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1. 发明授权

US5510422A Synthesis of latex capsules 失效
公开(公告)号：US5510422A
公开(公告)日：1996-04-23
申请号：US467642
申请日：1995-06-06
申请人： Robert M. Blankenship , Ronald W. Novak , Clarence J. Neyhart , Martin Vogel , Alexander Kowalski
发明人： Robert M. Blankenship , Ronald W. Novak , Clarence J. Neyhart , Martin Vogel , Alexander Kowalski
IPC分类号： C08F2/22 , C08F2/44 , C08F265/02 , C08F267/06 , C08J3/12 , B32B27/30
CPC分类号： C08J3/12 , C08F265/02 , C08J3/126 , C09D7/125 , C09D7/1291 , C08J2333/12 , C08J2433/12 , Y10T428/2989
摘要： The present invention is concerned with core and shell polymeric particles having microvoids in the core and one or more channels connecting the microvoids to the exterior of the particle. These particles, or LCAPs are produced by forming a core of polymeric acid, encasing the core in a shell polymer permeable to base, and then neutralizing the core such that the core swells, causing the shell to "explode" in a controlled fashion. This controlled explosion causes channels to form in the shell.These particles can be used as control release devices for target compounds, to impart reinforcing properties to acrylic films, as an opacifying agent in coating compositions, and as a supplement or replacement of part or all of the pigmentary material or extenders that would otherwise be used in such coating compositions.

2. 发明授权

US5527613A Synthesis of latex capsules 失效
标题翻译：乳胶胶囊的合成
公开(公告)号：US5527613A
公开(公告)日：1996-06-18
申请号：US233089
申请日：1994-04-25
申请人： Robert M. Blankenship , Ronald W. Novak , Clarence J. Neyhart , Martin Vogel
发明人： Robert M. Blankenship , Ronald W. Novak , Clarence J. Neyhart , Martin Vogel
IPC分类号： C08F2/22 , C08F2/44 , C08F265/02 , C08F267/06 , C08J3/12 , B32B27/30
CPC分类号： C08J3/12 , C08F265/02 , C08J3/126 , C09D7/125 , C09D7/1291 , C08J2333/12 , C08J2433/12 , Y10T428/2989
摘要： The present invention is concerned with core and shell polymeric particles having microvoids in the core and one or more channels connecting the microvoids to the exterior of the particle. These particles, or LCAPs are produced by forming a core of polymeric acid, encasing the core in a shell polymer permeable to base, and then neutralizing the core such that the core swells, causing the shell to "explode" in a controlled fashion. This controlled explosion causes channels to form in the shell.These particles can be used as control release devices for target compounds, to impart reinforcing properties to acrylic films, as an opacifying agent in coating compositions, and as a supplement or replacement of part or all of the pigmentary material or extenders that would otherwise be used in such coating compositions.
摘要翻译：本发明涉及在芯中具有微孔的核和壳聚合物颗粒和将微孔连接到颗粒外部的一个或多个通道。这些颗粒或LCAP通过形成聚合酸的核心，将核心包裹在可渗透碱的壳聚合物中，然后中和核心，从而使核心膨胀，导致壳体以受控的方式“爆炸”来生产。这种受控的爆炸导致通道在外壳中形成。这些颗粒可以用作目标化合物的控制释放装置，以赋予丙烯酸膜作为增强性能，作为涂料组合物中的遮光剂，以及补充或替代部分或全部的颜料或增量剂，否则将被使用在这样的涂料组合物中。

3. 发明授权

US4427836A Sequential heteropolymer dispersion and a particulate material obtainable therefrom, useful in coating compositions as a thickening and/or opacifying agent 失效
标题翻译：顺序杂聚物分散体和可由其获得的颗粒材料，可用作涂料组合物作为增稠剂和/或遮光剂
公开(公告)号：US4427836A
公开(公告)日：1984-01-24
申请号：US352396
申请日：1982-02-25
申请人： Alexander Kowalski , Martin Vogel , Robert M. Blankenship
发明人： Alexander Kowalski , Martin Vogel , Robert M. Blankenship
IPC分类号： C08F2/22 , C08F265/02 , C09D151/00
CPC分类号： C08F2/22 , C08F265/02 , C09D151/003 , C09D5/028 , C09D7/002 , C09D7/125 , C09D7/1291 , Y10S525/902
摘要： The present invention is concerned with the production and use of water-insoluble particulate heteropolymers made by sequential emulsion polymerization in dispersed particles of which a "core" of a polymeric acid is at least partially encased in a "sheath" polymer that is permeable to a volatile base, such as ammonia or an organic amine, adapted to cause swelling of the core by neutralization. The aqueous dispersion of the acid-containing core/sheath particles is useful in making water-base coating compositions wherein it may serve as an opacifying agent when a volatile base is used to at least partially (to a pH of at least 6) neutralize the heteropolymer, microvoids being formed in cores of the swollen particles in the film during the drying thereof. Thus, the heteropolymer dispersion can serve as an opacifying agent in coating compositions, such as water-base paints, as a supplement or replacement of part or all of the pigmentary material or extenders that would otherwise be used in such coating compositions.For convenience of description herein, the terms "core", "sheath", and "core/sheath polymr" are frequently used to refer to the distinct functional components of the individual polymer particles of the essential "mode" of the heteropolymers of the present invention even though in actuality, the components of the polymer particles thereof may not have the precise arrangement implied by this terminology.
摘要翻译：本发明涉及通过在其分散颗粒中顺序乳液聚合制备的水不溶性颗粒状杂聚物的制备和使用，其中聚合酸的“芯”至少部分地包封在可渗透的“护套”聚合物中挥发性碱，例如氨或有机胺，适于通过中和引起芯的溶胀。含酸芯/皮颗粒的含水分散体可用于制备水性涂料组合物，其中当使用挥发性碱至少部分（至少6的pH）时，其可以用作不透明剂，中和杂聚物，在其干燥期间在膜中的溶胀颗粒的芯中形成微孔。因此，杂聚聚物分散体可以用作涂料组合物中的遮光剂，例如水基涂料，作为另外将用于这种涂料组合物的部分或全部颜料材料或增量剂的补充或替代物。为了方便本文的描述，术语“芯”，“护套”和“芯/鞘多聚体”经常用于指本发明的杂聚物的基本“模式”的各个聚合物颗粒的不同功能组分即使实际上，其聚合物颗粒的组分可能不具有由该术语所暗示的精确布置。

4. 发明授权

US4468498A Sequential heteropolymer dispersion and a particulate materal obtainable therefrom, useful in coating compositions as a thickening and/or opacifying agent 失效
标题翻译：顺序杂聚物分散体和可由其获得的颗粒物，可用于涂料组合物中作为增稠剂和/或不透明剂
公开(公告)号：US4468498A
公开(公告)日：1984-08-28
申请号：US352397
申请日：1982-02-25
申请人： Alexander Kowalski , Martin Vogel , Robert M. Blankenship
发明人： Alexander Kowalski , Martin Vogel , Robert M. Blankenship
IPC分类号： C08F2/22 , C08F265/02 , C09D151/00
CPC分类号： C08F265/02 , C08F2/22 , C09D151/003 , C09D5/028 , C09D7/002 , C09D7/125 , C09D7/1291 , Y10S525/901
摘要： The present invention is concerned with the production and use of water-insoluble particulate heteropolymers made by sequential emulsion polymerization in dispersed particles of which a "core" of a polymeric acid is at least partially encased in a "sheath" polymer that is permeable to a volatile base, such as ammonia or an organic amine, adapted to cause swelling of the core by neutralization. The aqueous dispersion of the acid-containing core/sheath particles is useful in making water-base coating compositions wherein it may serve as the binder or as a part thereof. In that use, the heteropolymer dispersion serves to provide desirable rheological control of the coating compositions when a volatile base is used to at least partially (to a pH of at least 6) neutralize the heteropolymer. Thus, the heteropolymer dispersion can serve as a thickener, or part thereof in coating compositions, such as water-base paints.For convenience of description herein, the terms "core", "sheath", and "core/sheath polymer" are frequently used to refer to the distinct functional components of the individual polymer particles of the essential "mode" of the heteropolymers of the present invention even though in actuality, the components of the polymer particles thereof may not have the precise arrangement implied by this terminology.
摘要翻译：本发明涉及通过在其分散颗粒中顺序乳液聚合制备的水不溶性颗粒状杂聚物的制备和使用，其中聚合酸的“芯”至少部分地包封在可渗透的“护套”聚合物中挥发性碱，例如氨或有机胺，适于通过中和引起芯的溶胀。含酸芯/皮颗粒的水分散体可用于制备其中可用作粘合剂或作为其一部分的水性涂料组合物。在该用途中，当使用挥发性碱至少部分（至少6的pH）中和杂聚物时，杂聚聚物分散体用于提供涂料组合物的期望的流变学控制。因此，杂聚聚合物分散体可以用作涂料组合物中的增稠剂或其一部分，例如水基涂料。为了便于说明，术语“核心”，“护套”和“芯/鞘聚合物”通常用于指本发明的杂聚物的基本“模式”的各个聚合物颗粒的不同功能组分即使实际上，其聚合物颗粒的组分可能不具有由该术语所暗示的精确布置。

5. 发明授权

US08828289B2 Free-radical-polymerisable fixing mortar having silane additives 有权
标题翻译：具有硅烷添加剂的自由基聚合固定砂浆
公开(公告)号：US08828289B2
公开(公告)日：2014-09-09
申请号：US13515636
申请日：2010-11-16
申请人： Jurgen Grun , Martin Vogel , Clemens Schmidt , Christian Schlenk , Christian Weinelt
发明人： Jurgen Grun , Martin Vogel , Clemens Schmidt , Christian Schlenk , Christian Weinelt
IPC分类号： E04B1/35 , C04B26/16 , C04B28/06 , C04B28/04 , C04B26/06 , C04B26/32 , C04B26/18 , C04B26/14 , C04B111/00 , C04B103/00
CPC分类号： C04B26/32 , C04B16/065 , C04B24/42 , C04B26/06 , C04B26/14 , C04B26/16 , C04B26/18 , C04B28/04 , C04B28/06 , C04B2103/0047 , C04B2111/00715 , C04B24/2641 , C04B40/065 , C04B24/281 , C04B24/282 , C04B24/283
摘要： Two-component or multi-component fixing mortar, based on a free-radical-hardening unsaturated reactive resin, for embedding anchoring means in mortar in holes or crevices, which fixing mortar includes silanes which may or may not have reactive groups capable of participating in the polymerization with a synthetic resin based on free-radical-hardening unsaturated reactive resins but do in any case have Si-bonded hydrolysable groups, and, physically separate therefrom, a hardener.
摘要翻译：基于自由基硬化的不饱和反应性树脂的双组分或多组分固定砂浆用于将锚固装置嵌入孔或缝隙中的砂浆中，固定砂浆包括可能具有或不具有能够参与的反应性基团的硅烷使用基于自由基硬化不饱和反应性树脂的合成树脂的聚合，但是在任何情况下都具有Si键合的可水解基团，并且与其物理上分离出固化剂。

6. 发明申请

US20120247985A1 FREE-RADICAL-POLYMERISABLE FIXING MORTAR HAVING SILANE ADDITIVES 有权
标题翻译：具有硅烷添加剂的自由可聚合固定木糖
公开(公告)号：US20120247985A1
公开(公告)日：2012-10-04
申请号：US13515636
申请日：2010-11-16
申请人： Jurgen Grun , Martin Vogel , Clemens Schmidt , Christian Schlenk , Christian Weinelt
发明人： Jurgen Grun , Martin Vogel , Clemens Schmidt , Christian Schlenk , Christian Weinelt
IPC分类号： B65D25/08 , C08K5/5415 , C08K5/5435 , E04B1/35 , C08K5/548 , C08G77/00 , C08K5/5425 , B65D85/84 , C08L33/06 , C08K5/544
CPC分类号： C04B26/32 , C04B16/065 , C04B24/42 , C04B26/06 , C04B26/14 , C04B26/16 , C04B26/18 , C04B28/04 , C04B28/06 , C04B2103/0047 , C04B2111/00715 , C04B24/2641 , C04B40/065 , C04B24/281 , C04B24/282 , C04B24/283
摘要： Two-component or multi-component fixing mortar, based on a free-radical-hardening unsaturated reactive resin, for embedding anchoring means in mortar in holes or crevices, which fixing mortar includes silanes which may or may not have reactive groups capable of participating in the polymerisation with a synthetic resin based on free-radical-hardening unsaturated reactive resins but do in any case have Si-bonded hydrolysable groups, and, physically separate therefrom, a hardener.
摘要翻译：基于自由基硬化的不饱和反应性树脂的双组分或多组分固定砂浆用于将锚固装置嵌入孔或缝隙中的砂浆中，固定砂浆包括可能具有或不具有能够参与的反应性基团的硅烷使用基于自由基硬化的不饱和反应性树脂的合成树脂进行聚合，但是在任何情况下都具有硅键合的可水解基团，并与其物理分离，由硬化剂构成。

7. 发明申请

US20100294676A1 SYNTHETIC MORTAR COMPOSITION 审中-公开
标题翻译：合成麦芽糖组合物
公开(公告)号：US20100294676A1
公开(公告)日：2010-11-25
申请号：US12445621
申请日：2007-09-20
申请人： Jürgen Grün , Markus Semmler , Christian Schlenk , Martin Vogel
发明人： Jürgen Grün , Markus Semmler , Christian Schlenk , Martin Vogel
IPC分类号： B65D71/00 , C08K3/00
CPC分类号： C09D5/34 , C04B26/06 , C04B26/10 , C04B40/065 , C04B40/0666 , C04B2111/00715 , C09J11/04 , C04B7/00 , C04B14/06 , C04B14/28 , C04B38/10
摘要： A multi-component synthetic resin system, its use for securing fixing elements and a method for its preparation, and further embodiments mentioned in the description based on this invention, the multi-component synthetic resin system including one or more finely distributed gases in at least one of its components. Application is primarily in the construction industry.
摘要翻译：多组分合成树脂体系，其固定元件的固定用途及其制备方法以及基于本发明的说明书中提到的其它实施方案，所述多组分合成树脂体系至少包含一种或多种精细分布的气体其中一个组件。申请主要在建筑行业。

8. 发明申请

US20070042356A1 Variants of hepatitis B virus resistant against some nucleoside analogues, but sensitive to others, and uses thereof 有权
标题翻译：乙型肝炎病毒对某些核苷类似物具有抗性但对其他人敏感的变体及其用途
公开(公告)号：US20070042356A1
公开(公告)日：2007-02-22
申请号：US11375580
申请日：2006-03-15
申请人： Oliver Schildgen , Martin Vogel , Bertfried Matz , Juergen Rockstroh , Rolf Kaiser , Martin Daeumer , Martin Helm , Lutwin Weitner , Carl Schewe , Wolfram Gerlich
发明人： Oliver Schildgen , Martin Vogel , Bertfried Matz , Juergen Rockstroh , Rolf Kaiser , Martin Daeumer , Martin Helm , Lutwin Weitner , Carl Schewe , Wolfram Gerlich
IPC分类号： C12Q1/70 , C07H21/04 , A61K31/7072 , C07K14/02 , C12N15/86 , C12N7/01
CPC分类号： C12N7/00 , C07K14/005 , C12N9/1276 , C12N2730/10121 , C12N2730/10122 , C12Q1/706 , C12Q2600/156 , G01N33/5761 , G01N2333/02
摘要： The present invention relates generally to the field of Hepatitis B variants exhibiting a reduced sensitivity to nucleoside analogues both in vivo and in vitro. More in particular, reverse transcriptase mutant rt I233V is provided. Present invention provides assays and methods for detecting such variant, which assays are useful in monitoring anti-viral therapeutic regimes and adjusting patient therapy. A diagnostic kit for detecting the presence of an HBV variant in a biological sample has also been described. Finally, the use of a farmaceutical composition to cure a subject suffering from a HBV infection, which HBV is resistant to lamuvidine and/or adefovir has been provided, which farmaceutical composition comprises the nucleoside analogue tenofovir.
摘要翻译：本发明一般涉及在体内和体外对核苷类似物的敏感性降低的乙型肝炎变体领域。更具体地，提供逆转录酶突变体rt I233V。本发明提供了用于检测这种变体的测定和方法，该测定法可用于监测抗病毒治疗方案并调整患者治疗。还描述了用于检测生物样品中HBV变异体的存在的诊断试剂盒。最后，提供了一种药物组合物治疗患有HBV感染的受试者，其HBV对lamvvidine和/或阿德福韦具有抗性，该药物组合物包含核苷类似物替诺福韦。

9. 发明授权

US5663224A Process for preparing an aqueous dispersion 失效
标题翻译：制备水性分散体的方法
公开(公告)号：US5663224A
公开(公告)日：1997-09-02
申请号：US801989
申请日：1991-12-03
申请人： William David Emmons , Martin Vogel , Edward C. Kostansek , Jack C. Thibeault , Peter R. Sperry , Chao-Jen Chung
发明人： William David Emmons , Martin Vogel , Edward C. Kostansek , Jack C. Thibeault , Peter R. Sperry , Chao-Jen Chung
IPC分类号： C08J3/03 , C08J3/205 , C08J3/215 , C08K3/00 , C08L101/00 , C09D5/02 , C09J11/04 , C09J201/00 , D21H19/40 , C08K5/54
CPC分类号： D21H19/40 , C08J3/215 , C09D5/024
摘要： Inorganic material particles are dispersed in an aqueous medium with surface charge adjusting additives to give a moderately stable slurry or pigment grind. The dispersion can be used to prepare fully formulated compositions. Products formulated using the aqueous dispersion can be prepared to give the same performance as products including inorganic material dispersed with conventional polyelectrolyte pigment dispersants, but with higher levels of inorganic material, or superior performance properties with like levels of inorganic material.
摘要翻译：将无机材料颗粒分散在具有表面电荷调节添加剂的水性介质中，得到适度稳定的浆料或颜料研磨。分散体可用于制备完全配制的组合物。使用水分散体配制的产品可以制备成与包括用常规聚电解质颜料分散剂分散的无机材料的产品相同的性能，但是具有较高水平的无机材料或具有相似水平的无机材料的优异性能。

10. 发明授权

US4970241A Multi-stage opacifying polymer particles containing non-polymeric acid absorbed therein 失效
标题翻译：含有非聚合酸的多级不透明聚合物颗粒被吸收
公开(公告)号：US4970241A
公开(公告)日：1990-11-13
申请号：US382612
申请日：1989-07-19
申请人： Alexander Kowalski , Martin Vogel
发明人： Alexander Kowalski , Martin Vogel
IPC分类号： C08F285/00 , C08J9/28 , C09D7/12
CPC分类号： C08J9/28 , C08F285/00 , C09D7/1291 , Y10S525/902
摘要： Multi-stage polymer particles containing one or more void space(s) therein are produced by sequential emulsion polymerization of an essentially low-acid earlier polymer stage, encapsulation of said low-acid polymer stage with at least a final polymer stage, contacting said polymer particles with a non-polymeric carboxylic acid or anhydride to permit the acid or anhydride to be absorbed into said low-acid polymer stage and swelling the polymer particles by contacting the particles with an aqueous base. The low-acid polymer stage is formed by emulsion polymerizing a monomer system comprising ethylenically unsaturated monomer(s) and containing less than 5% by weight of monomer(s) containing acid functionality. The low-acid polymer stage is swubsequently encapsulated by one or more polymer stages by emulsion polymerizing ethylenically unsaturated monomer(s) in the presence of the low-acid polymer stage. The final stage has a glass transition temperature (Tg) of about 50.degree. C. or greater, and the total polymer stages having a Tg of about 50.degree. C. or greater comprise about 60% or more by weight of the polymer particles. A non-polymeric carboxylic acid or anhydride is absorbed into the polymer particles and the resultant particles are contacted with base at a pH sufficient to swell the particles with water at a temperature near or above the Tg of the neat polymer or plasticized polymer of the final polymer stage. When dried the particles contain void space(s) therein which produce(s) opacity in compositions in which the particles are contained.
摘要翻译：在其中含有一个或多个空隙空间的多级聚合物颗粒通过基本上低酸的较早聚合物阶段的顺序乳液聚合制备，所述低酸聚合物阶段至少包含最终聚合物阶段，使所述聚合物接触具有非聚合羧酸或酸酐的颗粒，以允许酸或酸酐被吸收到所述低酸聚合物阶段中，并通过使颗粒与碱水溶液接触来使聚合物颗粒膨胀。通过乳液聚合包含烯属不饱和单体并且含有少于5重量％的含有酸官能团的单体的单体体系形成低酸聚合物阶段。低酸聚合物阶段通过在低酸聚合物阶段的存在下通过乳液聚合烯键式不饱和单体而被一个或多个聚合物阶段封装。最终阶段具有约50℃或更高的玻璃化转变温度（Tg），并且具有约50℃或更高Tg的总聚合物阶段包含约60重量％或更多的聚合物颗粒。非聚合的羧酸或酸酐被吸收到聚合物颗粒中，并且所得颗粒在足以在最终纯净聚合物或增塑聚合物的Tg附近或更高的温度下用水溶胀颗粒的pH与碱接触聚合物阶段。当干燥时，颗粒中含有空隙空间，其中含有颗粒的组合物中产生不透明度。

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