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1. 发明授权

US4287074A Sec-ylbiphenyl composition and process for preparing the same 失效
标题翻译：二联联组合物及其制备方法
公开(公告)号：US4287074A
公开(公告)日：1981-09-01
申请号：US144490
申请日：1980-04-28
申请人： Harold W. Earhart , Donald F. Rugen
发明人： Harold W. Earhart , Donald F. Rugen
IPC分类号： B01F1/00 , B01J27/10 , B41M5/165 , C07C1/00 , C07C2/68 , C07C15/14 , C07C67/00 , H01B3/22 , H01G4/22
CPC分类号： H01B3/22 , B41M5/1655 , C07C2/68 , C07C2527/126
摘要： A water-white, essentially odorless liquid useful as a dieletric oil and as a dye solvent, particularly for a carbonless paper solvent, consisting essentially of about 82% to about 88% by weight of mono-sec-butylbiphenyl and about 12% to about 18% of di-sec-butylbiphenyl prepared by reacting highly pure 1-butene or 2-butene with biphenyl at a mol ratio of butene to biphenyl of from about 0.5 to about 0.9 and at a temperature of about 250.degree. F. to about 475.degree. F. in the presence of an aluminum chloride catalyst, distilling the reaction product under vacuum to remove unreacted biphenyl and distilling off the product mixture at a temperature between about 370.degree. F. and about 440.degree. F. at 30 mm Hg. pressure or the equivalent thereof.
摘要翻译：一种水白色，基本上无臭的液体，可用作消耗油和染料溶剂，特别是无碳纸溶剂，基本上由约82％至约88％重量的单仲丁基联苯和约12％至约 18％的二仲丁基联苯通过使高纯度1-丁烯或2-丁烯与联苯以丁烯与联苯的摩尔比为约0.5至约0.9，温度为约250°F至约475 在氟化铝催化剂的存在下，在真空下蒸馏反应产物以除去未反应的联苯，并在30mmHg的温度在约370°F至约440°F之间蒸馏产物混合物。压力或其等同物。

2. 发明授权

US5489332A Carbonless paper solvent comprising diisopropylmethylnaphthalene and products utilizing same 失效
标题翻译：含有二异丙基甲基萘的无碳纸溶剂和利用其的产物
公开(公告)号：US5489332A
公开(公告)日：1996-02-06
申请号：US333056
申请日：1994-11-01
申请人： Harold W. Earhart , Andrew P. Komin , Dustin K. James
发明人： Harold W. Earhart , Andrew P. Komin , Dustin K. James
IPC分类号： B41M5/165 , C07C2/70 , C08K5/01
CPC分类号： B41M5/1655 , C07C2/70 , C07C2527/11 , C07C2527/126
摘要： A carbonless paper solvent is provided comprising diisopropylmethylnaphthalene, generally in an amount of from 20% to 100% of the total weight of the solvent. The solvent is combined with a chromogenic substance and is encapsuled into microcapsules. The microcapsules are applied to a sheet of material and a color developing substance is then applied to another sheet to form a carbonless marking system. When the microcapsules are ruptured, the solubilized chromogenic substance contacts and reacts with the developer to form an image. In a method of the invention, a by-product fraction consisting of components with a boiling point range of 200.degree. to 400.degree. C. are contacted with propylene under conditions sufficient to form an alkylation product comprising diisopropylmethylnaphthalene.
摘要翻译：提供了包含二异丙基甲基萘的无碳纸溶剂，其通常为溶剂总重量的20％至100％。将溶剂与显色物质结合，并将其包封成微胶囊。将微胶囊施加到一片材料上，然后将彩色显影物质施加到另一片材上以形成无碳标记系统。当微胶囊破裂时，溶解的显色物质与显影剂接触并反应形成图像。在本发明的方法中，由足以形成包含二异丙基甲基萘的烷基化产物的条件，使丙烯的沸点范围为200-400℃的副产物馏分与丙烯接触。

3. 发明授权

US5385879A Carbonless paper solvent comprising diisopropylmethylnaphthalene and products utilizing same 失效
标题翻译：含有二异丙基甲基萘的无碳纸溶剂和利用其的产物
公开(公告)号：US5385879A
公开(公告)日：1995-01-31
申请号：US966295
申请日：1992-10-26
申请人： Harold W. Earhart , Andrew P. Komin , Dustin K. James
发明人： Harold W. Earhart , Andrew P. Komin , Dustin K. James
IPC分类号： B41M5/165 , C07C2/70
CPC分类号： B41M5/1655 , C07C2/70 , C07C2527/11 , C07C2527/126
摘要： A carbonless paper solvent is provided comprising diisopropylmethylnaphthalene, generally in an amount of from 20% to 100% of the total weight of the solvent. The solvent is combined with a chromogenic substance and is encapsuled into microcapsules. The microcapsules are applied to a sheet of material and a color developing substance is then applied to another sheet to form a carbonless marking system. When the microcapsules are ruptured, the solubilized chromogenic substance contacts and reacts with the developer to form an image. In a method of the invention, a byproduct fraction consisting of components with a boiling point range of 200.degree. to 400.degree. C. are contacted with propylene under conditions sufficient to form an alkylation product comprising diisopropylmethylnaphthalene.
摘要翻译：提供了包含二异丙基甲基萘的无碳纸溶剂，其通常为溶剂总重量的20％至100％。将溶剂与显色物质结合，并将其包封成微胶囊。将微胶囊施加到一片材料上，然后将彩色显影物质施加到另一片材上以形成无碳标记系统。当微胶囊破裂时，溶解的显色物质与显影剂接触并反应形成图像。在本发明的方法中，由沸点范围为200-400℃的组分组成的副产物馏分在足以形成包含二异丙基甲基萘的烷基化产物的条件下与丙烯接触。

4. 发明授权

US5696184A Lower alkyl biphenyls as plasticizers 失效
标题翻译：低级烷基联苯作为增塑剂
公开(公告)号：US5696184A
公开(公告)日：1997-12-09
申请号：US564706
申请日：1995-11-29
申请人： Jack B. Tatman , Gregory R. Hahn , Harold W. Earhart
发明人： Jack B. Tatman , Gregory R. Hahn , Harold W. Earhart
IPC分类号： C08F136/06 , C08K5/01 , C08L63/00
CPC分类号： C08K5/01 , C08F136/06
摘要： A significantly improved plasticizer-polymer composition embraces a polymer containing a di-, tri- and/or tetra- ethyl-, propyl- and/or butylbiphenyl plasticizer which constitutes the major proportion by weight of any other plasticizing/softening additive, provided that the polymer is not polyvinyl chloride and when the polymer is an elastomer or rubber, or is a polystyrene, said plasticizer is diisopropylbiphenyl and/or triisopropylbiphenyl, and when the polymer is of a plastisol, essentially no ester plasticizing additive is present. As well, a polymer fabrication composition comprises a monomer and/or oligomer component in combination with said plasticizer. A method for preparing the plasticizer-polymer composition and/or the fabrication composition comprises contacting the monomer and/or oligomer component with said plasticizer, mixing to provide a uniform mixture, and carrying out further processing as may be desired so as to optionally prepare the plasticized-polymer composition. For instance, thermosets such as epoxies and polyurethanes and elastomers such as polybutadienes and other polymers can have high loading levels of the plasticizer employed without sacrifice of plasticized polymer properties. Moreover, the high loading capacity in many cases can represent a significant increase over that found from prior art plasticizing/softening additives.
摘要翻译：显着改进的增塑剂 - 聚合物组合物包含含有二 - ，三 - 和/或四 - 乙基 - ，丙基 - 和/或丁基联苯增塑剂的聚合物，其构成任何其它增塑/软化添加剂的主要重量比，条件是聚合物不是聚氯乙烯，并且当聚合物是弹性体或橡胶或者是聚苯乙烯时，所述增塑剂是二异丙基联苯和/或三异丙基联苯，并且当聚合物是增塑溶胶时，基本上不存在酯增塑添加剂。同样，聚合物制造组合物包含与所述增塑剂组合的单体和/或低聚物组分。制备增塑剂 - 聚合物组合物和/或制造组合物的方法包括使单体和/或低聚物组分与所述增塑剂接触，混合以提供均匀的混合物，并根据需要进行进一步的处理，以便任选地制备增塑聚合物组合物。例如，诸如环氧树脂和聚氨酯的热固性材料和诸如聚丁二烯和其它聚合物的弹性体可以在不牺牲增塑聚合物性能的情况下使用增塑剂的高负载水平。此外，与现有技术的增塑/软化添加剂相比，许多情况下的高负载能力可以显着增加。

5. 发明授权

US5318940A Carbonless paper solvent comprising diisopropylbiphenyl and triisopropylbiphenyl and products utilizing same 失效
标题翻译：含有二异丙基联苯和三异丙基联苯的无碳纸溶剂和使用它们的产物
公开(公告)号：US5318940A
公开(公告)日：1994-06-07
申请号：US984992
申请日：1992-12-02
申请人： Harold W. Earhart , Gregory R. Hahn , Ronald W. Osman
发明人： Harold W. Earhart , Gregory R. Hahn , Ronald W. Osman
IPC分类号： B41M5/165 , C07C15/14
CPC分类号： B41M5/1655 , C07C15/14 , Y10T428/2984
摘要： A remarkably low odor carbonless paper solvent is provided comprising a mixture of diisopropylbiphenyl and triisopropylbiphenyl, generally in an amount of 50 to 90% by weight diisopropylbiphenyl and 10 to 40% by weight triisopropylbiphenyl. The solvent and a chromogenic substance such as a leuco dye are encapsulated to form microcapsules which are coated onto one surface of a carrier sheet. A color developing substance is then applied to another sheet to form a carbonless marking system. When the microcapsules are ruptured, the solubilized chromogenic substance contacts and reacts with the developer to form an image.
摘要翻译：提供了非常低气味的无碳纸溶剂，其包含二异丙基联苯和三异丙基联苯的混合物，通常为50至90重量％的二异丙基联苯和10至40重量％的三异丙基联苯。将溶剂和显色物质如无色染料包封以形成涂覆在载体片材的一个表面上的微胶囊。然后将彩色显影物质施加到另一片材上以形成无碳标记系统。当微胶囊破裂时，溶解的显色物质与显影剂接触并反应形成图像。

6. 发明授权

US5847040A Lower alkyl biphenyls as plasticizers for polyurethane 失效
标题翻译：低级烷基联苯作为聚氨酯的增塑剂
公开(公告)号：US5847040A
公开(公告)日：1998-12-08
申请号：US898632
申请日：1997-07-22
申请人： Jack B. Tatman , Gregory R. Hahn , Harold W. Earhart
发明人： Jack B. Tatman , Gregory R. Hahn , Harold W. Earhart
IPC分类号： C08F136/06 , C08K5/01
CPC分类号： C08K5/01 , C08F136/06
摘要： A significantly improved plasticizer-polymer composition embraces a polymer containing a di-, tri- and/or tetra-ethyl-, propyl- and/or butylbiphenyl plasticizer which constitutes the major proportion by weight of any other plasticizing/softening additive, provided that the polymer is not polyvinyl chloride and when the polymer is an elastomer or rubber, or is a polystyrene, said plasticizer is diisopropylbiphenyl and/or triisopropylbiphenyl, and when the polymer is of a plastisol, essentially no ester plasticizing additive is present. As well, a polymer fabrication composition comprises a monomer and/or oligomer component in combination with said plasticizer. A method for preparing the plasticizer-polymer composition and/or the fabrication composition comprises contacting the monomer and/or oligomer component with said plasticizer, mixing to provide a uniform mixture, and carrying out further processing as may be desired so as to optionally prepare the plasticized-polymer composition. For instance, thermosets such as epoxies and polyurethanes and elastomers such as polybutadienes and other polymers can have high loading levels of the plasticizer employed without sacrifice of plasticized polymer properties. Moreover, the high loading capacity in many cases can represent a significant increase over that found from prior art plasticizing/softening additives.
摘要翻译：显着改进的增塑剂 - 聚合物组合物包括含有二 - ，三 - 和/或四乙基 - 丙基 - 和/或丁基联苯增塑剂的聚合物，其构成任何其它增塑/软化添加剂的主要重量比，条件是聚合物不是聚氯乙烯，并且当聚合物是弹性体或橡胶或者是聚苯乙烯时，所述增塑剂是二异丙基联苯和/或三异丙基联苯，并且当聚合物是增塑溶胶时，基本上不存在酯增塑添加剂。同样，聚合物制造组合物包含与所述增塑剂组合的单体和/或低聚物组分。制备增塑剂 - 聚合物组合物和/或制造组合物的方法包括使单体和/或低聚物组分与所述增塑剂接触，混合以提供均匀的混合物，并根据需要进行进一步的处理，以便任选地制备增塑聚合物组合物。例如，诸如环氧树脂和聚氨酯的热固性材料和诸如聚丁二烯和其它聚合物的弹性体可以在不牺牲增塑聚合物性能的情况下使用增塑剂的高负载水平。此外，与现有技术的增塑/软化添加剂相比，许多情况下的高负载能力可以显着增加。

7. 发明授权

US5489646A Lower alkyl biphenyls as plasticizers 失效
标题翻译：低级烷基联苯作为增塑剂
公开(公告)号：US5489646A
公开(公告)日：1996-02-06
申请号：US179424
申请日：1994-01-10
申请人： Jack B. Tatman , Gregory R. Hahn , Harold W. Earhart
发明人： Jack B. Tatman , Gregory R. Hahn , Harold W. Earhart
IPC分类号： C08F136/06 , C08K5/01
CPC分类号： C08K5/01 , C08F136/06
摘要： A significantly improved plasticizer-polymer composition embraces a polymer containing a di-, tri- and/or tetra- ethyl-, propyl- and/or butylbiphenyl plasticizer which constitutes the major proportion by weight of any other plasticizing/softening additive, provided that the polymer is not polyvinyl chloride and when the polymer is an elastomer or rubber, or is a polystyrene, said plasticizer is diisopropylbiphenyl and/or triisopropylbiphenyl, and when the polymer is of a plastisol, essentially no ester plasticizing additive is present. As well, a polymer fabrication composition comprises a monomer and/or oligomer component in combination with said plasticizer. A method for preparing the plasticizer-polymer composition and/or the fabrication composition comprises contacting the monomer and/or oligomer component with said plasticizer, mixing to provide a uniform mixture, and carrying out further processing as may be desired so as to optionally prepare the plasticized-polymer composition. For instance, thermosets such as epoxies and polyurethanes and elastomers such as polybutadienes and other polymers can have high loading levels of the plasticizer employed without sacrifice of plasticized polymer properties. Moreover, the high loading capacity in many cases can represent a significant increase over that found from prior art plasticizing/softening additives.
摘要翻译：显着改进的增塑剂 - 聚合物组合物包含含有二 - ，三 - 和/或四 - 乙基 - ，丙基 - 和/或丁基联苯增塑剂的聚合物，其构成任何其它增塑/软化添加剂的主要重量比，条件是聚合物不是聚氯乙烯，并且当聚合物是弹性体或橡胶或者是聚苯乙烯时，所述增塑剂是二异丙基联苯和/或三异丙基联苯，并且当聚合物是增塑溶胶时，基本上不存在酯增塑添加剂。同样，聚合物制造组合物包含与所述增塑剂组合的单体和/或低聚物组分。制备增塑剂 - 聚合物组合物和/或制造组合物的方法包括使单体和/或低聚物组分与所述增塑剂接触，混合以提供均匀的混合物，并根据需要进行进一步的处理，以便任选地制备增塑聚合物组合物。例如，诸如环氧树脂和聚氨酯的热固性材料和诸如聚丁二烯和其它聚合物的弹性体可以在不牺牲增塑聚合物性能的情况下使用增塑剂的高负载水平。此外，与现有技术的增塑/软化添加剂相比，许多情况下的高负载能力可以显着增加。

8. 发明授权

US5458974A Microencapsulated composition containing solvent including triisopropyylbiphenyl 失效
标题翻译：包含三异丙基联苯的溶剂的微胶囊化组合物
公开(公告)号：US5458974A
公开(公告)日：1995-10-17
申请号：US202946
申请日：1994-02-28
申请人： Harold W. Earhart , Gregory R. Hahn , Ronald W. Osman
发明人： Harold W. Earhart , Gregory R. Hahn , Ronald W. Osman
IPC分类号： B41M5/165 , C07C15/14 , B01J13/10 , B01J13/20 , C09D11/00
CPC分类号： B41M5/1655 , C07C15/14 , Y10T428/2984
摘要： A remarkably low odor carbonless paper solvent is provided comprising a mixture of diisopropylbiphenyl and triisopropylbiphenyl, generally in an amount of 50 to 90% by weight diisopropylbiphenyl and 10 to 40% by weight triisopropylbiphenyl. The solvent and a chromogenic substance such as a leuco dye are encapsulated to form microcapsules which are coated onto one surface of a carrier sheet. A color developing substance is then applied to another sheet to form a carbonless marking system. When the microcapsules are ruptured, the solubilized chromogenic substance contacts and reacts with the developer to form an image.
摘要翻译：提供非常低气味的无碳纸溶剂，其包含二异丙基联苯和三异丙基联苯的混合物，通常为50至90重量％的二异丙基联苯和10至40重量％的三异丙基联苯。将溶剂和显色物质如无色染料包封以形成涂覆在载体片材的一个表面上的微胶囊。然后将彩色显影物质施加到另一片材上以形成无碳标记系统。当微胶囊破裂时，溶解的显色物质与显影剂接触并反应形成图像。

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