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1. 发明申请

US20090064752A1 PROCESS FOR STRAIGHTENING TUBE AND METHOD FOR PRODUCING TUBE THEREWITH 有权
公开(公告)号：US20090064752A1
公开(公告)日：2009-03-12
申请号：US12247912
申请日：2008-10-08
申请人： SATOSHI TSUYUGUCHI , Kouichi Kuroda , Tomio Yamakawa
发明人： SATOSHI TSUYUGUCHI , Kouichi Kuroda , Tomio Yamakawa
IPC分类号： B21D9/04
CPC分类号： B21D3/04
摘要： In straightening a tube using a roll straightening machine provided with drum type straightening roll pairs vertically opposingly disposed, at least an outer layer portion of a roll main body is made of elastic material having spring type hardness Hs (JIS K 6301 A type) of 50 to 100 in at least three pairs of straightening rolls on an outlet side of the roll straightening machine, and an offset amount is imparted to a tube engaged in the three pairs, at least, of straightening opposing rolls such that η defined by an equation (1) ranges from 1.0×10−3 to 1.5×10−3. The offset amount is set at each of three positions along a tube axis where the upper and lower rolls of each pair horizontally cross. Therefore, an S/N ratio can be enhanced in an eddy current test from inside of the tube to improve inspection efficiency, and excellent quality accuracy can be ensured in a heat transfer tube used in a steam generator and the like. [ Formula   1 ] η = 1 R × ( d 2 ) ( 1 ) where a relationship of R=(δ2+L2)/2δ holds, assuming that d (mm) is a tube outside diameter, L (mm) is a roll stand span of the roll straightening machine, and δ (mm) is an offset amount.

2. 发明授权

US07654122B2 Process for straightening a tube 有权
标题翻译：矫直管的工艺
公开(公告)号：US07654122B2
公开(公告)日：2010-02-02
申请号：US12247912
申请日：2008-10-08
申请人： Satoshi Tsuyuguchi , Kouichi Kuroda , Tomio Yamakawa
发明人： Satoshi Tsuyuguchi , Kouichi Kuroda , Tomio Yamakawa
IPC分类号： B21D1/02 , B21B19/02
CPC分类号： B21D3/04
摘要： In straightening a tube using a roll straightening machine provided with drum type straightening roll pairs vertically opposingly disposed, at least an outer layer portion of a roll main body is made of elastic material having spring type hardness Hs (JIS K 6301 A type) of 50 to 100 in at least three pairs of straightening rolls on an outlet side of the roll straightening machine, and an offset amount is imparted to a tube engaged in the three pairs, at least, of straightening opposing rolls such that η defined by an equation (1) ranges from 1.0×10−3 to 1.5×10−3. The offset amount is set at three positions along a tube axis where the upper and lower rolls of each pair horizontally cross. Therefore, an S/N ratio can be enhanced in an eddy current test from inside of the tube to improve inspection efficiency, and excellent quality accuracy can be ensured in a heat transfer tube used in a steam generator and the like. [ Formula ⁢ ⁢ 1 ] η = 1 R × ( d 2 ) ( 1 ) where a relationship of R=(δ2+L2)/2δ holds, assuming that d (mm) is a tube outside diameter, L (mm) is a roll stand span of the roll straightening machine, and δ (mm) is an offset amount.
摘要翻译：在使用设置有垂直相对设置的滚筒式矫直辊对的辊矫正机矫直管时，至少辊主体的外层部分由弹簧型硬度Hs（JIS K 6301A型）为50的弹性材料制成至少在辊矫直机的出口侧的三对矫正辊中至少100个，并且至少对对置的三个对的管赋予偏移量，使得由等式（ 1）的范围为1.0×10 -3〜1.5×10 -3。偏移量设置在沿着每个对的上下辊的横轴交叉的管轴的三个位置处。因此，可以在管内部的涡流试验中提高S / N比，提高检查效率，并且可以确保在蒸汽发生器等中使用的传热管中具有优良的质量精度。假设d（mm）为管外径，则L（mm）为R =（delta2 + L2）/ 2delta的关系为[公式1] 1 = 1 R x（d 2）（1）辊矫正机的轧辊架跨距，delta（mm）是偏移量。

3. 发明申请

US20120304724A1 METHOD FOR STRAIGHTENING TUBE AND STRAIGHTENING ROLL 有权
标题翻译：用于连接管和连接辊的方法
公开(公告)号：US20120304724A1
公开(公告)日：2012-12-06
申请号：US13589342
申请日：2012-08-20
申请人： Yoshiyuki KUROIWA , Kouichi Kuroda , Tomio Yamakawa
发明人： Yoshiyuki KUROIWA , Kouichi Kuroda , Tomio Yamakawa
IPC分类号： B21D3/04 , B21D37/00
CPC分类号： B21D3/04
摘要： A method for straightening a tube by using an asymmetric roll, which has different diameters D1 (exit side), D2 (entry side) at relative maximum diameter portions, left and right roll shoulder portions, as a straightening roll of a straightener, wherein the roll shoulder having a smaller diameter is disposed to be located on the tube entry side. The straightening roll used therefor comprises roll shoulders 3a and 3b and a roll barrel portion 4, in which D1>D2 and 0.004≦(D1−D2)/d≦0.2 (d: outer diameter of tube to be straightened) are satisfied. Further, an aspect of the invention may define radii of curvatures of entry-side and exit-side shoulder potions in a section of the roll cut along a plane including the roll central axis, or a curve representing an outer surface of the roll barrel portion.
摘要翻译：通过使用作为矫直机的矫直辊的相对最大直径部分（相对最大直径部分）D2直径（入口侧）不同直径的不对称辊矫直管的方法，其中，具有较小直径的辊肩设置在管入口侧。用于其的矫直辊包括辊肩3a和3b以及辊筒部分4，其中D1> D2和0.004＆amp; N1;（D1-D2）/d≤n1E.0.2（d：要矫直的管的外径）。此外，本发明的一个方面可以限定沿着包括辊中心轴的平面的辊切割部分中的入口侧和出口侧肩部的曲率半径，或表示辊筒部分的外表面的曲线。

4. 发明授权

US08783085B2 Method for straightening tube and straightening roll 有权
标题翻译：矫正矫直辊的方法
公开(公告)号：US08783085B2
公开(公告)日：2014-07-22
申请号：US13589342
申请日：2012-08-20
申请人： Yoshiyuki Kuroiwa , Kouichi Kuroda , Tomio Yamakawa
发明人： Yoshiyuki Kuroiwa , Kouichi Kuroda , Tomio Yamakawa
IPC分类号： B21B23/00 , B21D3/04 , B21D3/05 , B21B19/00
CPC分类号： B21D3/04
摘要： A method for straightening a tube by using an asymmetric roll, which has different diameters D1 (exit side), D2 (entry side) at relative maximum diameter portions, left and right roll shoulder portions, as a straightening roll of a straightener, wherein the roll shoulder having a smaller diameter is disposed to be located on the tube entry side. The straightening roll used therefor comprises roll shoulders 3a and 3b and a roll barrel portion 4, in which D1>D2 and 0.004≦(D1−D2)/d≦0.2 (d: outer diameter of tube to be straightened) are satisfied. Further, an aspect of the invention may define radii of curvatures of entry-side and exit-side shoulder potions in a section of the roll cut along a plane including the roll central axis, or a curve representing an outer surface of the roll barrel portion.
摘要翻译：通过使用作为矫直机的矫直辊的相对最大直径部分（相对最大直径部分）D2直径（入口侧）不同直径的不对称辊矫直管的方法，其中，具有较小直径的辊肩设置在管入口侧。用于其的矫直辊包括辊肩3a和3b以及辊筒部分4，其中D1> D2和0.004＆amp; N1;（D1-D2）/d≤n1E.0.2（d：要矫直的管的外径）。此外，本发明的一个方面可以限定沿着包括辊中心轴的平面的辊切割部分中的入口侧和出口侧肩部的曲率半径，或表示辊筒部分的外表面的曲线。

5. 发明授权

US09254511B2 Method for producing seamless tube/pipe 有权
标题翻译：生产无缝管/管的方法
公开(公告)号：US09254511B2
公开(公告)日：2016-02-09
申请号：US13991635
申请日：2011-12-06
申请人： Kenichi Saitou , Kazuhiro Shimoda , Tomio Yamakawa
发明人： Kenichi Saitou , Kazuhiro Shimoda , Tomio Yamakawa
IPC分类号： B21B21/02 , B21B19/04 , B21B25/00
CPC分类号： B21B21/02 , B21B19/04 , B21B25/00 , B21B2261/08 , B21B2261/10
摘要： By using a piercing mill that includes a pusher on the entrance side, a plug on the exit side along a pass line, and a plurality of angled rolls as being provided around the plug so as face to each other, in the case where the maximum diameter of an unsound region consisting of center segregation and porosity in a cross section of a billet is d [mm], piercing-rolling is performed under the condition that the plug nose rolling reduction ratio (TDF) expressed by Formula (1) satisfies Formula (2). TDF=(Bd−D1)/Bd (1) TDF≦−0.50×(d/Bd)+0.06 (2) In Formulae (1) and (2), Bd is the billet diameter [mm], and D1 is the opening [mm] between the angled rolls at the plug nose position. Thereby, when piercing-rolling is performed, the occurrence of an inner surface flaw attributable to the center segregation and porosity in the billet can be prevented reliably.
摘要翻译：通过使用包括在入口侧的推动器的穿孔机，沿着通行线的出口侧的塞子和在插头周围设置成彼此面对的多个成角度的辊，在最大值在坯料的横截面中由中心偏析和孔隙率组成的不固定区域的直径为d [mm]，在由式（1）表示的塞子前端滚动压下率（TDF）满足公式的条件下进行穿孔轧制（2）。 TDF =（Bd-D1）/ Bd（1）TDF＆nlE; -0.50×（d / Bd）+0.06（2）在式（1）和（2）中，Bd是坯料直径[mm]，D1是在插头前端位置的成角度的卷轴之间打开[mm]。因此，当进行穿孔轧制时，可以可靠地防止由于中心偏析引起的内表面缺陷的发生和坯料中的孔隙率的发生。

6. 发明授权

US08163942B2 Salt of (2S, 3S)-3-[[(1S)-1-isobutoxymethyl-3-methylbutyl]carbamoyl]oxirane-2-carboxylic acid 有权
标题翻译：（2S，3S）-3 - [[（1S）-1-异丁氧基甲基-3-甲基丁基]氨基甲酰基]环氧乙烷-2-羧酸
公开(公告)号：US08163942B2
公开(公告)日：2012-04-24
申请号：US12880655
申请日：2010-09-13
申请人： Atsushi Tendo , Toshihiro Takahashi , Tomio Yamakawa , Kazuki Okai , Susumu Nihashi
发明人： Atsushi Tendo , Toshihiro Takahashi , Tomio Yamakawa , Kazuki Okai , Susumu Nihashi
IPC分类号： C07D303/48
CPC分类号： C07D303/48
摘要： The invention relates to purification of (2S,3S)-3-[[(1S)-1-isobutoxymethyl-3-methylbutyl]carbamoyl]oxirane-2-carboxylic acid [hereinafter, referred to as the carboxylic acid] using the salt of the carboxylic acid with an organic amine selected from the group consisting of piperazine, adamantane amines and others. The invention also relates to providing crystalline sodium salt of the carboxylic acid. The sodium salt is usable as a material for preparing medicaments and improved in storage stability, and has the following characteristics: DSC: exothermic peak observed at a temperature in the range of 170 to 175° C. with weight decrease; and characteristic absorption bands of infrared absorption spectrum (KBr tablet): 3255, 2950, 2860, 1670, 1630, 1550, 1460, 1435, 1395, 1365, 1310, 1260, 1110, 890 cm−1.
摘要翻译：本发明涉及用（2S，3S）-3 - [[（1S）-1-异丁氧基甲基-3-甲基丁基]氨基甲酰基]环氧乙烷-2-羧酸[以下称为羧酸] 所述羧酸与选自哌嗪，金刚烷胺等的有机胺反应。本发明还涉及提供羧酸的结晶钠盐。钠盐可用作制备药物的材料并改善储存稳定性，具有以下特征：DSC：在170至175℃的温度范围内观察到的放热峰，重量减少; 和红外吸收光谱（KBr片剂）的特征吸收带：3255,2950,2860,1670,1630,1550,1460,1435,1395,1365,1310,1260,1110,890cm-1。

7. 发明申请

US20090301155A1 Method of manufacturing seamless pipes 有权
标题翻译：制造无缝管的方法
公开(公告)号：US20090301155A1
公开(公告)日：2009-12-10
申请号：US12453568
申请日：2009-05-15
申请人： Tomio Yamakawa , Kazuhiro Shimoda
发明人： Tomio Yamakawa , Kazuhiro Shimoda
IPC分类号： B21B19/04
CPC分类号： B21B19/04 , B21B25/00
摘要： Seamless pipes excellent in quality features with high productivity is made by a by carrying out piercing-rolling using a piercer provided with a pair of inclined rolls. The piercing-rolling is carried out under conditions such that the plug tip draft (TDFT) or the root of the product of the plug tip draft (TDFT) are controlled along with the number of billet revolutions (N), namely (TDFT×N)0.5. In addition, positions of the inclined rolls are controlled in connection with the gorge draft (GDFT) indicating the ratio of the roll gap (Rg) which is minimal in the gorge section between the inclined rolls to the billet outside diameter (Bd). The piercing-rolling is carried out using a plug having a particular shape.
摘要翻译：通过使用设置有一对倾斜辊的穿孔机进行穿孔轧制，可以实现高生产率的质量特性优良的无缝管。穿孔轧制在条件下进行，使得塞子末梢吃水深度（TDFT）或塞子末梢吃水深度（TDFT）的产物根与坯锭转数（N）一起被控制，即（TDFTxN）0.5 。此外，倾斜辊的位置与峡谷吃水（GDFT）相关联地控制，表示倾斜辊之间的峡谷部分中的辊间隙（Rg）与坯料外径（Bd）之间的最小比例。使用具有特定形状的塞子进行穿孔轧制。

8. 发明申请

US20090203908A1 Activator for Peroxisome Proliferator-Activated Receptor 审中-公开
标题翻译：过氧化物酶体增殖物激活受体活化剂
公开(公告)号：US20090203908A1
公开(公告)日：2009-08-13
申请号：US11920940
申请日：2006-05-24
申请人： Shogo Sakuma , Nobutaka Mochiduki , Rie Takahashi , Toshitake Hirai , Tomio Yamakawa , Seiichiro Masui
发明人： Shogo Sakuma , Nobutaka Mochiduki , Rie Takahashi , Toshitake Hirai , Tomio Yamakawa , Seiichiro Masui
IPC分类号： C07D417/06
CPC分类号： C07D277/28
摘要： A compound having the following formula or its salt is used as an activator for PPAR: in which W2 represents a bond, C(═O) or CH2; Z2 represents an oxygen or sulfur atom; R21, R22 and R23 independently represent a hydrogen atom, an alkyl group having 1 to 8 carbon atoms, an alkoxy group having 1 to 8 carbon atoms, a halogen atom, an alkyl group having 1 to 8 carbon atoms which is substituted with a halogen atom or the like; and R24 and R25 independently represent a hydrogen atom, an alkyl group having 1 to 8 carbon atoms or an alkyl group having 1 to 8 carbon atoms which is substituted with a halogen atom.
摘要翻译：具有下式的化合物或其盐用作PPAR的活化剂：其中W 2表示键，C（-O）或CH 2; Z2表示氧或硫原子; R 21，R 22和R 23独立地表示氢原子，碳原子数1〜8的烷基，碳原子数1〜8的烷氧基，卤原子，碳原子数1〜8的被卤素取代的烷基原子等; R 24和R 25独立地表示氢原子，碳原子数1〜8的烷基或碳原子数1〜8的被卤素原子取代的烷基。

9. 发明授权

US07402597B2 Activator of peroxisome proliferator-activated receptor δ 有权
标题翻译：过氧化物酶体增殖物激活受体δ的活化剂
公开(公告)号：US07402597B2
公开(公告)日：2008-07-22
申请号：US11544505
申请日：2006-10-06
申请人： Shogo Sakuma , Tomio Yamakawa , Takashi Kanda , Seiichiro Masui
发明人： Shogo Sakuma , Tomio Yamakawa , Takashi Kanda , Seiichiro Masui
IPC分类号： A61K31/4178 , A61K31/423 , A61K31/427
CPC分类号： C07D403/06 , A61K31/00 , A61K31/423 , A61K31/427 , A61K31/454 , C07D405/06 , C07D409/06 , C07D413/06 , C07D413/12 , C07D413/14 , C07D417/06 , C07D417/12 , C07D417/14
摘要： A compound represented by the formula (I) or a salt of the compound, and a PPAR-δ activator which contains the compound or salt as the active ingredient: (wherein A represents O or S; B1 represents N, etc.; B2 represents O, etc.; each of X1 and X2 represents O, S, a bond, etc.; Y represents C1-8 alkylene chain; z represents O or S; R1 represents aryl, etc. which can have substituents; R2 represents C1-8 alkyl, etc.; R3 represents C1-8 alkyl, C2-8 alkenyl, etc.; each of R4 and R5 represents hydrogen, C1-8 alkyl, etc.; and R6 represents hydrogen, etc.; provided that each of Z and R3 is attached to the benzene ring, and X2 is not attached to the benzene ring).
摘要翻译：由式（I）表示的化合物或化合物的盐和含有该化合物或盐作为活性成分的PPAR-δ活化剂：（其中A表示O或S; B < 表示N等; B 2表示O等; X 1和X 2各自表示O，S，键， Y表示C 1-8亚烷基链; z表示O或S; R 1表示可具有取代基的芳基等; R 2， / SUP表示C 1-8烷基等; R 3表示C 1-8烷基，C 2-8 链烯基等; R 4和R 5各自代表氢，C 1-8烷基等;和 R 6表示氢等;条件是Z和R 3各自连接到苯环上，并且X 2不连接到苯环）。

10. 发明申请

US20080134742A1 Seamless tube piercing/rolling plug, and seamless tube producing method using same 有权
标题翻译：无缝管穿孔/滚塞，以及使用其的无缝管生产方法
公开(公告)号：US20080134742A1
公开(公告)日：2008-06-12
申请号：US12010303
申请日：2008-01-23
申请人： Tomio Yamakawa , Kazuhiro Shimoda
发明人： Tomio Yamakawa , Kazuhiro Shimoda
IPC分类号： B21B19/04
CPC分类号： B21B25/06 , B21B25/00
摘要： The present invention provides a seamless tube piercing/rolling plug and a seamless tube producing method in which piercing/rolling is performed with an inclined rotary piercing mill while the seamless tube piercing/rolling plug is used as a piercing tool. The seamless tube piercing/rolling plug is used while a front part and a rear part of the split plug are held as an integral plug, at least the front part is made of low alloy steel, and oxide films are formed on surfaces of the front part and rear part. The present invention also provides a seamless tube piercing/rolling apparatus and a seamless tube producing method in which the front part and/or rear part is replaceable in a tube making process line using the seamless tube piercing/rolling apparatus. In the seamless tube piercing/rolling apparatus, the front part and rear part are held as the integral plug, the front part and/or rear part is removably mounted, a mandrel bar holding the plug goes through the rear part, and the mandrel bar is coupled with the front part. It is preferable that a thickness of the oxide film formed in the front part be set to 200 μm or more while the oxide film formed in the front part is thicker than the oxide film formed in the rear part. Even if a hard working material is pierced/rolled, a seam defect and inside surface defects are eliminated, and excellent life-time of plug and excellent plug cost per production quantity can be achieved.
摘要翻译：本发明提供了一种无缝管穿孔/滚压塞和无缝管制造方法，其中在使用无缝管穿孔/滚塞作为穿孔工具的同时，用倾斜的旋转穿孔机进行穿孔/轧制。使用无缝管穿刺/滚压塞，而分离塞的前部和后部被保持为整体塞，至少前部由低合金钢制成，并且氧化膜形成在前表面部分和后部。本发明还提供了一种无缝管穿孔/轧制装置和无缝管制造方法，其中使用无缝管穿孔机可以在管制造线中替换前部和/或后部。在无缝管穿刺/轧制装置中，前部和后部被保持为一体式塞子，前部和/或后部可拆卸地安装，保持插头的芯棒穿过后部，并且芯棒与前部相结合。优选的是，形成在前部的氧化膜的厚度设定为200μm以上，而在前部形成的氧化膜比形成在后部的氧化膜厚。即使硬质材料被刺穿/轧制，也可以消除接缝缺陷和内表面缺陷，并且可以实现优异的插头寿命和优异的插头成本。

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