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1. 发明授权

US08158716B2 Preparation of hydrolyzable group-containing organohydrogenpolysiloxane and organopolysiloxane derived therefrom 有权
标题翻译：制备含有水解性基团的有机氢聚硅氧烷和由其衍生的有机聚硅氧烷
公开(公告)号：US08158716B2
公开(公告)日：2012-04-17
申请号：US12504019
申请日：2009-07-16
申请人： Masahiro Amemiya , Hitoshi Uehara , Muneo Kudo , Mitsuo Asai
发明人： Masahiro Amemiya , Hitoshi Uehara , Muneo Kudo , Mitsuo Asai
IPC分类号： C08L83/04 , C08G77/12
CPC分类号： C08G77/12 , C08G77/08 , C08G77/34 , C08G77/38
摘要： A hydrolyzable group-containing organohydrogenpolysiloxane is prepared by (A) reacting (a) an organosiloxane with (b) an organosilane or organosiloxane containing a hydrolyzable group, at least one of components (a) and (b) containing hydrosilyl, in the presence of a superstrong acid catalyst, (B) adding an inorganic basic neutralizing agent and/or an adsorbent to the resulting reaction solution, and (C) removing the neutralized and/or adsorbed form of the superstrong acid catalyst. The process proceeds in an essentially non-aqueous system, and the organohydrogenpolysiloxane free of residual acidic catalyst is obtainable at low cost.
摘要翻译：通过（A）使（a）有机硅氧烷与（b）含有可水解基团的有机硅烷或有机硅氧烷，含有氢化甲硅烷基的组分（a）和（b）中的至少一种在有机硅氧烷存在下反应制备可水解基团的有机氢聚硅氧烷）超强酸催化剂，（B）向所得反应溶液中添加无机碱性中和剂和/或吸附剂，（C）除去超强酸催化剂的中和和/或吸附形式。该方法在基本上非水系统中进行，并且以低成本获得不含残留酸性催化剂的有机氢聚硅氧烷。

2. 发明申请

US20100022705A1 PREPARATION OF HYDROLYZABLE GROUP-CONTAINING ORGANOHYDROGENPOLYSILOXANE AND ORGANOPOLYSILOXANE DERIVED THEREFROM 有权
标题翻译：含有可氢化基团的组氨酸聚氧乙烯醚和衍生自其的有机聚硅氧烷的制备
公开(公告)号：US20100022705A1
公开(公告)日：2010-01-28
申请号：US12504019
申请日：2009-07-16
申请人： Masahiro Amemiya , Hitoshi Uehara , Muneo Kudo , Mitsuo Asai
发明人： Masahiro Amemiya , Hitoshi Uehara , Muneo Kudo , Mitsuo Asai
IPC分类号： C08L83/04
CPC分类号： C08G77/12 , C08G77/08 , C08G77/34 , C08G77/38
摘要： A hydrolyzable group-containing organohydrogenpolysiloxane is prepared by (A) reacting (a) an organosiloxane with (b) an organosilane or organosiloxane containing a hydrolyzable group, at least one of components (a) and (b) containing hydrosilyl, in the presence of a superstrong acid catalyst, (B) adding an inorganic basic neutralizing agent and/or an adsorbent to the resulting reaction solution, and (C) removing the neutralized and/or adsorbed form of the superstrong acid catalyst. The process proceeds in an essentially non-aqueous system, and the organohydrogenpolysiloxane free of residual acidic catalyst is obtainable at low cost.
摘要翻译：通过（A）使（a）有机硅氧烷与（b）含有可水解基团的有机硅烷或有机硅氧烷，含有氢化甲硅烷基的组分（a）和（b）中的至少一种在有机硅氧烷存在下反应制备可水解基团的有机氢聚硅氧烷）超强酸催化剂，（B）向所得反应溶液中添加无机碱性中和剂和/或吸附剂，（C）除去超强酸催化剂的中和和/或吸附形式。该方法在基本上非水系统中进行，并且以低成本获得不含残留酸性催化剂的有机氢聚硅氧烷。

3. 发明授权

US06316155B1 External additive for electrostatically charged latent image developing toner 有权
标题翻译：用于静电充电潜像显影调色剂的外用添加剂
公开(公告)号：US06316155B1
公开(公告)日：2001-11-13
申请号：US09524907
申请日：2000-03-13
申请人： Muneo Kudo , Masaki Tanaka , Yoshiteru Sakatsume , Shoji Ichinohe , Mitsuo Asai
发明人： Muneo Kudo , Masaki Tanaka , Yoshiteru Sakatsume , Shoji Ichinohe , Mitsuo Asai
IPC分类号： G03G908
CPC分类号： C09C1/3081 , C01P2004/32 , C01P2004/62 , G03G9/09725
摘要： An external additive for electrostatically charged latent image developing toner is provied. The additive includes spherical hydrophobic fine silica particles having primary particles having a particle diameter of from 0.01 to 5 &mgr;m, which fine silica particles fulfill the following conditions (i) and (ii): (i) when an organic compound which is liquid at room temperature and has a dielectric constant of from 1 to 40 F/m and fine silica particles are mixed in a weight ratio of 5:1 and shaken, the fine silica particles disperse uniformly in the organic compound; and (ii) the quantity of primary particles remaining as primary particles when methanol is evaporated under heating by means of an evaporator from a dispersion prepared by dispersing the fine silica particles in methanol and thereafter the particles are held at a temperature of 100° C. for 2 hours, represents at least 20% of the quantity of primary particles originally present. The external additive does not react or has no interaction with an organic photoreceptor and therefore change in quality does not occur or the photoreceptor is not scraped. Furthermore, it has a good flowability and therefore adhesion of a toner to the photoreceptor does not occur.
摘要翻译：证明了静电充电潜像显影调色剂的外用添加剂。添加剂包括具有粒径为0.01〜5μm的一次粒子的球状疏水性细二氧化硅粒子，二氧化硅微粒满足以下条件（i）和（ii）：（i）当室内为液体的有机化合物时介电常数为1〜40F / m，二氧化硅微粒以5:1的重量比混合并摇动，二氧化硅微粒分散在有机化合物中; 和（ii）当通过蒸发器在加热下从通过将二氧化硅微粒分散在甲醇中制备的分散体蒸发而蒸发甲醇时的初级颗粒的量，然后将颗粒保持在100℃的温度。 2小时，表示原始存在的初级粒子的量的至少20％。外部添加剂不与有机感光体反应或没有相互作用，因此不会发生质量变化或感光体不被刮擦。此外，它具有良好的流动性，因此不会发生调色剂对感光体的粘附。

4. 发明授权

US06855759B2 Silica particles surface-treated with silane, process for producing the same and uses thereof 有权
标题翻译：用硅烷表面处理的二氧化硅颗粒，其制造方法及其用途
公开(公告)号：US06855759B2
公开(公告)日：2005-02-15
申请号：US10284149
申请日：2002-10-31
申请人： Muneo Kudo , Shoji Ichinohe , Atsushi Asami , Mitsuo Asai , Kazuyuki Matsumura , Masaki Tanaka
发明人： Muneo Kudo , Shoji Ichinohe , Atsushi Asami , Mitsuo Asai , Kazuyuki Matsumura , Masaki Tanaka
IPC分类号： C08K9/06 , C08K5/24
CPC分类号： C08K9/06
摘要： Fine silica particles surface-treated with a silane and having primary particles having a particle diameter of from 0.01 to 5 μm, which fine silica particles fulfill the following conditions (i) and (ii), a process for their production and an organic resin composition containing such particles as a component are provided. (i) When an organic compound which is liquid at room temperature and has a dielectric constant of from 1 to 40 F/m and fine silica particles are mixed in a weight ratio of 5:1 and shaked, the fine silica particles disperse uniformly in the organic compound, and (ii) the quantity of primary particles remaining as primary particles when methanol is evaporated under heating by means of an evaporator from a dispersion prepared by dispersing the fine silica particles in methanol and thereafter the particles are held at a temperature of 100° C. for 2 hours, is in a percentage of at least 20% based on the quantity of primary particles originally present. The present fine silica particles are highly dispersible and low aggregative, and the organic resin composition containing them is useful for obtaining films having a good transparency and superior blocking resistance, slip properties and scratch resistance.
摘要翻译：二氧化硅微粒用硅烷表面处理，具有粒径为0.01〜5μm的一次粒子，二氧化硅微粒满足下述条件（i）和（ii），其制造方法和有机树脂组合物提供含有作为组分的颗粒。（i）当室温下介电常数为1〜40F / m的有机化合物和二氧化硅微粒以5:1的重量比混合并摇动时，二氧化硅微粒分散在有机化合物，和（ii）当通过蒸发器从通过将二氧化硅微粒分散在甲醇中制备的分散体在蒸发器中加热蒸发甲醇时剩余的一次颗粒的量，然后将颗粒保持在 100℃，2小时，以原始存在的一次粒子的量为至少20％的百分比。本发明的二氧化硅微粒高分散性和低聚集性，含有它们的有机树脂组合物可用于获得具有良好透明性和优异的抗粘连性，滑爽性和耐划伤性的膜。

5. 发明授权

US6124369A Process for producing organosilicon resin, and process for producing polyurethane foam by using the organosilicon resin obtained by that process 失效
标题翻译：制造有机硅树脂的方法，以及使用通过该方法得到的有机硅树脂制造聚氨酯泡沫的方法
公开(公告)号：US6124369A
公开(公告)日：2000-09-26
申请号：US397635
申请日：1999-09-16
申请人： Muneo Kudo , Shinichi Morioka , Mitsuo Asai
发明人： Muneo Kudo , Shinichi Morioka , Mitsuo Asai
IPC分类号： C08G18/00 , C08G77/06 , C08G77/08 , C08G101/00 , C08G18/61
CPC分类号： C08G77/10 , C08G77/06
摘要： A process for producing an organosilicon resin is disclosed. The process includes the steps of equilibrating a mixture of silane compounds of Si(OR.sup.3).sub.4 wherein R.sup.3 's are a monovalent hydrocarbon group having 1 to 6 carbon atoms; R.sup.2 Si(OR.sup.4).sub.3 wherein R.sup.2 is a monovalent hydrocarbon group having 1 to 20 carbon atoms, and R.sup.4 's are a monovalent hydrocarbon group having 1 to 6 carbon atoms; and R.sup.1.sub.3 SiX wherein X is an --OH group, an --OSiR.sup.1.sub.3 group or a hydrolyzable group, and R.sup.1 's are a monovalent hydrocarbon group having 1 to 6 carbon atoms; adding water to the product of the equilibration reaction to carry out hydrolysis reaction; and adding an aqueous alkali to the product of the hydrolysis reaction to carry out condensation reaction. The organosilicon resin obtained is well dispersible in a resin premix containing a polyol, a blowing agent, a catalyst and a foam stabilizer, and also is highly hydrophobic and low reactive. Hence, the resin premix containing the organosilicon resin has good storage stability. Accordingly, this resin premix need not be agitated when used and also can provide polyurethane foams having superior properties such as dimensional stability.
摘要翻译：公开了一种制备有机硅树脂的方法。该方法包括使Si（OR 3）4的硅烷化合物的混合物平衡的步骤，其中R 3是具有1至6个碳原子的一价烃基; R2Si（OR4）3，其中R2是具有1至20个碳原子的一价烃基，R4是具有1至6个碳原子的一价烃基; 和R 13 SiX，其中X为-OH基，-OSiR13基或可水解基，R 1为具有1至6个碳原子的一价烃基; 向平衡反应产物中加入水进行水解反应; 并向水解反应产物中加入碱水溶液进行缩合反应。获得的有机硅氧烷树脂可以良好地分散在含有多元醇，发泡剂，催化剂和泡沫稳定剂的树脂预混物中，并且还具有高疏水性和低反应性。因此，含有有机硅树脂的树脂预混物具有良好的储存稳定性。因此，该树脂预混物在使用时不需要搅拌，也可以提供具有优异性能如尺寸稳定性的聚氨酯泡沫。

6. 发明授权

US06521290B1 Silica particles surface-treated with silane, process for producing the same and uses thereof 有权
标题翻译：用硅烷表面处理的二氧化硅颗粒，其制造方法及其用途
公开(公告)号：US06521290B1
公开(公告)日：2003-02-18
申请号：US09312054
申请日：1999-05-17
申请人： Muneo Kudo , Shoji Ichinohe , Atsushi Asami , Mitsuo Asai , Kazuyuki Matsumura , Masaki Tanaka
发明人： Muneo Kudo , Shoji Ichinohe , Atsushi Asami , Mitsuo Asai , Kazuyuki Matsumura , Masaki Tanaka
IPC分类号： B05D700
CPC分类号： C08K9/06
摘要： Fine silica particles surface-treated with a silane and having primary particles having a particle diameter of from 0.01 to 5 &mgr;m, which fine silica particles fulfill the following conditions (i) and (ii), a process for their production and an organic resin composition containing such particles as a component are provided. (i) When an organic compound which is liquid at room temperature and has a dielectric constant of from 1 to 40 F/m and fine silica particles are mixed in a weight ratio of 5:1 and shaked, the fine silica particles disperse uniformly in the organic compound, and (ii) the quantity of primary particles remaining as primary particles when methanol is evaporated under heating by means of an evaporator from a dispersion prepared by dispersing the fine silica particles in methanol and thereafter the particles are held at a temperature of 100° C. for 2 hours, is in a percentage of at least 20% based on the quantity of primary particles originally present. The present fine silica particles are highly dispersible and low aggregative, and the organic resin composition containing them is useful for obtaining films having a good transparency and superior blocking resistance, slip properties and scratch resistance.
摘要翻译：二氧化硅微粒用硅烷表面处理，具有粒径为0.01〜5μm的一次粒子，二氧化硅微粒满足下述条件（i）和（ii），其制造方法和有机树脂组合物提供含有作为组分的颗粒。（i）当室温下介电常数为1〜40F / m的有机化合物和二氧化硅微粒以5:1的重量比混合并摇动时，二氧化硅微粒分散在有机化合物，和（ii）当通过蒸发器从通过将二氧化硅微粒分散在甲醇中制备的分散体在蒸发器中加热蒸发甲醇时剩余的一次颗粒的量，然后将颗粒保持在 100℃，2小时，以原始存在的一次粒子的量为至少20％的百分比。本发明的二氧化硅微粒高分散性和低聚集性，含有它们的有机树脂组合物可用于获得具有良好透明性和优异的抗粘连性，滑爽性和耐划伤性的膜。

7. 发明授权

US6166163A Process for producing organosilicon resin and process for producing polyurethane foam by using the organosilicon resin obtained by that process 失效
标题翻译：生产有机硅树脂的方法和使用通过该方法获得的有机硅树脂生产聚氨酯泡沫的方法
公开(公告)号：US6166163A
公开(公告)日：2000-12-26
申请号：US593058
申请日：2000-06-13
申请人： Muneo Kudo , Shinichi Morioka , Mitsuo Asai
发明人： Muneo Kudo , Shinichi Morioka , Mitsuo Asai
IPC分类号： C08G18/00 , C08G77/06 , C08G77/08 , C08G101/00
CPC分类号： C08G77/10 , C08G77/06
摘要： A process for producing an organosilicon resin is disclosed. The process includes the steps of equilibrating a mixture of silane compounds of Si(OR.sup.3).sub.4 wherein R.sup.3 's are a monovalent hydrocarbon group having 1 to 6 carbon atoms; R.sup.2 Si(OR.sup.4).sub.3 wherein R.sup.2 is a monovalent hydrocarbon group having 1 to 20 carbon atoms, and R.sup.4 's are a monovalent hydrocarbon group having 1 to 6 carbon atoms; and R.sup.1.sub.3 SiX wherein X is an --OH group, an --OSiR.sup.1.sub.3 group or a hydrolyzable group, and R.sup.1 's are a monovalent hydrocarbon group having 1 to 6 carbon atoms; adding water to the product of the equilibration reaction to carry out hydrolysis reaction; and adding an aqueous alkali to the product of the hydrolysis reaction to carry out condensation reaction. The organosilicon resin obtained is well dispersible in a resin premix containing a polyol, a blowing agent, a catalyst and a foam stabilizer, and also is highly hydrophobic and low reactive. Hence, the resin premix containing the organosilicon resin has good storage stability. Accordingly, this resin premix need not be agitated when used and also can provide polyurethane foams having superior properties such as dimensional stability.
摘要翻译：公开了一种制备有机硅树脂的方法。该方法包括使Si（OR 3）4的硅烷化合物的混合物平衡的步骤，其中R 3是具有1至6个碳原子的一价烃基; R2Si（OR4）3，其中R2是具有1至20个碳原子的一价烃基，R4是具有1至6个碳原子的一价烃基; 和R 13 SiX，其中X为-OH基，-OSiR13基或可水解基，R 1为具有1至6个碳原子的一价烃基; 向平衡反应产物中加入水进行水解反应; 并向水解反应产物中加入碱水溶液进行缩合反应。获得的有机硅氧烷树脂可以良好地分散在含有多元醇，发泡剂，催化剂和泡沫稳定剂的树脂预混物中，并且还具有高疏水性和低反应性。因此，含有有机硅树脂的树脂预混物具有良好的储存稳定性。因此，该树脂预混物在使用时不需要搅拌，也可以提供具有优异性能如尺寸稳定性的聚氨酯泡沫。

8. 发明授权

US6140451A Surface treating compositions 失效
标题翻译：表面处理组合物
公开(公告)号：US6140451A
公开(公告)日：2000-10-31
申请号：US174257
申请日：1998-10-16
申请人： Mitsuo Asai , Hitoshi Uehara
发明人： Mitsuo Asai , Hitoshi Uehara
IPC分类号： C09D183/14 , C09D183/16 , C08G77/24
CPC分类号： C09D183/14 , C09D183/16
摘要： A composition comprising a trifunctional polysilazane and a polysiloxane having at least one hydrolyzable group and an optional fluoroalkyl group is effective for treating substrates to render their surface water repellent, oil repellent, and anti-fouling.
摘要翻译：包含三官能聚硅氮烷和具有至少一个可水解基团和任选的氟烷基的聚硅氧烷的组合物对于处理基材以使其表面具有防水性，拒油性和防污性是有效的。

9. 发明授权

US06780514B2 Optical communication device substrate and optical communication device 失效
标题翻译：光通信设备基板和光通信设备
公开(公告)号：US06780514B2
公开(公告)日：2004-08-24
申请号：US10212763
申请日：2002-08-07
申请人： Satoru Yoshihara , Takahiro Matano , Akihiko Sakamoto , Mitsuo Asai , Hitoshi Uehara
发明人： Satoru Yoshihara , Takahiro Matano , Akihiko Sakamoto , Mitsuo Asai , Hitoshi Uehara
IPC分类号： B32B1706
CPC分类号： G02B6/12 , C03C17/30 , G02B6/0218 , G02B6/02209 , Y10T428/24926 , Y10T428/249953 , Y10T428/249956 , Y10T428/249969 , Y10T428/31612 , Y10T428/31663
摘要： An optical communication device substrate made of ceramic or glass-ceramic having a negative thermal expansion coefficient in the range of −10 to −120×10−7/° C. in a temperature range of −40 to 100° C., treated with a solution containing at least one organic silicon compound selected from the group consisting of siloxane compounds and silazane compounds.
摘要翻译：一种由陶瓷或玻璃陶瓷制成的光通讯器件衬底，其在-40至100℃的温度范围内具有在-10至-120×10 -7 /℃范围内的负热膨胀系数，用含有至少一种选自硅氧烷化合物和硅氮烷化合物的有机硅化合物的溶液。

10. 发明授权

US06652640B2 Surface treating agent and water repellent, oil repellent article 失效
公开(公告)号：US06652640B2
公开(公告)日：2003-11-25
申请号：US09893601
申请日：2001-06-29
申请人： Mitsuo Asai , Hitoshi Uehara
发明人： Mitsuo Asai , Hitoshi Uehara
IPC分类号： C09D520
CPC分类号： C09K3/18 , C08G77/388 , C09D183/14 , Y10T428/31663
摘要： A surface treating agent is comprised of the reaction product obtained by reacting with ammonia a mixture of (A) an organosilicon compound having a fluorinated organic group and (B) an organosilicon compound having a hydrolyzable group. Substrates treated therewith exhibit high water and oil repellency and allow sticking contaminants to be effectively wiped off.

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