching method therefor. In particular, the present invention relates to a metal laminate which includes a layer obtained by laminating a metal layer and an insulating layer, where the insulating layer is subjected to an etching process, wherein, in a surface of the metal layer which is positioned so as to come in contact with the insulating layer, respective concentrations of main metal element and oxygen element constituting the metal layer are measured from the surface of the metal layer towards inside of the metal layer in a time-elapsing manner according to AES (Auger electron spectroscopy) and a value of the thickness of a metal oxide film of the surface of the metal layer measured at a time when atomic concentrations of the main metal element and the oxygen element constituting the metal layer become equal to each other is in a range of at least 0 Å to less than 50 Å.According to the present invention, an etching time of polyimide in the polyimide metal laminate can be calculated and a flexure used for a suspension for a hard disc drive having a high productivity can be provided.
摘要翻译：本发明涉及广泛用于柔性布线板等的金属层压体及其蚀刻方法。特别地，本发明涉及一种金属层压体，其包括通过层压金属层和绝缘层而获得的层，其中绝缘层进行蚀刻处理，其中在该金属层的表面上为了与绝缘层接触，根据AES（俄歇电子学（俄歇电子学），从金属层的表面到金属层的内部）以时间流逝的方式测量构成金属层的主要金属元素和氧元素的各自浓度光谱），并且在构成金属层的主金属元素和氧元素的原子浓度变得相等的时刻测量的金属层的表面的金属氧化物膜的厚度的值在至少从0到小于50。根据本发明，可以计算聚酰亚胺金属层叠体中的聚酰亚胺的蚀刻时间，并且可以提供用于具有高生产率的硬盘驱动器的悬架的挠曲。

5. 发明授权

US06340518B1 Flexible metal-clad laminates and preparation of the same 有权
标题翻译：柔性金属复合层压板及其制备方法
公开(公告)号：US06340518B1
公开(公告)日：2002-01-22
申请号：US09268684
申请日：1999-03-16
申请人： Mikio Kitahara , Minehiro Mori , Naoshi Mineta , Takashi Kayama
发明人： Mikio Kitahara , Minehiro Mori , Naoshi Mineta , Takashi Kayama
IPC分类号： B32B702
CPC分类号： B32B15/08 , B32B7/02 , B32B27/34 , H05K1/0346 , Y10T428/24959 , Y10T428/24967 , Y10T428/26 , Y10T428/266 , Y10T428/31681 , Y10T428/31721
摘要： A flexible metal foil laminate sheet wherein a polyimide layer comprises a polyimide laminate having a three-layer structure in which thermoplastic polyimide layers are formed on both the surfaces of a polyimide film; metal foil layers are heated and pressed against both the sides of the polyimide laminate; and the thickness of the thermoplastic polyimide layer is 100% or more of an average roughness at 10 points on the surface of the metal foil which contacts the thermoplastic polyimide layer; and a method for manufacturing the flexible metal foil laminate sheet. According to the present invention, there can be manufactured the flexible metal foil laminate sheet in which a necessary and sufficient adhesive force is present in an interface between a metal foil and an insulating layer and which is excellent in heat resistance, chemical resistance, electrical properties and the like.
摘要翻译：一种柔性金属箔层压片，其中聚酰亚胺层包括具有三层结构的聚酰亚胺层压体，其中热塑性聚酰亚胺层形成在聚酰亚胺膜的两个表面上; 金属箔层被加热并压在聚酰亚胺层压板的两侧; 并且热塑性聚酰亚胺层的厚度在与热塑性聚酰亚胺层接触的金属箔的表面上的10点处的平均粗糙度为100％以上; 以及柔性金属箔层压片的制造方法。根据本发明，可以制造在金属箔和绝缘层之间的界面中存在必要且充分的粘合力的柔性金属箔层压片，并且其耐热性，耐化学性，电性能等等。

6. 发明申请

US20050087509A1 Metal laminate and method of etching the same 失效
标题翻译：金属层压板及其蚀刻方法
公开(公告)号：US20050087509A1
公开(公告)日：2005-04-28
申请号：US10500846
申请日：2003-07-28
申请人： Koji Hirota , Masano Kobayashi , Minehiro Mori , Naoki Nakazawa
发明人： Koji Hirota , Masano Kobayashi , Minehiro Mori , Naoki Nakazawa
IPC分类号： G11B5/48 , H05K1/03 , H05K1/05 , H05K3/00 , H05K3/38 , H01B13/00
CPC分类号： H05K3/002 , G11B5/4833 , H05K1/0346 , H05K1/056 , H05K3/0041 , H05K3/385 , H05K2201/0154 , H05K2203/0315 , H05K2203/163 , Y10T428/12951 , Y10T428/265 , Y10T428/31681
摘要： The present invention relates to a metal laminate which is broadly used for a flexible wiring board or the like and an etching method therefor. In particular, the present invention relates to a metal laminate which includes a layer obtained by laminating a metal layer and an insulating layer, where the insulating layer is subjected to an etching process, wherein, in a surface of the metal layer which is positioned so as to come in contact with the insulating layer, respective concentrations of main metal element and oxygen element constituting the metal layer are measured from the surface of the metal layer towards inside of the metal layer in a time-elapsing manner according to AES (Auger electron spectroscopy) and a value of the thickness of a metal oxide film of the surface of the metal layer measured at a time when atomic concentrations of the main metal element and the oxygen element constituting the metal layer become equal to each other is in a range of at least 0 Å to less than 50 Å. According to the present invention, an etching time of polyimide in the polyimide metal laminate can be calculated and a flexure used for a suspension for a hard disc drive having a high productivity can be provided.
摘要翻译：本发明涉及广泛用于柔性布线板等的金属层压体及其蚀刻方法。特别地，本发明涉及一种金属层压体，其包括通过层压金属层和绝缘层而获得的层，其中绝缘层进行蚀刻处理，其中在该金属层的表面上为了与绝缘层接触，根据AES（俄歇电子学（俄歇电子学），从金属层的表面到金属层的内部）以时间流逝的方式测量构成金属层的主要金属元素和氧元素的各自浓度光谱），并且在构成金属层的主金属元素和氧元素的原子浓度变得相等的时刻测量的金属层的表面的金属氧化物膜的厚度的值在至少从0到小于50。根据本发明，可以计算聚酰亚胺金属层叠体中的聚酰亚胺的蚀刻时间，并且可以提供用于具有高生产率的硬盘驱动器的悬架的挠曲。

7. 发明授权

US06737503B2 Aromatic diamine and polyimide thereof 失效
标题翻译：芳族二胺及其聚酰亚胺
公开(公告)号：US06737503B2
公开(公告)日：2004-05-18
申请号：US10232744
申请日：2002-09-03
申请人： Yoichi Kodama , Minehiro Mori , Naoshi Nagai , Masaru Kawaguchi
发明人： Yoichi Kodama , Minehiro Mori , Naoshi Nagai , Masaru Kawaguchi
IPC分类号： C08G7310
CPC分类号： C08G73/1071 , C08G73/1039 , C08G73/105
摘要： The aromatic diamine compound of the present invention is represented by the following formula (1), and from the aromatic diamine compound a polyimide having a repeating unit represented by the following formula (4), which has low-temperature adherability, can be obtained. In the formulas (1) and (4), n is an integer of 3 to 7, each R is independently an atom or a group selected from the group consisting of a hydrogen atom, a halogen atom and a hydrocarbon group, the same or different two hetero atoms selected from nitrogen atoms and oxygen atoms bonded to each benzene ring are at the ortho- or meta-positions to each other on at least one benzene ring, and when n is 3, the hetero atoms are at the ortho- or meta-positions to each other on all the benzene rings. In the formula (4), Y is a tetravalent organic group.
摘要翻译：本发明的芳香族二胺化合物由下式（1）表示，由芳族二胺化合物得到具有低温粘合性的下述式（4）表示的重复单元的聚酰亚胺。在式（1）和（4）中，n为3〜7的整数，R各自独立地为选自氢原子，卤素原子和烃基的原子或基团，相同或选自与每个苯环键合的氮原子和氧原子的不同的两个杂原子在至少一个苯环上彼此相邻或间位，当n为3时，杂原子处于邻位或间隔在所有苯环上彼此相互排列。在式（4）中，Y是四价有机基团。

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