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1. 发明授权

US4315079A Process of making an isocyanurate foam 失效
标题翻译：制备异氰脲酸酯泡沫的方法
公开(公告)号：US4315079A
公开(公告)日：1982-02-09
申请号：US249800
申请日：1981-04-01
申请人： Heinz Schulze , Robert L. Zimmerman , Harold G. Waddill
发明人： Heinz Schulze , Robert L. Zimmerman , Harold G. Waddill
IPC分类号： C08G18/22 , C08G65/332 , C08L63/00 , C08J9/00
CPC分类号： C08G65/332 , C08G18/225 , C08L63/00 , C08G2105/02 , Y10S521/902
摘要： Compounds typified by N,N'-polyoxyalkylene bis(pyrrolidinone-3-carboxylic acid) are useful as epoxy curing accelerators. Salts thereof, including alkali metal salts, are curing agents for isocyanurate foams.
摘要翻译：以N，N'-聚氧化烯双（吡咯烷酮-3-羧酸）为代表的化合物可用作环氧固化促进剂。其盐，包括碱金属盐，是用于异氰脲酸酯泡沫的固化剂。

2. 发明授权

US4332720A N,N'-Polyoxyalkylene bis(lactam carboxylic acids) 失效
标题翻译： N，N'-聚氧化烯双（内酰胺羧酸）
公开(公告)号：US4332720A
公开(公告)日：1982-06-01
申请号：US847642
申请日：1977-11-01
申请人： Heinz Schulze , Robert L. Zimmerman , Harold G. Waddill
发明人： Heinz Schulze , Robert L. Zimmerman , Harold G. Waddill
IPC分类号： C08G18/22 , C08G65/332 , C08L63/00 , C07D207/277 , C07D211/78 , C07D223/10 , C07D227/087
CPC分类号： C08G65/332 , C08G18/225 , C08L63/00 , C08G2105/02
摘要： Compounds typified by N,N'-polyoxyalkylene bis (pyrrolidinone-3-carboxylic acid) are useful as epoxy curing accelerators. Salts thereof, including alkali metal salts, are curing agents for isocyanurate foams.
摘要翻译：以N，N'-聚氧化烯双（吡咯烷酮-3-羧酸）为代表的化合物可用作环氧固化促进剂。其盐，包括碱金属盐，是用于异氰脲酸酯泡沫的固化剂。

3. 发明授权

US4326050A Process and product 失效
标题翻译：工艺和产品
公开(公告)号：US4326050A
公开(公告)日：1982-04-20
申请号：US249799
申请日：1981-04-01
申请人： Heinz Schulze , Robert L. Zimmerman , Harold G. Waddill
发明人： Heinz Schulze , Robert L. Zimmerman , Harold G. Waddill
IPC分类号： C08G18/22 , C08G65/332 , C08L63/00 , C08G59/52 , C08G59/58
CPC分类号： C08G65/332 , C08G18/225 , C08L63/00 , C08G2105/02
摘要： Compounds typified by N,N'-polyoxyalkylene bis (pyrrolidinone-3-carboxylic acid) are useful as epoxy curing accelerators. Salts thereof, including alkali metal salts, are curing agents for isocyanurate foams.
摘要翻译：以N，N'-聚氧化烯双（吡咯烷酮-3-羧酸）为代表的化合物可用作环氧固化促进剂。其盐，包括碱金属盐，是用于异氰脲酸酯泡沫的固化剂。

4. 发明授权

US4304889A Solvent resistant epoxy coatings 失效
标题翻译：耐溶剂环氧涂料
公开(公告)号：US4304889A
公开(公告)日：1981-12-08
申请号：US167512
申请日：1980-07-11
申请人： Harold G. Waddill , Heinz Schulze
发明人： Harold G. Waddill , Heinz Schulze
IPC分类号： C08G59/00 , C08G59/56 , C08L63/00 , C09D163/00 , C08G59/58
CPC分类号： C08G59/56 , C08L63/00
摘要： A solvent resistant epoxy resin composition comprises a vicinal polyepoxide, an aromatic polyamine and a condensation product of a polyoxyalkylenediamine of about 400 molecular weight or below with at least two moles of maleic anhydride.
摘要翻译：耐溶剂环氧树脂组合物包含邻位聚环氧化物，芳族多胺和约400分子量或更低分子量的聚氧化烯二胺与至少两摩尔马来酸酐的缩合产物。

5. 发明授权

US4178427A Polyether urea epoxy curing agent 失效
标题翻译：聚醚脲环氧固化剂
公开(公告)号：US4178427A
公开(公告)日：1979-12-11
申请号：US875473
申请日：1978-02-06
申请人： Harold G. Waddill , Heinz Schulze
发明人： Harold G. Waddill , Heinz Schulze
IPC分类号： C08G18/50 , C08G59/40 , C08G71/02 , C08G59/50
CPC分类号： C08G71/02 , C08G18/5021 , C08G59/4021 , Y10T428/31529
摘要： An improved curable epoxy resin composition of a vicinalpolyepoxide and an effective amount of a novel polyether urea curing agent is disclosed. The improved curable epoxy resins which are useful as coatings, castings, sealants, and adhesives show improved tensile shear strength, flexural strength, and ultimate elongation. The novel polyether urea curing agents of the instant invention are characterized by terminal primary amino groups and are formed by reaction of polyoxyalkylenepolyamines with urea, urea forming compounds, or bifunctional isocyanates.A preferred curing agent includes a mixture of a novel polyether urea formed by reaction of a polyoxypropylenepolyamine having a molecular weight of from about 200-2000 and an effective amount of urea; and another known epoxy resin curing agent such as polyoxyalkylenepolyamine in ratios of from about 5:1 to 1:5 by weight.
摘要翻译：公开了一种改进的邻位多环氧化物的可固化环氧树脂组合物和有效量的新型聚醚脲固化剂。可用作涂料，铸件，密封剂和粘合剂的改进的可固化环氧树脂显示出改进的拉伸剪切强度，弯曲强度和极限伸长率。本发明的新型聚醚脲固化剂的特征在于末端伯氨基，并通过聚氧亚烷基多胺与脲，脲形成化合物或双官能异氰酸酯反应形成。优选的固化剂包括通过分子量为约200-2000的聚氧丙烯聚胺与有效量的脲反应形成的新型聚醚脲的混合物; 和另一种已知的环氧树脂固化剂如聚氧亚烷基多胺，其重量比为约5:1至1:5。

6. 发明授权

US4115360A Polyether urea epoxy additives 失效
标题翻译：聚醚尿素环氧添加剂
公开(公告)号：US4115360A
公开(公告)日：1978-09-19
申请号：US743815
申请日：1976-11-22
申请人： Heinz Schulze , Harold G. Waddill
发明人： Heinz Schulze , Harold G. Waddill
IPC分类号： C08G59/00 , C08G59/50 , C08G59/56 , C08L63/00 , C08L63/02 , C09J163/00
CPC分类号： C08G59/56 , C08L63/00
摘要： The adhesion properties of amine-cured epoxy resins are unexpectedly enhanced by addition of certain amino terminated polyether ureylene additives. The adhesively superior epoxy resin composition comprises a vicinal polyepoxide, a curing amount of an amine curing agent, and an effective amount of a polyether ureylene having terminal amino groups and a molecular weight of from about 4000 to about 4500.
摘要翻译：胺固化的环氧树脂的粘合性能通过加入某些氨基封端的聚醚亚芳基添加剂而出人意料地增强。粘合性优异的环氧树脂组合物包含邻位聚环氧化物，固化量的胺固化剂和有效量的具有末端氨基并且分子量为约4000至约4500的聚醚亚芳基。

7. 发明授权

US4110313A Epoxy curing agent 失效
标题翻译：环氧固化剂
公开(公告)号：US4110313A
公开(公告)日：1978-08-29
申请号：US812558
申请日：1977-07-05
申请人： Heinz Schulze , Harold G. Waddill
发明人： Heinz Schulze , Harold G. Waddill
IPC分类号： C08G59/40 , C08G59/68 , C08L63/00 , C08G59/50 , C08G59/56
CPC分类号： C08G59/686 , C08G59/4057 , C08L63/00
摘要： Epoxy resins, particularly those of the polyglycidyl ether of a polyhydric phenol type, are cured by incorporating therein a polyoxyalkylenepolyamine usually with an accelerator such as a combination of piperazine and an alkanolamine. Rapidity of curing is further improved by substituting from about 50 wt% to 100 wt% of the dithiocarbamate salt of the polyoxyalkylenepolymine for the polyoxyalkylenepolyamine. The epoxy resin products are useful in protective coatings, adhesives, seamless and terrazzo flooring, castings, laminates, and in grouting, potting, encapsulating, caulking and sealing compositions.
摘要翻译：环氧树脂，特别是多元酚型聚缩水甘油醚的树脂通过在其中加入聚氧亚烷基多胺通常与加速剂如哌嗪和链烷醇胺的组合来固化。通过用约50wt％至100wt％的聚氧亚烷基多胺的二硫代氨基甲酸盐代替聚氧亚烷基多胺，进一步提高了固化的快速性。环氧树脂产品可用于保护涂料，粘合剂，无缝和水磨石地板，铸件，层压材料以及灌浆，灌封，封装，填缝和密封组合物中。

8. 发明授权

US4169177A Polyether diureide epoxy additives 失效
标题翻译：聚醚二脲环氧添加剂
公开(公告)号：US4169177A
公开(公告)日：1979-09-25
申请号：US891580
申请日：1978-03-30
申请人： Harold G. Waddill , Heinz Schulze
发明人： Harold G. Waddill , Heinz Schulze
IPC分类号： C08G59/42 , C08G71/02 , C08L63/00 , C08G59/48
CPC分类号： C08G71/02 , C08G59/4215 , C08L63/00
摘要： Resistance to thermal shock of certain anhydride cured epoxy resins is unexpectedly enhanced by addition of a diamide of a polyoxyalkylenepolyamine-urea condensate. This superior resistance does not appreciably compromise heat deflection properties. The resins comprise a vicinal polyepoxide, a curing amount of a certain bicyclic anhydride and an effective amount of a diamide of a polyoxyalkylenepolyamine-urea condensate having a molecular weight of from about 4000 to 4500.
摘要翻译：通过加入聚氧亚烷基多胺 - 脲缩合物的二酰胺，某些酸酐固化环氧树脂的耐热冲击性出人意料地得到提高。这种优异的阻力不会明显损害热偏转性能。树脂包括邻位聚环氧化物，固化量的某些双环酸酐和有效量的分子量为约4000至4500的聚氧亚烷基多胺 - 脲缩合物的二酰胺。

9. 发明授权

US4146701A Polyether diureide epoxy additives 失效
标题翻译：聚醚二环氧化物添加剂
公开(公告)号：US4146701A
公开(公告)日：1979-03-27
申请号：US890743
申请日：1978-03-27
申请人： Harold G. Waddill , Heinz Schulze
发明人： Harold G. Waddill , Heinz Schulze
IPC分类号： C08G59/40 , C08G59/42 , C08G59/44 , C08G59/48
CPC分类号： C08G59/44 , C08G59/4021 , C08G59/4284
摘要： An epoxy resin having superior resistance to thermal shock comprises a vicinal polyepoxide, a curing amount of a certain bicyclic anhydride and an effective amount of an additive comprising a polyoxyalkylenepolyamine-maleic anhydride condensation product having thioureide, ureide or thioformamide or formamide end groups.

10. 发明授权

US4113697A Polyether diamide epoxy additives 失效
标题翻译：聚醚二酰胺环氧添加剂
公开(公告)号：US4113697A
公开(公告)日：1978-09-12
申请号：US743818
申请日：1976-11-22
申请人： Heinz Schulze , Harold G. Waddill
发明人： Heinz Schulze , Harold G. Waddill
IPC分类号： C08G59/42 , C08L63/02 , C08G59/46
CPC分类号： C08G59/4215 , C08L63/00
摘要： Resistance to thermal shock of certain anhydride cured epoxy resins is unexpectedly enhanced by addition of certain polyether diamide additives. This superior resistance does not appreciably compromise heat deflection properties. The resins comprise a vicinal polyepoxide, a curing amount of certain bicyclic anhydride and an effective amount of a polyether diamide having terminal amido groups and a molecular weight of from about 2000 to about 3000.
摘要翻译：通过加入某些聚醚二酰胺添加剂，某些酸酐固化环氧树脂的耐热冲击性出人意料地得到提高。这种优异的阻力不会明显损害热偏转性能。树脂包括邻位聚环氧化物，固化量的某些双环酸酐和有效量的具有末端酰氨基并且分子量为约2000至约3000的聚醚二酰胺。

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