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1. 发明授权

US07151146B1 Neodymium-carbon nanotube and method of preparing high 1,4-cis-polybutadiene using the same 有权
标题翻译：钕碳纳米管及使用其制备高1,4-顺式聚丁二烯的方法
公开(公告)号：US07151146B1
公开(公告)日：2006-12-19
申请号：US11315322
申请日：2005-12-23
申请人： Gwanghoon Kwag , Pilsung Kim , Shin Han , Hyung Kyu Choi , Dong Hwan Kim , Seung Hwa Lee , Sung Hoon Han
发明人： Gwanghoon Kwag , Pilsung Kim , Shin Han , Hyung Kyu Choi , Dong Hwan Kim , Seung Hwa Lee , Sung Hoon Han
IPC分类号： C08F4/52 , C08F36/02
CPC分类号： C08F36/04 , Y10S526/908 , Y10S977/746 , Y10S977/748 , C08F4/545
摘要： The present invention relates to a method for preparing neodymium-carbon-nanotube and a process for preparing 1,4-cis-polybutadiene utilizing the same and more particularly, neodymium-carbon-nanotube. Neodymium is introduced by coordination with carboxylic acid, which is formed on the surface of carbon nanotube. In 1,3-butadiene polymerization with the neodymium-catalyst comprising the neodymium-carbon nanotube, a particular halogen compound, and a particular organometallic compound in an appropriate ratio, high 1,4-cis polybutadiene having molecular weight of 10,000 to 2,000,000 is produced, which exhibits excellent mechanical properties such as elasticity and durability.
摘要翻译：本发明涉及一种制备钕 - 碳纳米管的方法和一种使用该方法制备1,4-顺式聚丁二烯的方法，特别是钕 - 碳纳米管。通过与碳纳米管表面上形成的羧酸的配位引入钕。在含有钕 - 碳纳米管的钕 - 催化剂，特定的卤素化合物和特定的有机金属化合物的1,3-丁二烯聚合反应中，产生分子量为10,000至2,000,000的高1,4-顺式聚丁二烯其具有优异的机械性能如弹性和耐久性。

2. 发明申请

US20090048408A1 CATALYST COMPRISING HETEROLEPTIC ALUMINUM AND COBALT COMPOUNDS AND A METHOD OF PREPARING POLYBUTADIENE USING THE SAME 审中-公开
标题翻译：包含异丁烯铝和钴化合物的催化剂和使用其制备聚丁二烯的方法
公开(公告)号：US20090048408A1
公开(公告)日：2009-02-19
申请号：US12187420
申请日：2008-08-07
申请人： Gwanghoon Kwag , Pilsung Kim , Seung Hwon Lee , Hyung Kyu Choi
发明人： Gwanghoon Kwag , Pilsung Kim , Seung Hwon Lee , Hyung Kyu Choi
IPC分类号： C08F4/602
CPC分类号： C08F36/04 , C08F4/7096
摘要： The present invention relates to a novel catalyst for diene polymerization comprising a heteroleptic single-molecule aluminum compound and a cobalt compound having a carboxyl group with a predetermined proportion and a method for preparing polybutadiene from 1,3-butadiene using a catalyst for diene polymerization.The novel catalyst of the present invention, which comprises a heteroleptic single-molecule aluminum compound with a huge stereostructure and a cobalt compound, has a stabilized catalytic active site without the need of adding a special material for controlling the activity of cobalt, such as water, phenol, alcohol, and phosphorus compound, and has good activity without a catalyst aging process since the reduction of cobalt is minimized. Consequently, the catalyst may be used to polymerize 1,3-butadiene to obtain polybutadienes having cis and trans structures with good yield and narrow molecular weight distribution.
摘要翻译：本发明涉及一种新型二烯聚合催化剂，其包含异位单分子铝化合物和具有预定比例的羧基的钴化合物，以及使用二烯聚合催化剂由1,3-丁二烯制备聚丁二烯的方法。本发明的新型催化剂包括具有巨大立体结构的杂多单分子铝化合物和钴化合物，具有稳定的催化活性位点，而不需要添加用于控制钴的活性的特殊材料，例如水，苯酚，醇和磷化合物，并且由于钴的还原最小化，所以没有催化剂老化过程具有良好的活性。因此，催化剂可用于聚合1,3-丁二烯以获得具有良好产率和窄分子量分布的顺式和反式结构的聚丁二烯。

3. 发明授权

US08242204B2 Organic-inorganic nano composites and preparation method thereof 有权
标题翻译：有机 - 无机纳米复合材料及其制备方法
公开(公告)号：US08242204B2
公开(公告)日：2012-08-14
申请号：US12608717
申请日：2009-10-29
申请人： Gwanghoon Kwag , Hoochae Kim , Seunghwon Lee , Hwieon Park , Hyung Kyu Choi
发明人： Gwanghoon Kwag , Hoochae Kim , Seunghwon Lee , Hwieon Park , Hyung Kyu Choi
IPC分类号： C08L33/06 , B60C1/00
CPC分类号： C08K5/548 , B60C1/0016 , C08F2/38 , C08F236/10 , C08F279/02 , C08F2438/03 , C08K3/36 , C08L9/00 , C08L9/06 , C08L51/04 , Y02T10/862 , C08F220/14 , C08L2666/02
摘要： Provided is an organic-inorganic nano composite, and more particularly, an organic-inorganic nano composite which is a product formed by the reaction of a styrene-butadiene copolymer; an acryl-based monomer; a living radical polymerization initiator; silica; and a coupling agent, in which radiality is maximized. The organic-inorganic nano composite has excellent tensile and tear properties, and high wet fraction capability. Thus, if the organic-inorganic nano composite according to the present invention is applied to organic filler for tires, rolling resistance can be decreased and wet traction capability can be increased, and the organic-inorganic nano composite can be efficiently applied to a hard coating material as well.
摘要翻译：本发明提供一种有机 - 无机纳米复合物，更具体地说，是通过苯乙烯 - 丁二烯共聚物的反应形成的产物的有机 - 无机纳米复合物。丙烯酸类单体; 活性自由基聚合引发剂; 二氧化硅和其中径向性最大化的偶联剂。有机 - 无机纳米复合材料具有优异的拉伸和撕裂性能，以及高的分级能力。因此，如果将本发明的有机无机纳米复合体用于轮胎用有机填料，则能够降低滚动阻力，提高湿牵引能力，能够有效地将有机 - 无机纳米复合材料应用于硬涂层材料以及。

4. 发明申请

US20100184922A1 ORGANIC-INORGANIC NANO COMPOSITES AND PREPARATION METHOD THEREOF 有权
标题翻译：有机无机纳米复合材料及其制备方法
公开(公告)号：US20100184922A1
公开(公告)日：2010-07-22
申请号：US12608717
申请日：2009-10-29
申请人： Gwanghoon Kwag , Hoochae Kim , Seunghwon Lee , Hwieon Park , Hyung Kyu Choi
发明人： Gwanghoon Kwag , Hoochae Kim , Seunghwon Lee , Hwieon Park , Hyung Kyu Choi
IPC分类号： C08F257/00
CPC分类号： C08K5/548 , B60C1/0016 , C08F2/38 , C08F236/10 , C08F279/02 , C08F2438/03 , C08K3/36 , C08L9/00 , C08L9/06 , C08L51/04 , Y02T10/862 , C08F220/14 , C08L2666/02
摘要： Provided is an organic-inorganic nano composite, and more particularly, an organic-inorganic nano composite including: a styrene-butadiene copolymer; an acryl-based monomer; a living radical polymerization initiator; silica; and a coupling agent, in which radiality is maximized. The organic-inorganic nano composite is prepared using a method comprising: preparing a spherical styrene-butadiene copolymer; preparing a nano-sized spherical styrene-butadiene-acrylate copolymer using living radical polymerization of the spherical styrene-butadiene copolymer and an acryl-based monomer; and preparing a composite by coupling the nano-sized spherical styrene-butadiene-acrylate copolymer and silica using a coupling agent. The organic-inorganic nano composite has excellent tensile and tear properties, and high wet traction capability. Thus, if the organic-inorganic nano composite according to the present invention is applied to organic filler for tires, rolling resistance can be decreased and wet traction capability can be increased, and the organic-inorganic nano composite can be efficiently applied to a hard coating material as well.
摘要翻译：本发明提供一种有机 - 无机纳米复合体，更具体地说，涉及含有：苯乙烯 - 丁二烯共聚物的有机 - 无机纳米复合物，丙烯酸类单体; 活性自由基聚合引发剂; 二氧化硅和其中径向性最大化的偶联剂。有机 - 无机纳米复合材料是使用以下方法制备的：制备球形苯乙烯 - 丁二烯共聚物; 使用球形苯乙烯 - 丁二烯共聚物和丙烯酸类单体的活性自由基聚合制备纳米尺寸的球形苯乙烯 - 丁二烯 - 丙烯酸酯共聚物; 并通过使用偶联剂偶联纳米尺寸的球形苯乙烯 - 丁二烯 - 丙烯酸酯共聚物和二氧化硅来制备复合材料。有机 - 无机纳米复合材料具有优异的拉伸和撕裂性能，以及高湿牵引能力。因此，如果将本发明的有机无机纳米复合体用于轮胎用有机填料，则能够降低滚动阻力，提高湿牵引能力，能够有效地将有机 - 无机纳米复合材料应用于硬涂层材料以及。

5. 发明授权

US06624256B2 Method of preparation of siloxane-functionalized high 1,4-cis polybutadiene 失效
公开(公告)号：US06624256B2
公开(公告)日：2003-09-23
申请号：US10035498
申请日：2001-11-09
申请人： Gwanghoon Kwag , Aju Kim , Seunghwon Lee
发明人： Gwanghoon Kwag , Aju Kim , Seunghwon Lee
IPC分类号： C08C1925
CPC分类号： C08C19/25
摘要： Disclosed is a method of preparation of a siloxane-functionalized high 1,4-cis polybutadiene using a siloxane compound, in which the siloxane group expands the usage of the high 1,4-cis polybutadiene.

6. 发明授权

US09328176B2 Functional styrene-butadiene copolymer 有权
标题翻译：功能性苯乙烯 - 丁二烯共聚物
公开(公告)号：US09328176B2
公开(公告)日：2016-05-03
申请号：US12732666
申请日：2010-03-26
申请人： Gwanghoon Kwag , Hoo Chae Kim , Donghyuk Na , Hyun-jong Paik , Jongyeop Lee
发明人： Gwanghoon Kwag , Hoo Chae Kim , Donghyuk Na , Hyun-jong Paik , Jongyeop Lee
IPC分类号： C08F220/32 , C08C19/40 , B60C1/00 , C08K3/36 , C08L9/06 , C08L15/00 , C08L19/00 , C08F236/10 , C08F212/08 , C08F236/06 , C08K5/548 , C08L9/00
CPC分类号： C08C19/40 , B60C1/00 , C08F212/08 , C08F220/32 , C08F236/06 , C08F236/10 , C08F2220/325 , C08F2810/50 , C08K3/36 , C08K5/548 , C08L9/00 , C08L9/06 , C08L15/00 , C08L19/006 , C08L2666/02 , C08L2666/08
摘要： A functional styrene-butadiene copolymer is disclosed. More specifically, the copolymer is prepared by radical polymerization of a styrene monomer, a butadiene monomer and an epoxy acrylate monomer in an emulsion state and ring-opening of the resultant styrene-butadiene-epoxy acrylate copolymer. When blended with silica, the disclosed copolymer provides excellent wet stopping performance and superior wear resistance. Therefore, it can be usefully applied for industrial materials including fuel-efficient tires, snow tires, belts, hoses, etc.
摘要翻译：公开了一种功能性苯乙烯 - 丁二烯共聚物。更具体地说，共聚物通过苯乙烯单体，丁二烯单体和环氧丙烯酸酯单体以乳液状态和所得苯乙烯 - 丁二烯 - 环氧丙烯酸酯共聚物的开环自由基聚合制备。当与二氧化硅混合时，所公开的共聚物提供优异的湿阻止性能和优异的耐磨性。因此，它可以有效地应用于工业材料，包括节能轮胎，雪地轮胎，皮带，软管等。

7. 发明授权

US08530017B2 Method for preparing styrene-butadiene copolymer using reactive emulsifier and styrene-butadiene copolymer prepared by the same 有权
标题翻译：使用反应性乳化剂和由其制备的苯乙烯 - 丁二烯共聚物制备苯乙烯 - 丁二烯共聚物的方法
公开(公告)号：US08530017B2
公开(公告)日：2013-09-10
申请号：US13167073
申请日：2011-06-23
申请人： Gwanghoon Kwag , Dong Hyuk Na , Jun Keol Choi
发明人： Gwanghoon Kwag , Dong Hyuk Na , Jun Keol Choi
IPC分类号： B32B1/08 , C08F236/14
CPC分类号： C08K3/36 , B60C1/00 , B65G15/32 , C08F212/08 , C08F236/06 , C08F236/10 , F16G1/06 , F16G5/04 , F16L11/04 , C08L9/06 , C08F4/26 , C08F4/04 , C08F4/34 , C08F4/40 , C08F2220/286
摘要： Provided is a method for preparing a styrene-butadiene copolymer having improved silica affinity through introduction of a novel reactive emulsifier. The styrene-butadiene copolymer prepared according to the disclosed method has superior affinity for thereby and thus has superior processability and tensile properties and remarkably improved dynamic properties. Therefore, when the styrene-butadiene copolymer according to the present invention is used as a tire tread material, it can greatly improve its physical properties.
摘要翻译：提供通过引入新的反应性乳化剂制备具有改善的二氧化硅亲和性的苯乙烯 - 丁二烯共聚物的方法。根据所公开的方法制备的苯乙烯 - 丁二烯共聚物对其具有优异的亲和性，因此具有优异的加工性能和拉伸性能，并且显着提高动态性能。因此，当将本发明的苯乙烯 - 丁二烯共聚物用作轮胎胎面材料时，其可以大大提高其物理性能。

8. 发明授权

US08455600B2 Styrene-butadiene copolymer highly functionalized with reactive polyol and manufacturing method thereof 有权
标题翻译：用反应性多元醇高官能化的苯乙烯 - 丁二烯共聚物及其制备方法
公开(公告)号：US08455600B2
公开(公告)日：2013-06-04
申请号：US13085279
申请日：2011-04-12
申请人： Seung Su Kim , Gwanghoon Kwag , Dong Hyuk Na , Jun Keol Choi , Seung Moo Huh , Jeon Koo Lee , Hye Min Kim
发明人： Seung Su Kim , Gwanghoon Kwag , Dong Hyuk Na , Jun Keol Choi , Seung Moo Huh , Jeon Koo Lee , Hye Min Kim
IPC分类号： C08L25/10 , C08L25/14 , C08L9/06 , B60C1/00
CPC分类号： C08F236/10 , C08F212/08
摘要： Provided is a functional styrene-butadiene copolymer having superior silica affinity. The copolymer is prepared by radical polymerizing a styrene monomer, a butadiene monomer and a reactive polyol monomer in emulsion state in order to maximize the mixing effect when compounding with silica. When mixed with silica, the disclosed styrene-butadiene copolymer provides excellent wet traction and superior abrasion resistance, and is suitable to be used for an industrial material of snow tires, belts, hoses, etc.
摘要翻译：提供了具有优异的二氧化硅亲和性的功能性苯乙烯 - 丁二烯共聚物。共聚物通过在乳液状态下自由基聚合苯乙烯单体，丁二烯单体和反应性多元醇单体来制备，以便在与二氧化硅配混时最大化混合效果。当与二氧化硅混合时，公开的苯乙烯 - 丁二烯共聚物提供优良的湿牵引力和优异的耐磨性，并且适用于雪轮胎，皮带，软管等的工业材料。

9. 发明申请

US20120164363A1 Method for Preparing Styrene-Butadiene Copolymer Using Reactive Emulsifier and Styrene-Butadiene Copolymer Prepared By the Same 有权
标题翻译：使用其制备的反应性乳化剂和苯乙烯 - 丁二烯共聚物制备苯乙烯 - 丁二烯共聚物的方法
公开(公告)号：US20120164363A1
公开(公告)日：2012-06-28
申请号：US13167073
申请日：2011-06-23
申请人： Gwanghoon Kwag , Dong Hyuk Na , Jun Keol Choi
发明人： Gwanghoon Kwag , Dong Hyuk Na , Jun Keol Choi
IPC分类号： B32B1/08 , C08L9/06 , C08F236/14
CPC分类号： C08K3/36 , B60C1/00 , B65G15/32 , C08F212/08 , C08F236/06 , C08F236/10 , F16G1/06 , F16G5/04 , F16L11/04 , C08L9/06 , C08F4/26 , C08F4/04 , C08F4/34 , C08F4/40 , C08F2220/286
摘要： Provided is a method for preparing a styrene-butadiene copolymer having improved silica affinity through introduction of a novel reactive emulsifier. The styrene-butadiene copolymer prepared according to the disclosed method has superior affinity for thereby and thus has superior processability and tensile properties and remarkably improved dynamic properties. Therefore, when the styrene-butadiene copolymer according to the present invention is used as a tire tread material, it can greatly improve its physical properties.
摘要翻译：提供通过引入新的反应性乳化剂制备具有改善的二氧化硅亲和性的苯乙烯 - 丁二烯共聚物的方法。根据所公开的方法制备的苯乙烯 - 丁二烯共聚物对其具有优异的亲和性，因此具有优异的加工性能和拉伸性能，并且显着提高动态性能。因此，当将本发明的苯乙烯 - 丁二烯共聚物用作轮胎胎面材料时，其可以大大提高其物理性能。

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