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1. 发明授权

US06342612B1 Indane aldehydes and derivatives 有权
标题翻译：吲哚醛及其衍生物
公开(公告)号：US06342612B1
公开(公告)日：2002-01-29
申请号：US09770739
申请日：2001-01-26
申请人： Mark A. Sprecker , Richard A. Weiss , Robert P. Belko , Ellen Ann Molner
发明人： Mark A. Sprecker , Richard A. Weiss , Robert P. Belko , Ellen Ann Molner
IPC分类号： C07D30700
CPC分类号： C07C47/235 , C07C43/168 , C07C2602/08 , C07D317/12 , C11B9/0049 , C11B9/0076
摘要： The present invention is directed to indanyl derivatives and the use of the indanyl derivatives in creating fragrances, and scents in items such as perfumes colognes and personal care products.
摘要翻译：本发明涉及茚满基衍生物以及茚满基衍生物在制备香料中的用途，以及香料如香水和个人护理产品中的香料。

2. 发明授权

US06362141B1 Indanyl derivatives 有权
标题翻译：茚基衍生物
公开(公告)号：US06362141B1
公开(公告)日：2002-03-26
申请号：US09948511
申请日：2001-09-06
申请人： Mark A. Sprecker , Richard A. Weiss , Robert P. Belko , Ellen Ann Molner
发明人： Mark A. Sprecker , Richard A. Weiss , Robert P. Belko , Ellen Ann Molner
IPC分类号： C11D320
CPC分类号： C07C47/235 , C07C43/168 , C07C2602/08 , C07D317/12 , C11B9/0049 , C11B9/0076
摘要： The present invention is directed to indanyl derivatives and the use of the indanyl derivatives in creating fragrances, and scents in items such as perfumes, colognes and personal care products.
摘要翻译：本发明涉及茚满基衍生物和茚满基衍生物在制备香料中的用途，以及香料，古龙水和个人护理产品中的香料。

3. 发明授权

US5023352A Alkyl-substituted tetra- or hexahydrobenzopyran derivatives, organoleptic uses thereof and process for preparing same 失效
标题翻译：烷基取代的四或六氢苯并吡喃衍生物，其感官用途及其制备方法
公开(公告)号：US5023352A
公开(公告)日：1991-06-11
申请号：US546356
申请日：1990-06-29
申请人： Mark A. Sprecker , Robert P. Belko , Marie R. Hanna , Charles E. J. Beck , Salvatore M. Brucato
发明人： Mark A. Sprecker , Robert P. Belko , Marie R. Hanna , Charles E. J. Beck , Salvatore M. Brucato
IPC分类号： C07D311/74 , C07D311/94 , C11B9/00 , C11D3/50
CPC分类号： C07D311/74 , C07D311/94 , C11B9/008 , C11D3/50
摘要： Described are alkyl-substituted tetra- or hexahydrobenzopyran derivatives defined according to one of the generic structures: ##STR1## wherein Z is a moiety in the alternative either ##STR2## wherein in the moiety having the structure: ##STR3## R' is methyl or ethyl and in the moiety having the structure: ##STR4## one of the dashed lines is a carbon-carbon double bond and each of the other of the dashed lines represent carbon-carbon single bonds; wherein R.sub.1 and R.sub.2 taken separately represent hydrogen or C.sub.1 -C.sub.3 lower alkyl (with the proviso that R.sub.1 and R.sub.2 are not both hydrogen) or R.sub.1 and R.sub.2 taken together complete a C.sub.5 or C.sub.6 cycloalkyl moiety; and uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles including but not limited to solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles, hair preparations, cosmetic powder and perfumed polymers. Also described are synthesis processes for preparing such alkyl-substituted tetra- or hexahydrobenzopyran derivatives by means of reacting isopulegol or an isomer thereof with an acetal or ketal.
摘要翻译：描述了根据以下通用结构之一定义的烷基取代的四或六氢苯并吡喃衍生物：其中Z是可选择的部分或其中的“IMAGE”或“IMAGE”，其中在具有以下结构的部分中： R'是甲基或乙基，并且在具有以下结构的部分中：虚线之一是碳 - 碳双键，虚线中的每一个代表碳 - 碳单键; 其中R1和R2分别代表氢或C1-C3低级烷基（前提是R1和R2不同时为氢）或R1和R2一起形成C5或C6环烷基部分; 包括但不限于固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，织物柔软剂制品，毛发制剂，化妆品粉末和加香聚合物的香料组合物，古龙水和香料制品的香气。。还描述了通过异丙醇或其异构体与缩醛或缩酮反应制备这种烷基取代的四或六氢苯并吡喃衍生物的合成方法。

4. 发明授权

US4902672A Polyalkyl indanyl n-propyl and allyl ethers and perfumery uses thereof 失效
标题翻译：聚烷基茚基丙基正丙基和烯丙基醚及其香料用途
公开(公告)号：US4902672A
公开(公告)日：1990-02-20
申请号：US371294
申请日：1989-06-26
申请人： Mark A. Sprecker , Robert P. Belko , Ronald S. Fenn
发明人： Mark A. Sprecker , Robert P. Belko , Ronald S. Fenn
IPC分类号： C07C43/188 , C11B9/00 , C11D3/50
CPC分类号： C11B9/0049 , C07C43/188 , C11D3/50 , C07C2102/24
摘要： Described are polyalkyl indanyl n-propyl and allyl ethers defined according to the structure: ##STR1## wherein R.sub.3 represents methyl or hydrogen; wherein R.sub.1, R.sub.2, R.sub.4 and R.sub.5 each represents methyl or ethyl and wherein the dashed line represents a carbon-carbon single bond or a carbon-carbon double bond with the provisos that:1. at least three of R.sub.1, R.sub.2, R.sub.4 and R.sub.5 represents methyl;2. when each of R.sub.1, R.sub.2, R.sub.4 and R.sub.5 is methyl, then R.sub.3 is methyl; and3. when the dashed line is a carbon-carbon double bond and R.sub.1, R.sub.2, R.sub.3, R.sub.4 and R.sub.5 are each methyland uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles including but not limited to perfumed polymers, solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles, cosmetic powders and hair preparations.
摘要翻译：描述了根据以下结构定义的聚烷基茚满基丙基和烯丙基醚：其中R 3表示甲基或氢; 其中R1，R2，R4和R5各自表示甲基或乙基，其中虚线表示碳 - 碳单键或碳 - 碳双键，条件是：1. R1，R2，R4和R5中的至少三个代表甲基; 当R1，R2，R4和R5各自为甲基时，则R3为甲基; 和3.当虚线是碳 - 碳双键时，R 1，R 2，R 3，R 4和R 5各自是甲基，并且其用途用于增强或增强香水组合物，古龙水和香料制品的香气，包括但不限于香料聚合物，固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，织物柔软剂制品，化妆粉和头发制剂。

5. 发明授权

US4772583A Beta-alkylidene phenethyl alcohol esters and ethers, organoleptic uses thereof and processes for preparing same 失效
标题翻译： β-亚烷基苯乙醇酯和醚，其感官用途及其制备方法
公开(公告)号：US4772583A
公开(公告)日：1988-09-20
申请号：US134817
申请日：1987-12-18
申请人： Mark A. Sprecker , Robert P. Belko , Richard M. Boden , Marie R. Hanna
发明人： Mark A. Sprecker , Robert P. Belko , Richard M. Boden , Marie R. Hanna
IPC分类号： C11B9/00 , A61K7/46
CPC分类号： C11B9/0061
摘要： Described is the novel compound genus the beta-alkylidene phenethyl alcohol esters and ethers of our invention defined according to the generic structure: ##STR1## wherein R.sub.5 represents hydrogen or methyl; wherein R.sub.6 represents one of the moieties: ##STR2## wherein R.sub.1, R.sub.2, R.sub.3 and R.sub.4 each represents the same or different hydrogen or methyl; wherein R.sub.7 represents methyl or ethyl; and wherein R.sub.8 represents hydrogen or methyl; useful in augmenting or enhancing the aroma of consumable materials including perfumes, colognes and perfumed articles including solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener articles, fabric softener compositions, cosmetic powders and hair preparations.
摘要翻译：描述了根据通用结构定义的本发明的β-亚烷基苯乙醇酯和醚的新化合物：其中R 5表示氢或甲基; 其中R 6表示以下部分之一：其中R 1，R 2，R 3和R 4各自表示相同或不同的氢或甲基; 其中R 7表示甲基或乙基; 并且其中R8表示氢或甲基; 可用于增强或增强消耗材料的香气，包括香料，古龙水和加香制品，包括固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂制品，织物柔软剂组合物，化妆粉和头发制剂。

6. 发明授权

US4629805A Alkyl substituted and unsubstituted para-carboalkoxy cyclohexanones and organoleptic uses thereof 失效
公开(公告)号：US4629805A
公开(公告)日：1986-12-16
申请号：US726603
申请日：1985-04-23
申请人： Mark A. Sprecker , Wilhelmus J. Wiegers , Robert P. Belko , Richard M. Boden
发明人： Mark A. Sprecker , Wilhelmus J. Wiegers , Robert P. Belko , Richard M. Boden
IPC分类号： C08K5/101 , C11B9/00 , C11D3/50 , C07C69/757
CPC分类号： C11B9/0034 , C08K5/101 , C11D3/50
摘要： Described are para-carboalkoxy cyclohexanones defined according to the structure: ##STR1## wherein R.sub.1 represents hydrogen or C.sub.1 -C.sub.7 alkyl and R.sub.2 represents methyl or ethyl and uses thereof in augmenting or enhancing the aroma of consumable materials including foodstuffs, chewing gums, toothpastes, medicinal products, chewing tobaccos, perfume compositions, colognes and perfumed articles (e.g., solid or liquid anionic, cationic, nonionic or zwitterionic detergents, cosmetic compositions, fabric softener compositions, fabric softener articles, hair preparations and perfumed polymers. The compounds defined according to the structure: ##STR2## wherein R.sub.1 ' represents C.sub.4 -C.sub.7 alkyl and R.sub.2 represents methyl or ethyl are novel compounds.

7. 发明授权

US4613706A Isomer-directed process for producing asymmetric ketones using catalytic Claisen rearrangement of allylic ethers, intermediates, and uses of products and intermediates of process in perfumery 失效
公开(公告)号：US4613706A
公开(公告)日：1986-09-23
申请号：US765231
申请日：1985-08-13
申请人： Mark A. Sprecker , Robert P. Belko , William L. Schreiber , Michael Licciardello
发明人： Mark A. Sprecker , Robert P. Belko , William L. Schreiber , Michael Licciardello
IPC分类号： C07C43/305 , C07C45/51 , C07C49/203 , C07C49/217 , C07C403/00 , C11B9/00
CPC分类号： C07C403/16 , C07C43/305 , C07C45/515 , C11B9/0015 , C11B9/0034 , C11B9/0061 , C07C2101/14 , C07C2101/16
摘要： Described is an isomer-directed process for producing asymmetric ketones defined according to the generic structure: ##STR1## wherein one of Z.sub.1 or Z.sub.2 is the moiety: ##STR2## and the other of Z.sub.1 or Z.sub.2 is hydrogen; wherein R.sub.11 and R.sub.21 represent hydrogen or the same or different alkyl or alkenyl with the proviso that R.sub.11 and R.sub.21 are not both hydrogen or wherein R.sub.11 and R.sub.21 taken together:(i) complete a cycloalkyl, cycloalkenyl, bicycloalkyl, mono or polyalkyl cycloalkyl or mono or polyalkyl cycloalkenyl ring, or(ii) represent alkylidene, cycloalkenyl alkylidene, aralkylidene, mono or polyalkyl cycloalkenyl alkylidene or mono or polyalkyl aralkylidene;and wherein R.sub.6, R.sub.7 and R.sub.8 are the same or different and each represents hydrogen or methyl, using a catalytic Claisen rearrangement of allylic ethers previously formed by reacting substituted or unsubstituted allylic alcohols defined according to the structure: ##STR3## with dialkyl ketals defined according to the structure: ##STR4## wherein R.sub.4 and R.sub.5 represent the same or different C.sub.1 -C.sub.4 alkyl.Also described are compounds and processes for using same in perfumery defined according the structures: ##STR5## Also described are certain diallylic ethers defined according to the generic structure: ##STR6##

8. 发明授权

US4493790A Organoleptic use of isopropyl tetramethylindanes 失效
标题翻译：感官使用异丙基四甲基茚满
公开(公告)号：US4493790A
公开(公告)日：1985-01-15
申请号：US541263
申请日：1983-10-12
申请人： Mark A. Sprecker , Robert P. Belko , Roger E. Greene
发明人： Mark A. Sprecker , Robert P. Belko , Roger E. Greene
IPC分类号： C07C5/29 , C07C45/46 , C07C49/792 , C11B9/00
CPC分类号： C11B9/0049 , C07C45/46 , C07C49/792 , C07C5/29
摘要： Described are isopropyl tetramethylindan musks defined according to the generic structure: ##STR1## wherein R.sub.3 and R.sub.4 are each acetyl or methyl with the provisos:(a) one of R.sub.3 or R.sub.4 is methyl;(b) when R.sub.4 is methyl, then R.sub.3 is acetyl and(c) when R.sub.4 is acetyl, R.sub.3 is methyland organoleptic uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles.
摘要翻译：描述了根据通用结构定义的异丙基四甲基茚满麝香：其中R 3和R 4各自为乙酰基或甲基，条件是：（a）R 3或R 4中的一个为甲基; （b）当R 4为甲基时，R 3为乙酰基，（c）当R 4为乙酰基时，R 3为甲基和感官用途，用于增强或增强香水组合物，古龙水和香料制品的香味。

9. 发明授权

US4460795A Process for preparing mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives 失效
公开(公告)号：US4460795A
公开(公告)日：1984-07-17
申请号：US478355
申请日：1983-03-24
申请人： Mark A. Sprecker , Marie R. Hanna , Richard J. Tokarzewski , Robert P. Belko , Hugh Watkins , Manfred H. Vock
发明人： Mark A. Sprecker , Marie R. Hanna , Richard J. Tokarzewski , Robert P. Belko , Hugh Watkins , Manfred H. Vock
IPC分类号： A24B15/34 , C07C47/347 , C07C47/445 , C07C93/16
CPC分类号： A24B15/345 , C07C47/347 , C07C47/445
摘要： Described are mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives having the generic structure: ##STR1## wherein the dashed line represents a carbon-carbon single bond or a carbon-carbon double bond; wherein R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 "', R.sub.1 "", R.sub.3, R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 "', R.sub.5 "" and R.sub.6 represent hydrogen or methyl with the provisos:(i) at least four of R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 "' and R.sub.1 "" are hydrogen; and (ii) at least four of R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 "' and R.sub.5 "" represent hydrogen;and wherein Z represents one of the moieties:(i) carboxaldehyde having the structure: ##STR2## (ii) alkylene dioxy or dialkoxy methyl having the structure: ##STR3## (iii) hydroxy methyl having the structure: ##STR4## (iv) acetoxymethyl having the structure: ##STR5## and wherein R.sub.7 and R.sub.8 taken separately represent C.sub.1 -C.sub.4 lower alkyl or R.sub.7 and R.sub.8 taken together represent C.sub.2 -C.sub.4 alkylene; wherein the line represented by:[++++]is either (i) a carbon-carbon single bond when R.sub.7 and R.sub.8 taken together are C.sub.2 -C.sub.4 alkylene or (ii) no bond at all when R.sub.7 and R.sub.8 taken separately represent C.sub.1 -C.sub.4 lower alkyl. Also described are processes for preparing such mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives, and processes for using the above defined mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives for their organoleptic properties and compositions containing said mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives including perfumes, perfumed articles (such as solid or liquid anionic, cationic, nonionic or zwitterionic detergents, perfumed polymers, fabric softeners and cosmetic powders), foodstuffs, chewing gums, toothpastes, medicinal products, chewing tobaccos, smoking tobaccos and smoking tobacco articles.

10. 发明授权

US5378685A Process for preparing mixture of trimethyl and dimethylmethylene propyl polyhydropyrans, products produced thereby perfumery uses of such product 失效
标题翻译：制备三甲基和二甲基亚甲基丙基多羟基吡喃的混合物的方法，由此产生的产品由此产生香料的用途
公开(公告)号：US5378685A
公开(公告)日：1995-01-03
申请号：US214185
申请日：1994-03-17
申请人： Mark A. Sprecker , Robert P. Belko , Marie R. Hanna
发明人： Mark A. Sprecker , Robert P. Belko , Marie R. Hanna
IPC分类号： C07D309/04 , C07D309/12 , C11B9/00 , A61K7/46
CPC分类号： C07D309/12 , C07D309/04 , C11B9/008
摘要： Described is a process for preparing trimethyl and dimethylmethylene propyl polyhydropyran derivatives including compounds defined according to the structure: ##STR1## which defines a mixture wherein in the mixture, in each of the compounds one of the dashed lines is a carbon-carbon double bond and each of the other of the dashed lines represents a carbon-carbon single bond as well as the compound having the structure: ##STR2## products produced thereby; perfumery uses of such products; process intermediates of such process including compounds defined according to the structures: ##STR3## wherein X represents chloro or bromo.
摘要翻译：描述了一种制备三甲基和二甲基亚甲基丙基多氢吡喃衍生物的方法，其包括根据以下结构定义的化合物：其定义为混合物，其中在每种化合物中，虚线中的一个为碳 - 碳双键，虚线中的每一个代表碳 - 碳单键，以及具有以下结构的化合物：由此产生的产物; 这种产品的香水用途; 该方法的加工中间体包括根据以下结构定义的化合物：其中X表示氯或溴。

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