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1. 发明申请

US20150165652A1 ELECTROLYTIC CELL COVERS COMPRISING A RESIN COMPOSITION POLYMERIZED WITH A GROUP 8 OLEFIN METATHESIS CATALYST 审中-公开
标题翻译：含有8个烯烃METATHESIS催化剂聚合的树脂组合物的电解槽
公开(公告)号：US20150165652A1
公开(公告)日：2015-06-18
申请号：US14343513
申请日：2012-09-14
申请人： Michael A. Giardello , Mark S. Trimmer , Christopher J. Cruce , Anthony R. Stephen , Stuart A. M. Toner , Albert E. Pappano
发明人： Michael A. Giardello , Mark S. Trimmer , Christopher J. Cruce , Anthony R. Stephen , Stuart A. M. Toner , Albert E. Pappano
IPC分类号： B29C39/00 , C25B9/00
CPC分类号： C25B9/00 , B29C39/003 , B29C67/246 , B29K2023/00 , B29K2023/38 , B29K2105/0014 , B29K2995/0029 , B29L2031/7146 , C08G61/02 , C08G2120/00 , C08G2261/3325 , C08G2261/418 , C08G2261/58 , C25B1/34
摘要： Articles of manufacture possessing corrosion resistance characteristics are described, in particular for use in the chlor-alkali and other industries. The articles are formed from a resin composition, e.g., a cyclic olefin composition, polymerized with a Group 8 olefin metathesis catalyst. In particular aspects, an electrolytic cell component, such as a cell cover for use in the electrolysis of brine, may be formed from the resin composition. Among other benefits, such articles provide improved corrosion resistance compared to articles molded from other resin compositions, such as Fiberglass reinforced polyesters and vinyl esters, and two-component dicyclopentadiene (DCPD) resins comprising molybdenum or tungsten pre-catalysts.
摘要翻译：描述了具有耐腐蚀特性的制品，特别是用于氯碱等行业。制品由用8族烯烃复分解催化剂聚合的树脂组合物形成，例如环烯烃组合物。在特定方面，可以由树脂组合物形成用于电解盐水的电解池组件，例如电池盖。除了其它益处之外，与由其它树脂组合物（例如玻璃纤维增强聚酯和乙烯基酯）和包含钼或钨预催化剂的双组分二环戊二烯（DCPD）树脂模制的制品相比，这些制品提供了改进的耐腐蚀性。

2. 发明申请

US20140329017A1 ADHESION PROMOTERS AND GEL-MODIFIERS FOR OLEFIN METATHESIS COMPOSITIONS 审中-公开
标题翻译：粘合剂组合物的粘合促进剂和凝胶改性剂
公开(公告)号：US20140329017A1
公开(公告)日：2014-11-06
申请号：US14125837
申请日：2012-06-17
申请人： Li-Sheng Wang , Anthony R. Stephen , Paul W. Booth , Tessa Schulze , Michael A. Giardello , Mark S. Trimmer , Christopher J. Cruce , Farshad J. Motamedi , Brian Edgecombe
发明人： Li-Sheng Wang , Anthony R. Stephen , Paul W. Booth , Tessa Schulze , Michael A. Giardello , Mark S. Trimmer , Christopher J. Cruce , Farshad J. Motamedi , Brian Edgecombe
IPC分类号： C03C25/30
CPC分类号： C03C25/30 , C08F32/02 , C08G61/08 , C08G2261/3325 , C08G2261/418 , C08K5/0025 , C08K5/14 , C08K5/29 , C08K2201/014 , C08L65/00
摘要： This invention relates to compositions and methods for improving the adhesion of resin compositions to substrate materials, pre-treating substrate materials to improve the adhesion of resin compositions to the substrate materials, and/or controlling gel formation of resin compositions. More particularly, the invention relates to compositions and methods for improving the adhesion of ring opening metathesis polymerization (ROMP) compositions to substrate materials using adhesion promoters containing isocyariate groups in a resin composition. The invention also relates to methods for improving the adhesion of resin compositions to substrate materials by pre-treating substrate materials with adhesion promoters containing isocyanate groups. The invention further relates to a method of providing a gel-modified ROMP composition, in which a hydroperoxide is added to a ROMP polymerizable resin composition in order to control gel formation of the polymerizing resin. An improved ROMP composition is further disclosed, comprising a cyclic olefin, a ROMP metathesis catalyst, an adhesion promoter, and an added hydroperoxide gel modifier. The polymer products produced via ROMP reactions of the invention may be utilized for a wide range of materials and composite applications. The invention has utility in the fields of catalysis, organic synthesis, and polymer and materials chemistry and manufacture.
摘要翻译：本发明涉及用于改善树脂组合物与基材的粘合性，预处理基材以改善树脂组合物与基材的粘合性和/或控制树脂组合物凝胶形成的组合物和方法。更具体地，本发明涉及使用在树脂组合物中含有异质基团的粘合促进剂来改善开环易位聚合（ROMP）组合物与基材的粘合性的组合物和方法。本发明还涉及通过用含有异氰酸酯基团的粘合促进剂预处理底物材料来改善树脂组合物对基材的粘附性的方法。本发明还涉及一种提供凝胶改性的ROMP组合物的方法，其中将氢过氧化物加入到ROMP可聚合树脂组合物中以控制聚合树脂的凝胶形成。进一步公开了改进的ROMP组合物，其包含环烯烃，ROMP复分解催化剂，粘合促进剂和加入的氢过氧化物凝胶改性剂。通过本发明的ROMP反应生产的聚合物产品可用于广泛的材料和复合材料应用。本发明可用于催化，有机合成，聚合物和材料的化学和制造领域。

3. 发明授权

US10457597B2 Adhesion promoters and gel-modifiers for olefin metathesis compositions 有权
公开(公告)号：US10457597B2
公开(公告)日：2019-10-29
申请号：US14125837
申请日：2012-06-17
申请人： Li-Sheng Wang , Anthony R. Stephen , Paul W. Boothe , Tessa Schulze , Michael A. Giardello , Mark S. Trimmer , Christopher J. Cruce , Farshad J. Motamedi , Brian Edgecombe
发明人： Li-Sheng Wang , Anthony R. Stephen , Paul W. Boothe , Tessa Schulze , Michael A. Giardello , Mark S. Trimmer , Christopher J. Cruce , Farshad J. Motamedi , Brian Edgecombe
IPC分类号： C03C25/30 , C08K5/00 , C08K5/14 , C08K5/29 , C08F32/02 , C08G61/08
摘要： This invention relates to compositions and methods for improving the adhesion of resin compositions to substrate materials, pre-treating substrate materials to improve the adhesion of resin compositions to the substrate materials, and/or controlling gel formation of resin compositions. More particularly, the invention relates to compositions and methods for improving the adhesion of ring opening metathesis polymerization (ROMP) compositions to substrate materials using adhesion promoters containing isocyariate groups in a resin composition. The invention also relates to methods for improving the adhesion of resin compositions to substrate materials by pre-treating substrate materials with adhesion promoters containing isocyanate groups. The invention further relates to a method of providing a gel-modified ROMP composition, in which a hydroperoxide is added to a ROMP polymerizable resin composition in order to control gel formation of the polymerizing resin. An improved ROMP composition is further disclosed, comprising a cyclic olefin, a ROMP metathesis catalyst, an adhesion promoter, and an added hydroperoxide gel modifier. The polymer products produced via ROMP reactions of the invention may be utilized for a wide range of materials and composite applications. The invention has utility in the fields of catalysis, organic synthesis, and polymer and materials chemistry and manufacture.

4. 发明授权

US07285593B1 Polyolefin compositions optionally having variable toughness and/or hardness 有权
标题翻译：任选具有可变韧性和/或硬度的聚烯烃组合物
公开(公告)号：US07285593B1
公开(公告)日：2007-10-23
申请号：US09312811
申请日：1999-05-17
申请人： Michael A. Giardello , Jonathan G. Lasch , Christopher J. Cruce , Jessie G. Macleod
发明人： Michael A. Giardello , Jonathan G. Lasch , Christopher J. Cruce , Jessie G. Macleod
IPC分类号： C08G61/04 , A63B53/10
CPC分类号： A63B60/00 , A63B53/04 , A63B53/10 , A63B60/06 , A63B60/08 , A63B60/10 , A63B2053/002 , A63B2209/00 , A63B2209/02 , C08F32/00 , C08L65/00 , C08L83/00
摘要： The present invention provides novel polyolefin compositions having variable hardness and/or toughness properties. The polyolefin compositions include: a polyolefin prepared by the metathesis of an olefin monomer using a ruthenium or osmium carbene catalyst; and one or more hardness and/or toughness modulators. The polyolefin is preferably poly(dicyclopentadiene), or poly-DCPD. Also provided are articles of manufacture, such as molded parts, produced from the polyolefin compositions. The disclosed compositions are useful in marine, recreational and sports products.
摘要翻译：本发明提供具有可变硬度和/或韧性的新型聚烯烃组合物。聚烯烃组合物包括：通过使用钌或锇卡因催化剂复分解烯烃单体制备的聚烯烃; 和一种或多种硬度和/或韧性调节剂。聚烯烃优选为聚（二环戊二烯）或聚-DCPD。还提供了由聚烯烃组合物制备的制品，例如模制件。所公开的组合物可用于海洋，娱乐和运动产品。

5. 发明授权

US06525125B1 Polyolefin compositions having variable density and methods for their production and use 有权
标题翻译：具有可变密度的聚烯烃组合物及其生产和使用方法
公开(公告)号：US06525125B1
公开(公告)日：2003-02-25
申请号：US09497950
申请日：2000-02-04
申请人： Michael A. Giardello , Jonathon G. Lasch , Christopher J. Cruce , Jessie G. Macleod , Christopher M. Haar
发明人： Michael A. Giardello , Jonathon G. Lasch , Christopher J. Cruce , Jessie G. Macleod , Christopher M. Haar
IPC分类号： C08K308
CPC分类号： A63B53/04 , A63B53/0487 , A63B53/12 , A63B2053/0408 , A63B2209/00 , C08G61/08 , C08K5/13
摘要： The invention discloses a composition comprising one or more density modulators dispersed in a polymer matrix wherein the matrix is prepared by the metathesis of an olefin monomer using a ruthenium or osmium metal carbene catalyst. The composition may use a catalyst of the formula wherein: M is ruthenium or osmium; X and X1 are either the same or different and are any anionic ligand; L and L1 are either the same or different and are any neutral electron donor; R and R1 are either the same or different and are each independently hydrogen or a substitutent selected from the group consisting of C1-C20 alkyl, C2-C20 alkenyl, C2-C20 alkynyl, aryl, C1-C20 carboxylate, C1-C20 alkoxy, C2-C20 alkenyloxy, C2-C20 alkynyloxy, aryloxy, C2-C20 alkoxycarbonyl, C1-C20 alkylthio, C1-C20 alkylsulfonyl and C1-C20 alkylsulfinyl, wherein each of the substituents is substituted or unsubstituted. The density modulators are selected from the group consisting of metallic density modulators, microparticulate density modulators and macroparticulate density modulators.
摘要翻译：本发明公开了一种组合物，其包含分散在聚合物基质中的一种或多种密度调节剂，其中基质通过使用钌或锇金属卡宾催化剂的烯烃单体的复分解来制备。组合物可以使用糠醛的催化剂：M是钌或锇; X和X 1相同或不同，为任何阴离子配体; L和L1可以相同或不同，并且是任何中性电子给体; R和R 1相同或不同，各自独立地为氢或选自C 1 -C 20烷基，C 2 -C 20烯基，C 2 -C 20炔基，芳基，C 1 -C 20羧酸酯，C 1 -C 20烷氧基， C 2 -C 20链烯氧基，C 2 -C 20炔氧基，芳氧基，C 2 -C 20烷氧基羰基，C 1 -C 20烷硫基，C 1 -C 20烷基磺酰基和C 1 -C 20烷基亚磺酰基，其中每个取代基是取代或未取代的。密度调节剂选自金属浓度调节剂，微粒密度调节剂和大粒子密度调节剂。

6. 发明申请

US20090048405A1 METATHESIS-ACTIVE ADHESION AGENTS AND METHODS FOR ENHANCING POLYMER ADHESION TO SURFACES 有权
标题翻译： METATHESIS-ACTIVE粘合剂和增强聚合物粘附于表面的方法
公开(公告)号：US20090048405A1
公开(公告)日：2009-02-19
申请号：US12042236
申请日：2008-03-04
申请人： Michael A. Giardello , Christopher M. Haar
发明人： Michael A. Giardello , Christopher M. Haar
IPC分类号： C08F255/00
CPC分类号： C09J4/00 , C08F263/04 , C08G61/08 , C08L2666/02 , C09J151/003 , C09J151/06 , C09J151/10 , Y10T428/31536 , Y10T428/31855
摘要： The invention discloses an adhesion agent composition comprising at least one C3-C200 olefin compound having at least one metathesis active double bond, wherein the olefin is substituted or unsubstituted; and at least one compatibilizing functionality for interacting with a substrate surface. The substrate surface can be any surface, for example, silicate glasses, silicate minerals, metals, metal alloys, ceramics, natural stones, plastics, carbon, silicon, and semiconductors. The invention also discloses articles of manufacture utilizing these adhesion agents as well as methods for adhering a polyolefin to a substrate surface.
摘要翻译：本发明公开了一种粘合剂组合物，其包含至少一种具有至少一个复分解活性双键的C 3 -C 20烯烃化合物，其中所述烯烃是取代或未取代的; 以及用于与衬底表面相互作用的至少一种相容性功能。衬底表面可以是任何表面，例如硅酸盐玻璃，硅酸盐矿物，金属，金属合金，陶瓷，天然石，塑料，碳，硅和半导体。本发明还公开了利用这些粘合剂的制品以及将聚烯烃粘附到基材表面的方法。

7. 发明授权

US08597794B2 Metathesis-active adhesion agents and methods for enhancing polymer adhesion to surfaces 有权
公开(公告)号：US08597794B2
公开(公告)日：2013-12-03
申请号：US13165515
申请日：2011-06-21
申请人： Michael A. Giardello , Christopher M. Haar
发明人： Michael A. Giardello , Christopher M. Haar
IPC分类号： B32B27/00
CPC分类号： C09J4/00 , C08F263/04 , C08G61/08 , C08L2666/02 , C09J151/003 , C09J151/06 , C09J151/10 , Y10T428/31536 , Y10T428/31855
摘要： The invention discloses an adhesion agent composition comprising at least one C3-C200 olefin compound having at least one metathesis active double bond, wherein the olefin is substituted or unsubstituted; and at least one compatibilizing functionality for interacting with a substrate surface. The substrate surface can be any surface, for example, silicate glasses, silicate minerals, metals, metal alloys, ceramics, natural stones, plastics, carbon, silicon, and semiconductors. The invention also discloses articles of manufacture utilizing these adhesion agents as well as methods for adhering a polyolefin to a substrate surface.

8. 发明授权

US07964320B2 Metathesis-active adhesion agents and methods for enhancing polymer adhesion to surfaces 有权
标题翻译：复分解活性粘合剂和增强聚合物与表面粘附的方法
公开(公告)号：US07964320B2
公开(公告)日：2011-06-21
申请号：US12042236
申请日：2008-03-04
申请人： Michael A. Giardello , Christopher M. Haar
发明人： Michael A. Giardello , Christopher M. Haar
IPC分类号： B32B27/00
CPC分类号： C09J4/00 , C08F263/04 , C08G61/08 , C08L2666/02 , C09J151/003 , C09J151/06 , C09J151/10 , Y10T428/31536 , Y10T428/31855
摘要： The invention discloses an adhesion agent composition comprising at least one C3-C200 olefin compound having at least one metathesis active double bond, wherein the olefin is substituted or unsubstituted; and at least one compatibilizing functionality for interacting with a substrate surface. The substrate surface can be any surface, for example, silicate glasses, silicate minerals, metals, metal alloys, ceramics, natural stones, plastics, carbon, silicon, and semiconductors. The invention also discloses articles of manufacture utilizing these adhesion agents as well as methods for adhering a polyolefin to a substrate surface.
摘要翻译：本发明公开了一种粘合剂组合物，其包含至少一种具有至少一个复分解活性双键的C 3 -C 20烯烃化合物，其中所述烯烃是取代或未取代的; 以及用于与衬底表面相互作用的至少一种相容性功能。衬底表面可以是任何表面，例如硅酸盐玻璃，硅酸盐矿物，金属，金属合金，陶瓷，天然石，塑料，碳，硅和半导体。本发明还公开了利用这些粘合剂的制品以及将聚烯烃粘附到基材表面的方法。

9. 发明申请

US20110294971A1 Telechelic Olefin Metathesis Polymers from Renewable Feedstocks 有权
标题翻译：来自可再生原料的非线性烯烃复分解聚合物
公开(公告)号：US20110294971A1
公开(公告)日：2011-12-01
申请号：US13060058
申请日：2009-08-21
申请人： Simon C. Jones , Farshad J. Motamedi , Li-Sheng Wang , Brian Edgecombe , Michael A. Giardello
发明人： Simon C. Jones , Farshad J. Motamedi , Li-Sheng Wang , Brian Edgecombe , Michael A. Giardello
IPC分类号： C08F216/04 , C08F232/06 , C08F232/04 , C08F4/80 , C08F222/20 , C08F220/68 , C08F216/10
CPC分类号： C08G61/08 , C08G2261/3322 , C08G2261/418
摘要： Olefin metathesis polymerization reactions are disclosed, and more particularly ring-opening metathesis polymerization of cyclic olefins with olefinic compounds, such as are derived from seed oils and the like, to form telechelic polymers. In one aspect, a method is provided for carrying out a catalytic ring-opening metathesis polymerization reaction, comprising contacting at least one olefinic compound with at least one cyclic olefin, in the presence of a ruthenium alkylidene olefin metathesis catalyst under conditions effective to allow ring-opening metathesis polymerization of the cyclic olefin, whereby the cyclic olefin polymer formed is terminated with the olefinic compound. The invention has utility in the fields of catalysis, organic synthesis, polymer chemistry, and industrial chemistry.
摘要翻译：公开了烯烃易位聚合反应，更具体地说，环烯烃与烯烃化合物如来自种子油等的开环易位聚合反应形成遥爪聚合物。在一个方面，提供了一种用于进行催化开环易位聚合反应的方法，包括在钌亚烷基烯烃复分解催化剂存在下使至少一种烯烃化合物与至少一种环烯烃接触，所述条件有效地允许环开环环烯烃的易位聚合，由此所形成的环烯烃聚合物用烯烃化合物终止。本发明可用于催化，有机合成，聚合物化学和工业化学领域。

10. 发明申请

US20090095635A1 MICROFLUIDIC RADIOSYNTHESIS OF A RADIOLABELED COMPOUND USING ELECTROCHEMICAL TRAPPING AND RELEASE 审中-公开
标题翻译：使用电化学捕获和释放的无定形化合物的微流体放射线
公开(公告)号：US20090095635A1
公开(公告)日：2009-04-16
申请号：US12176296
申请日：2008-07-18
申请人： Arkadij M. Elizarov , Hartmuth C. Kolb , R. Michael van Dam , James R. Heath , Brian Edgecombe , Farshad Motamedi , Anthony Stephen , Michael A. Giardello
发明人： Arkadij M. Elizarov , Hartmuth C. Kolb , R. Michael van Dam , James R. Heath , Brian Edgecombe , Farshad Motamedi , Anthony Stephen , Michael A. Giardello
IPC分类号： C25B3/08
CPC分类号： C07B59/00
摘要： Methods and apparatus enable radiosynthesis of radiolabeled compounds using electrochemical trapping and release. The trapping and release of radioactive isotopes all occur inside a microreactor, a vial or similar device, thus eliminating the need for azeotropic drying and several dead-end filling steps, as well as the necessity to move concentrated radioisotopes from one compartment of the chip to another. These and other features allow radioisotope enrichment to be carried out internally within a radiochemical synthesis chip, providing faster and more robust operation, as well as producing very high radiochemical labeling yields.
摘要翻译：方法和装置能够使用电化学捕获和释放来放射性标记化合物的放射合成。放射性同位素的捕获和释放都发生在微反应器，小瓶或类似装置内，因此不需要共沸干燥和几个死端填充步骤，以及将浓缩放射性同位素从芯片的一个室移动到另一个。这些和其他特征允许放射性同位素富集在放射化学合成芯片内部进行，提供更快和更强的操作，以及产生非常高的放射化学标记产率。

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