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1. 发明授权

US5364541A Method to impart coffee stain resistance to polyamide textile substrates 失效
标题翻译：赋予聚酰胺纺织品基材耐咖啡渍耐性的方法
公开(公告)号：US5364541A
公开(公告)日：1994-11-15
申请号：US894702
申请日：1992-06-05
申请人： Lidia T. Calcaterra , Mathias P. Koljack , Qamardin Farishta , Michael G. Koehler , William B. Bedwell , Dale A. Hangey , George D. Green
发明人： Lidia T. Calcaterra , Mathias P. Koljack , Qamardin Farishta , Michael G. Koehler , William B. Bedwell , Dale A. Hangey , George D. Green
IPC分类号： D06M15/233 , D06M15/263 , D06M101/00 , D06M101/16 , D06M101/30 , D06M101/34 , D06M101/36 , D06M15/00
CPC分类号： D06M15/263 , D06M15/233
摘要： The present invention provides methods and compositions to impart coffee stain resistance to polyamide textile substrates such as carpets. The compositions comprise either (i) a copolymer selected from the group consisting of a hydrolyzed aromatic-containing vinyl ether maleic anhydride copolymer, a half ester of an aromatic-containing vinyl ether maleic anhydride copolymer, and mixtures thereof, or (ii) an aromatic-containing acrylate copolymerized with an acid selected from the group consisting of acrylic acid and maleic acid. The coffee stain-resistant polyamide textile substrates made are also part of the invention.
摘要翻译：本发明提供了对诸如地毯的聚酰胺纺织物基材赋予咖啡耐污染性的方法和组合物。所述组合物包含（i）选自由水解的含芳族乙烯基醚马来酸酐共聚物，含芳族乙烯基醚马来酸酐共聚物的半酯及其混合物组成的组的共聚物，或（ii）芳族化合物的丙烯酸酯与选自丙烯酸和马来酸的酸共聚。制成的咖啡耐污染的聚酰胺纺织品基材也是本发明的一部分。

2. 发明授权

US5359010A Method to impart coffee stain resistant to polyamide textile substances 失效
标题翻译：赋予耐聚酰胺纺织物质的咖啡污渍的方法
公开(公告)号：US5359010A
公开(公告)日：1994-10-25
申请号：US988506
申请日：1992-12-10
申请人： Lidia T. Calcaterra , Mathias P. Koljack , Qamardin Farishta , Michael G. Koehler , William B. Bedwell , Dale A. Hangey , George D. Green
发明人： Lidia T. Calcaterra , Mathias P. Koljack , Qamardin Farishta , Michael G. Koehler , William B. Bedwell , Dale A. Hangey , George D. Green
IPC分类号： D06M15/233 , D06M15/263 , D06M101/00 , D06M101/16 , D06M101/30 , D06M101/34 , D06M101/36 , C08F222/20 , C08F222/08
CPC分类号： D06M15/263 , D06M15/233
摘要： The present invention provides methods and compositions to impart coffee stain resistance to polyamide textile substrates such as carpets. The compositions comprise either (i) a copolymer selected from the group consisting of a hydrolyzed aromatic-containing vinyl ether maleic anhydride copolymer, a half ester of an aromatic-containing vinyl ether maleic anhydride copolymer, and mixtures thereof, or (ii) an aromatic-containing acrylate copolymerized with an acid selected from the group consisting of acrylic acid and maleic acid. The coffee stain-resistant polyamide textile substrates made are also part of the invention.
摘要翻译：本发明提供了对诸如地毯的聚酰胺纺织物基材赋予咖啡耐污染性的方法和组合物。所述组合物包含（i）选自由水解的含芳族乙烯基醚马来酸酐共聚物，含芳族乙烯基醚马来酸酐共聚物的半酯及其混合物组成的组的共聚物，或（ii）芳族化合物的丙烯酸酯与选自丙烯酸和马来酸的酸共聚。制成的咖啡耐污染的聚酰胺纺织品基材也是本发明的一部分。

3. 发明授权

US5135774A Method to impart coffee stain resistance to polyamide fibers 失效
标题翻译：提高咖啡对聚酰胺纤维的耐污染性的方法
公开(公告)号：US5135774A
公开(公告)日：1992-08-04
申请号：US500813
申请日：1990-03-27
申请人： Lidia T. Calcaterra , Mathias P. Koljack , Qamardin Farishta , Michael G. Koehler , William B. Bedwell , Dale A. Hangey , George D. Green
发明人： Lidia T. Calcaterra , Mathias P. Koljack , Qamardin Farishta , Michael G. Koehler , William B. Bedwell , Dale A. Hangey , George D. Green
IPC分类号： D06M15/233 , D06M15/263 , D06M101/00 , D06M101/16 , D06M101/30 , D06M101/34 , D06M101/36
CPC分类号： D06M15/263 , D06M15/233
摘要： A method to impart coffee stain resistance to polyamide fibers such as those found in textile substrates (e.g., carpets). The method includes preparing an aqueous dispersion of charged microfine beads of either (i) a copolymer selected from the group consisting of a hydrolyzed aromatic-containing vinyl ether maleic anhydride copolymer, a half ester of an aromatic-containing vinyl ether maleic anhydride copolymer, and mixtures thereof, or (ii) an aromatic-containing acrylate copolymerized with an acid selected from the group consisting of acrylic acid and maleic acid, immersing the polyamide fiber in the aqueous dispersion so that the beads contact and coat the fiber via an electrostatic attraction. The aqueous dispersion is prepared by dissolving the polymer into a water-soluble solvent to form a solution, injecting the solution into water, and evaporating the solvent.
摘要翻译：赋予聚酰胺纤维耐咖啡污染性的方法，例如在织物基材（例如地毯）中发现的那些。该方法包括制备带电微细珠粒的水性分散体，其选自（i）选自由水解的含芳族乙烯基醚马来酸酐共聚物，含芳族乙烯基醚马来酸酐共聚物的半酯，和其混合物，或（ii）与选自丙烯酸和马来酸的酸共聚的含芳族酯的丙烯酸酯，将聚酰胺纤维浸渍在水性分散体中，使得珠粒通过静电吸引而接触和涂覆纤维。通过将聚合物溶解在水溶性溶剂中以形成溶液，将溶液注入水中并蒸发溶剂来制备水分散体。

4. 发明授权

US5118551A Method to impart stain resistance to polyamide textile substrates 失效
标题翻译：赋予聚酰胺纺织品基材耐污性的方法
公开(公告)号：US5118551A
公开(公告)日：1992-06-02
申请号：US716163
申请日：1991-07-11
申请人： Lidia T. Calcaterra , Mathias P. Koljack , Qamardin Farishta , Michael G. Koehler , William B. Bedwell , Dale A. Hangey , George D. Green
发明人： Lidia T. Calcaterra , Mathias P. Koljack , Qamardin Farishta , Michael G. Koehler , William B. Bedwell , Dale A. Hangey , George D. Green
IPC分类号： D06M15/233 , D06M15/263
CPC分类号： D06M15/233 , D06M15/263 , Y10S8/21 , Y10S8/924 , Y10S8/925 , Y10T428/23986 , Y10T428/2907 , Y10T428/2938 , Y10T428/2969 , Y10T428/31743 , Y10T428/3175 , Y10T442/2279
摘要： The present invention provides methods and compositions to impart coffee stain resistance to polyamide textile substrate such as carpets. The compositions comprise either (i) a copolymer selected from the group consisting of a hydrolyzed aromatic-containing vinyl ether maleic anhydride copolymer, a half ester of an aromatic-containing vinyl ether maleic anhydride copolymer, and mixtures thereof, or (ii) an aromatic-containing acrylate copolymerized with an acid selected from the group consisting of acrylic acid and maleic acid. The coffee stain-resistant polyamide textile substrates made are also part of the invention.
摘要翻译：本发明提供了对诸如地毯的聚酰胺纺织基材赋予咖啡耐污染性的方法和组合物。所述组合物包含（i）选自由水解的含芳族乙烯基醚马来酸酐共聚物，含芳族乙烯基醚马来酸酐共聚物的半酯及其混合物组成的组的共聚物，或（ii）芳族化合物的丙烯酸酯与选自丙烯酸和马来酸的酸共聚。制成的咖啡耐污染的聚酰胺纺织品基材也是本发明的一部分。

5. 发明授权

US5230708A Methods and compositions to enhance stain resistance of nylon carpet fibers: thlocyanate to reduce yellowing 失效
标题翻译：增强尼龙地毯纤维耐污染性的方法和组合物：硫氰酸盐以减少黄变
公开(公告)号：US5230708A
公开(公告)日：1993-07-27
申请号：US361671
申请日：1989-06-01
申请人： Dale A. Hangey , Paul W. Harris , Daniel J. Corcoran, Jr. , Michael P. Friedberger , Charles J. Cole , William A. Archie , Roger N. Spitz
发明人： Dale A. Hangey , Paul W. Harris , Daniel J. Corcoran, Jr. , Michael P. Friedberger , Charles J. Cole , William A. Archie , Roger N. Spitz
IPC分类号： D06M15/277 , D06M15/41
CPC分类号： D06M15/412 , D06M15/277 , D06M2101/12 , D06M2101/34 , Y10S8/924 , Y10S8/929 , Y10T428/23979 , Y10T428/23986 , Y10T428/23993 , Y10T428/2969
摘要： This invention relates to improved methods and compositions to enhance stain resistance of carpet fiber. The improved methods relate to a continuous aftertreatment for dyed carpet fabric and to two-step processes, either batch-batch, batch-continuous or continuous-continuous. The improved compositions are used in the processes to enhance stain resistance of carpet or carpet fiber and to overcome various prior drawbacks, such as, yellowing, oxidation and durability to cleaning. The sulfonated aromatic condensates are used to enhance stain resistance, and can be combined with fluorocarbon compounds for soil resistance, thiocyanates, and/or salts having divalent cations, such as magnesium sulfate. Also various dispersing agents, buffering acids and sequestering agents are disclosed.
摘要翻译：本发明涉及改善地毯纤维耐污染性的方法和组合物。改进的方法涉及染色地毯织物的连续后处理和批次间歇，间歇连续或连续连续的两步法。改进的组合物用于增强地毯或地毯纤维的抗污性和克服各种先前缺点的方法，例如变黄，氧化和对清洁的耐久性。磺化芳族缩合物用于增强耐污染性，并且可以与用于土壤抗性的碳氟化合物，硫氰酸盐和/或具有二价阳离子的盐如硫酸镁组合。还公开了各种分散剂，缓冲酸和螯合剂。

6. 发明授权

US07258920B2 Multiphase fiber materials and compositions, methods of manufacture and uses thereof 有权
标题翻译：多相纤维材料及组合物，制造方法及其应用
公开(公告)号：US07258920B2
公开(公告)日：2007-08-21
申请号：US10717048
申请日：2003-11-18
申请人： John B. Boyle , James A. Kweeder , Dale A. Hangey , Samir Abdalla
发明人： John B. Boyle , James A. Kweeder , Dale A. Hangey , Samir Abdalla
IPC分类号： D02G3/00
CPC分类号： D01F6/90 , C08K5/3412 , Y10T428/2913 , C08L77/00
摘要： A pre-fiber composition is disclosed herein that includes: a) a first fiber constituent having a first melting point; b) a second fiber constituent having a second melting point; and c) a gelling agent that solvates at least one of the first fiber constituent or the second fiber constituent, wherein the gelling agent significantly reduces co-polymerization of either of the constituents in the composition. A fiber is also disclosed herein that includes: a) at least two amide-based polymers, each having a melting point, wherein the melting point of one amide-based polymer is dissimilar to the melting point of a second amide-based polymer; and b) a gelling agent that is compatible with at least one of the amide-based polymers, wherein the fiber comprises two differentiatable melting points that are substantially similar to the melting points of each of the amide-based polymers. A method of producing a pre-fiber composition is disclosed herein that includes: a) providing a first fiber constituent having a first melting point; b) providing a second fiber constituent having a second melting point, wherein the first melting point and the second melting point are dissimilar; c) providing at least one gelling agent; and d) mixing the first constituent, the second constituent and the at least one gelling agent such that there is sufficient viscosity and sufficient melt strength in the composition so that it can be spun into a fiber and such that the first melting point and the second melting point in the fiber are substantially similar to their original values before mixing.
摘要翻译：本文公开了一种预纤维组合物，其包括：a）具有第一熔点的第一纤维组分; b）具有第二熔点的第二纤维成分; 和c）溶剂化第一纤维组分或第二纤维组分中的至少一种的胶凝剂，其中胶凝剂显着降低组合物中任一组分的共聚。本文还公开了一种纤维，其包括：a）至少两种各自具有熔点的酰胺类聚合物，其中一种酰胺类聚合物的熔点不同于第二种酰胺类聚合物的熔点; 和b）与至少一种酰胺类聚合物相容的胶凝剂，其中纤维包含基本上类似于每种酰胺类聚合物的熔点的两个可分离的熔点。本文公开了一种生产预纤维组合物的方法，其包括：a）提供具有第一熔点的第一纤维成分; b）提供具有第二熔点的第二纤维成分，其中所述第一熔点和所述第二熔点不相似; c）提供至少一种胶凝剂; 和d）混合第一组分，第二组分和至少一种胶凝剂，使得在组合物中具有足够的粘度和足够的熔体强度，使得其可以纺成纤维，使得第一熔点和第二熔点纤维中的熔点基本上与混合前的原始值相似。

7. 发明授权

US5152803A Methods and compositions to enhance stain resistance of carpet fibers with water-soluble thiocyanate 失效
标题翻译：用水溶性硫氰酸盐提高地毯纤维耐污染性的方法和组合物
公开(公告)号：US5152803A
公开(公告)日：1992-10-06
申请号：US671624
申请日：1991-03-19
申请人： Dale A. Hangey , Paul W. Harris , Daniel J. Corcoran, Jr. , Michael P. Friedberger , Charles J. Cole , William A. Archie , Roger N. Spitz
发明人： Dale A. Hangey , Paul W. Harris , Daniel J. Corcoran, Jr. , Michael P. Friedberger , Charles J. Cole , William A. Archie , Roger N. Spitz
IPC分类号： D06M15/277 , D06M15/41
CPC分类号： D06M15/412 , D06M15/277 , D06M2101/12 , D06M2101/34 , Y10S8/924 , Y10S8/929
摘要： This invention relates to improved methods and compositions to enhance stain resistance of carpet fiber. The improved methods relate to a continuous aftertreatment for dyed carpet fabric and to two-step processes, either batch-batch, batch-continuous or continuous-continuous. The improved compositions are used in the processes to enhance stain resistance of carpet or carpet fiber and to overcome various prior drawbacks, such as, yellowing, oxidation and durability to cleaning. The sulfonated aromatic condensates are used to enhance stain resistance, and can be combined with fluorocarbon compounds for soil resistance, thiocyanates, and/or salts having divalent cations, such as magnesium sulfate. Also various dispersing agents, buffering acids and sequestering agents are disclosed.
摘要翻译：本发明涉及改善地毯纤维耐污染性的方法和组合物。改进的方法涉及染色地毯织物的连续后处理和批次间歇，间歇连续或连续连续的两步法。改进的组合物用于增强地毯或地毯纤维的抗污性和克服各种先前缺点的方法，例如变黄，氧化和对清洁的耐久性。磺化芳族缩合物用于增强耐污染性，并且可以与用于土壤抗性的碳氟化合物，硫氰酸盐和/或具有二价阳离子的盐如硫酸镁组合。还公开了各种分散剂，缓冲酸和螯合剂。

8. 发明授权

US5145487A Methods and compositions to enhance stain resistance of carpet fibers using sulfonated aromatic condensates 失效
标题翻译：使用磺化芳族缩合物增强地毯纤维耐污染性的方法和组合物
公开(公告)号：US5145487A
公开(公告)日：1992-09-08
申请号：US818475
申请日：1992-01-06
申请人： Dale A. Hangey , Paul W. Harris , Charles J. Cole , Daniel J. Corcoran, Jr.
发明人： Dale A. Hangey , Paul W. Harris , Charles J. Cole , Daniel J. Corcoran, Jr.
IPC分类号： D06M15/277 , D06M15/41
CPC分类号： D06M15/412 , D06M15/277 , D06M2101/12 , D06M2101/34 , Y10S8/924 , Y10S8/929
摘要： This invention relates to improved methods and compositions to enhance stain resistance of carpet fiber. The improved methods relate to a continuous aftertreatment for dyed carpet fabric and to two-step processes, either batch-batch, batch-continuous or continuous-continuous. The improved compositions are used in the processes to enhance stain resistance of carpet or carpet fiber and to overcome various prior drawbacks, such as, yellowing, oxidation and durability to cleaning. The sulfonated aromatic condensates are used to enhance stain resistance, and can be combined with fluorocarbon compounds for soil resistance, thiocyanates, and/or salts having divalent cations, such as magnesium sulfate. Also various dispersing agents, buffering acids and sequestering agents are disclosed.
摘要翻译：本发明涉及改善地毯纤维耐污染性的方法和组合物。改进的方法涉及染色地毯织物的连续后处理和批次间歇，间歇连续或连续连续的两步法。改进的组合物用于增强地毯或地毯纤维的抗污性和克服各种先前缺点的方法，例如变黄，氧化和对清洁的耐久性。磺化芳族缩合物用于增强耐污染性，并且可以与用于土壤抗性的碳氟化合物，硫氰酸盐和/或具有二价阳离子的盐如硫酸镁组合。还公开了各种分散剂，缓冲酸和螯合剂。

9. 发明授权

US5131909A Molecular size of hydrodynamic volume of sulfonated aromatic condensates used to impart stain resistance to polyamide carpets 失效
标题翻译：用于抵抗多胺地毯的磺化芳族聚合物的水力动力学分子尺寸
公开(公告)号：US5131909A
公开(公告)日：1992-07-21
申请号：US524601
申请日：1990-05-17
申请人： Dale A. Hangey
发明人： Dale A. Hangey
IPC分类号： D06M13/02 , D06M13/248 , D06M13/256 , D06M15/41 , D06M101/00 , D06M101/16 , D06M101/30 , D06M101/34 , D06M101/36
CPC分类号： D06M15/412 , Y10S8/929 , Y10T428/23979 , Y10T428/23993
摘要： In a continuous application process with post-steaming, SAC's having molecular size (hydrodynamic volume) defined by elution volume (Ve) determined by Size Exclusion Chromatography (SEC) of between 6.3 and 6.5 ml. using the procedure described, are such that they are not too small so that migration into the fiber occurs (reduces ring dyeing effect) nor are they too large such that they require extremely long steaming times or the use of swelling agents to be effective. This is independent of the degree of sulfonation of the SAC.
摘要翻译：在具有后蒸汽的连续应用方法中，SAC具有由尺寸排阻色谱（SEC）确定的洗脱体积（Ve）定义为6.3至6.5ml的分子尺寸（流体动力学体积）。使用所述的方法使得它们不太小，使得发生纤维的迁移（降低环染色效果）也不太大，使得它们需要非常长的蒸煮时间或使用溶胀剂有效。这与SAC的磺化程度无关。

10. 发明授权

US5110317A Methods and compositions to enhance stain resistance of dyed nylon carpet fibers: thiocyanate to reduce yellowing 失效
标题翻译：提高染色尼龙地毯纤维耐污染性的方法和组合：硫氰酸盐减少黄化
公开(公告)号：US5110317A
公开(公告)日：1992-05-05
申请号：US709041
申请日：1991-06-03
申请人： Dale A. Hangey , Michael P. Friedberger , William A. Archie , Roger N. Spitz
发明人： Dale A. Hangey , Michael P. Friedberger , William A. Archie , Roger N. Spitz
IPC分类号： D06M15/277 , D06M15/41
CPC分类号： D06M15/412 , D06M15/277 , D06M2101/12 , D06M2101/34 , Y10S8/924 , Y10S8/929 , Y10T428/23979 , Y10T428/23986 , Y10T428/23993 , Y10T428/2969
摘要： This invention relates to improved methods and compositions to enhance stain resistance of carpet fiber. The improved methods relate to a continuous aftertreatment for dyed carpet fabric and to two-step processes, either batch-batch, batch-continuous or continuous-continuous. The improved compositions are used in the processes to enhance stain resistance of carpet or carpet fiber and to overcome various prior drawbacks, such as, yellowing, oxidation and durability to cleaning. The sulfonated aromatic condensates are used to enhance stain resistance, and can be combined with fluorocarbon compounds for soil resistance, thiocyanates, and/or salts having divalent cations, such as magnesium sulfate. Also various dispersing agents, buffering acids and sequestering agents are disclosed.
摘要翻译：本发明涉及改善地毯纤维耐污染性的方法和组合物。改进的方法涉及染色地毯织物的连续后处理和批次间歇，间歇连续或连续连续的两步法。改进的组合物用于增强地毯或地毯纤维的抗污性和克服各种先前缺点的方法，例如变黄，氧化和对清洁的耐久性。磺化芳族缩合物用于增强耐污染性，并且可以与用于土壤抗性的碳氟化合物，硫氰酸盐和/或具有二价阳离子的盐如硫酸镁组合。还公开了各种分散剂，缓冲酸和螯合剂。

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