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1. 发明授权

US4902813A Process for preparing diorganopolysiloxanes having terminal Si-bonded hydroxyl groups 失效
标题翻译：制备具有末端Si键合的羟基的二有机聚硅氧烷的方法
公开(公告)号：US4902813A
公开(公告)日：1990-02-20
申请号：US280852
申请日：1988-12-07
申请人： Karl-Heinrich Wegehaupt , Karl Braunsperger , Gunter von Au , Fridolin Stary
发明人： Karl-Heinrich Wegehaupt , Karl Braunsperger , Gunter von Au , Fridolin Stary
IPC分类号： C08G77/08 , C08G77/16 , C08G77/22 , C08G77/32 , C08G77/34 , C08G77/36
CPC分类号： C08G77/16 , C08G77/34
摘要： A process for preparing diorganopolysiloxanes having terminal Si-bonded hydroxyl groups which comprises reacting an organosilicon compound selected from a cyclic diorganopolysiloxane, a diorganodichlorosilane hydrolysis product and mixtures thereof with from 0.1 to 3 percent by weight of a diorganodichlorosilane, based on the weight of the organosilicon compound, i.e., the cyclic diorganopolysiloxane and/or diorganodichlorosilane hydrolysis product employed, in the presence of from 1 to 50 ppm by weight of phosphonitrile chloride, based on the total weight of the organosilicon compound and diorganodichlorosilane employed, to form diorganopolysiloxanes containing an Si-bonded chlorine atom in each of the terminal units, then treating the reaction mixture with water or an aqueous solution, separating off the aqueous phase from the diorganopolysiloxanes containing an Si-bonded hydroxyl group in each of the terminal units and thereafter removing the low boiling constituents by distillation.
摘要翻译：一种制备具有末端Si键合的羟基的二有机聚硅氧烷的方法，其包括将选自环状二有机基聚硅氧烷，二有机二氯硅烷水解产物及其混合物的有机硅化合物与0.1至3重量％的二有机二氯硅烷基于有机硅的重量化合物，即所用的环状二有机基聚硅氧烷和/或二有机二氯硅烷水解产物，基于所用的有机硅化合物和二有机二氯硅烷的总重量，在1-50ppm重量的磷腈氯化物的存在下，形成含有Si- 在每个末端单元中连接氯原子，然后用水或水溶液处理反应混合物，从每个末端单元中含有与Si键合的羟基的二有机聚硅氧烷分离水相，然后除去低沸点组分通过蒸馏。

2. 发明授权

US07671125B2 Process for the continuous preparation of high-viscosity silicone compositions 有权
标题翻译：连续制备高粘度硅酮组合物的方法
公开(公告)号：US07671125B2
公开(公告)日：2010-03-02
申请号：US10802455
申请日：2004-03-17
申请人： Manfred Heisler , Johann Schuster , Alois Schlierf , Fridolin Stary
发明人： Manfred Heisler , Johann Schuster , Alois Schlierf , Fridolin Stary
IPC分类号： B29B7/48
CPC分类号： B29C47/76 , B01F7/00291 , B01F7/00416 , B01F7/00975 , B01F13/1027 , B29B7/423 , B29B7/7461 , B29B7/7495 , B29C47/0009 , B29C47/38 , B29C47/44 , B29C47/667 , B29K2083/00
摘要： A process for preparing organopolysiloxane compositions (A) having a viscosity measured at 25° C. of at least 500 Pa·s., wherein organopolysiloxanes (O) and fillers (F) are mixed and kneaded in a first process stage in a kneading cascade having at least two kneading chambers arranged in series adjacent one another, each containing kneading tools having parallel axes and capable of being driven in co-rotating or counter-rotating directions, the chambers connected to one another by means of openings through which material can pass in a direction transverse to the axes of the kneading tools, with the first kneading chamber having a feed opening and the last kneading chamber having a discharge opening, to give raw mixtures, and the raw mixtures are kneaded and degassed in a reciprocating kneader in a second process stage.
摘要翻译：一种制备在25℃下测得的粘度为至少500Pa·s的有机聚硅氧烷组合物（A）的方法，其中有机聚硅氧烷（O）和填料（F）在捏合级联中在第一工艺阶段中混合和捏合具有彼此相邻排列的至少两个捏合室，每个捏合室包含具有平行轴线并能够以同向旋转或反向旋转方向驱动的捏合工具，所述室通过材料可以通过的开口彼此连接在与捏合工具的轴线横向的方向上，第一捏合室具有进料口，最后的捏合室具有排出口，得到原料混合物，并将原料混合物在往复式捏合机中捏合并脱气第二个过程阶段

3. 发明授权

US6124392A Process for the continuous preparation of HTV silicone compositions 失效
标题翻译：连续制备HTV硅酮组合物的方法
公开(公告)号：US6124392A
公开(公告)日：2000-09-26
申请号：US74819
申请日：1993-06-10
申请人： Manfred Heisler , Fridolin Stary , Rudolf Ratka , Alois Schlierf
发明人： Manfred Heisler , Fridolin Stary , Rudolf Ratka , Alois Schlierf
IPC分类号： B29B7/42 , B29K83/00 , C08J3/20 , C08K3/36 , C08L83/04 , C08K3/34
CPC分类号： C08J3/20 , B29C47/366 , B29C47/369 , B29C47/92 , C08J2383/04
摘要： The invention relates to a process for the continuous preparation of HTV silicone compositions, which comprises mixing and homogenizing 100 parts by weight of diorgano(poly)siloxane which has a viscosity of 50 to 100,000 Pas at 25.degree. C. with at least 20 parts by weight of finely divided silicon dioxide which has a tamped density of more than 0.01 kg/l in an oscillating single-shaft pilgrim-step kneader.
摘要翻译： PCT No.PCT / EP92 / 00080 Sec。 371日期：1993年6月10日 102（e）日期1993年6月10日PCT提交1992年1月16日PCT公布。公开号WO92 / 13694 日期：1992年8月20日本发明涉及连续制备HTV有机硅组合物的方法，该方法包括将100重量份在25℃下粘度为50-100,000Pa·s的二有机（聚）硅氧烷混合均化，至少20重量份的细碎二氧化硅，其在振荡的单轴朝圣阶梯式捏合机中具有大于0.01kg / l的夯实密度。

4. 发明授权

US4737561A Process for the continuous production of room temperature-vulcanizable silicone compositions 失效
标题翻译：连续生产室温可硫化硅酮组合物的方法
公开(公告)号：US4737561A
公开(公告)日：1988-04-12
申请号：US948193
申请日：1986-12-31
申请人： Fridolin Stary , Peter Kremer
发明人： Fridolin Stary , Peter Kremer
IPC分类号： C08J3/24 , B29B7/74 , C08J3/20 , C08L83/04 , C08G77/06
CPC分类号： C08J3/20 , B29B7/7461 , C08L83/04 , B29K2083/00 , C08G77/06 , C08J2383/04 , Y10S528/901
摘要： A process for producing room temperature-vulcanizable silicone compositions which comprises mixing, in a first step, crosslinkable diorgano(poly)siloxanes, filler(s) and either catalyst(s) or crosslinking agent(s) and a part or all of the optional additives to be used in a continuusly operating closed mixer, and in a second step, metering the crosslinking agents and/or catalyst(s) not added in the first step and the remainder of the optional additivies to be used into the mixture thus obtained in an oscillating pilgrim-step kneader where the mixture is homogenized and degassed.
摘要翻译：一种制备室温可硫化硅氧烷组合物的方法，其包括在第一步中混合可交联的二有机（聚）硅氧烷，填料和催化剂或交联剂和一部分或全部可任选的在连续操作的密闭混合器中使用的添加剂，在第二步中，计量在第一步中未加入的交联剂和/或催化剂，并将剩余的任选添加剂用于如此获得的混合物中振荡的朝圣者捏合机，将混合物匀化并脱气。

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