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1. 发明申请

US20110232656A1 METHOD FOR MAKING PARTICLE OF A HYDROPHOBIC ADDITIVE AND A POLYSACCHARIDE COATING AND TOBACCO PRODUCTS CONTAINING PARTICLE OF A HYDROPHOBIC ADDITIVE AND A POLYSACCHARIDE COATING 有权
标题翻译：制造含有疏水性添加剂和多糖涂料颗粒的疏水添加剂和多糖涂层和烟草制品的方法
公开(公告)号：US20110232656A1
公开(公告)日：2011-09-29
申请号：US12748227
申请日：2010-03-26
申请人： Yi Zeng , Shuzhong Zhuang , Georgios D. Karles
发明人： Yi Zeng , Shuzhong Zhuang , Georgios D. Karles
IPC分类号： A23L1/221 , A24C5/00 , A24B15/40
CPC分类号： A24B15/283 , A23L27/72 , A24B13/00 , A24D1/002 , A24D3/048
摘要： A method for providing particles of encapsulated flavorants or chemesthetic agents comprises forming an emulsion comprising: (i) a first aqueous solution, comprising one or more polysaccharides; and (ii) a hydrophobic additive; atomizing said emulsion in an atomizer into droplets; introducing said droplets into a second aqueous solution, comprising one or more metal cations, to form particles comprising one or more cross-linked polysaccharides and said additive encapsulated therein; and removing said particles from said second aqueous solution and drying said particles.
摘要翻译：提供包封的香料或化学剂的颗粒的方法包括形成乳液，其包含：（i）包含一种或多种多糖的第一水溶液; 和（ii）疏水性添加剂; 将雾化器中的所述乳液雾化成液滴; 将所述液滴引入包含一种或多种金属阳离子的第二水溶液中，以形成包含一种或多种交联多糖的颗粒，并将所述添加剂包封在其中; 并从所述第二水溶液中除去所述颗粒并干燥所述颗粒。

2. 发明授权

US09993019B2 Method for making particle of a hydrophobic additive and a polysaccharide coating and tobacco products containing particle of a hydrophobic additive and a polysaccharide coating 有权
公开(公告)号：US09993019B2
公开(公告)日：2018-06-12
申请号：US12748227
申请日：2010-03-26
申请人： Yi Zeng , Shuzhong Zhuang , Georgios D. Karles
发明人： Yi Zeng , Shuzhong Zhuang , Georgios D. Karles
IPC分类号： A24B13/00 , A24B15/28 , A24D1/00 , A24D3/04 , A23L27/00
CPC分类号： A24B15/283 , A23L27/72 , A24B13/00 , A24D1/002 , A24D3/048
摘要： A method for providing particles of encapsulated flavorants or chemesthetic agents comprises forming an emulsion comprising: (i) a first aqueous solution, comprising one or more polysaccharides; and (ii) a hydrophobic additive; atomizing said emulsion in an atomizer into droplets; introducing said droplets into a second aqueous solution, comprising one or more metal cations, to form particles comprising one or more cross-linked polysaccharides and said additive encapsulated therein; and removing said particles from said second aqueous solution and drying said particles.

3. 发明申请

US20120037171A1 PROCESS FOR MAKING A CONTINUOUS STRUCTURE OF AN ENCAPSULATED MATERIAL 有权
标题翻译：制造封装材料连续结构的工艺
公开(公告)号：US20120037171A1
公开(公告)日：2012-02-16
申请号：US13071570
申请日：2011-03-25
申请人： Shuzhong Zhuang , Yi Zeng , Georgios D. Karles
发明人： Shuzhong Zhuang , Yi Zeng , Georgios D. Karles
IPC分类号： A24B15/30 , A24D3/04 , B01J13/00 , A24C5/00
CPC分类号： A24D1/002 , A23L27/72 , A23L27/80 , A23P10/30 , A24B3/12 , A24D3/061 , A24D3/062 , A24D3/163
摘要： A method for providing an encapsulated flavorant or chemesthetic agent in a smoking article includes forming an emulsion including: (i) a first aqueous solution, comprising one or more cross-linkable polysaccharides; and (ii) a hydrophobic additive comprising one or more flavorants or chemesthetic agents. The method also includes extruding the emulsion into a second aqueous solution in the form of an elongated structure, cross-linking at least a portion of the one or more cross-linkable polysaccharides, removing the cross-linked elongated structure from the second aqueous solution, introducing the cross-linked elongated structure into a filter, or into a rod including a smoking composition, or both; and forming the filter or the rod of the smoking composition into a smoking article. The method can include a drying step.
摘要翻译：在吸烟制品中提供包封的香料或化学治疗剂的方法包括形成乳液，其包括：（i）包含一种或多种可交联多糖的第一水溶液; 和（ii）包含一种或多种调味剂或化学试剂的疏水性添加剂。该方法还包括将乳液挤出成细长结构形式的第二水溶液，交联至少一部分一种或多种可交联多糖，从第二种水溶液中除去交联的细长结构，将交联的细长结构引入过滤器或引入包括吸烟组合物的杆或两者; 以及将吸烟组合物的过滤器或棒形成为吸烟制品。该方法可以包括干燥步骤。

4. 发明授权

US09034107B2 Process for making a continuous structure of an encapsulated material 有权
标题翻译：制造封装材料的连续结构的方法
公开(公告)号：US09034107B2
公开(公告)日：2015-05-19
申请号：US13071570
申请日：2011-03-25
申请人： Shuzhong Zhuang , Yi Zeng , Georgios D. Karles
发明人： Shuzhong Zhuang , Yi Zeng , Georgios D. Karles
IPC分类号： A23L1/22 , A24D1/00 , A24B3/12 , A23P1/04
CPC分类号： A24D1/002 , A23L27/72 , A23L27/80 , A23P10/30 , A24B3/12 , A24D3/061 , A24D3/062 , A24D3/163
摘要： A method for providing an encapsulated flavorant or chemesthetic agent in a smoking article includes forming an emulsion including: (i) a first aqueous solution, comprising one or more cross-linkable polysaccharides; and (ii) a hydrophobic additive comprising one or more flavorants or chemesthetic agents. The method also includes extruding the emulsion into a second aqueous solution in the form of an elongated structure, cross-linking at least a portion of the one or more cross-linkable polysaccharides, removing the cross-linked elongated structure from the second aqueous solution, introducing the cross-linked elongated structure into a filter, or into a rod including a smoking composition, or both; and forming the filter or the rod of the smoking composition into a smoking article. The method can include a drying step.
摘要翻译：在吸烟制品中提供包封的香料或化学治疗剂的方法包括形成乳液，其包括：（i）包含一种或多种可交联多糖的第一水溶液; 和（ii）包含一种或多种调味剂或化学试剂的疏水性添加剂。该方法还包括将乳液挤出成细长结构形式的第二水溶液，交联至少一部分一种或多种可交联多糖，从第二水溶液中除去交联的细长结构，将交联的细长结构引入过滤器或引入包括吸烟组合物的杆或两者; 以及将吸烟组合物的过滤器或棒形成为吸烟制品。该方法可以包括干燥步骤。

5. 发明授权

US10051884B2 Controlled release mentholated tobacco beads 有权
公开(公告)号：US10051884B2
公开(公告)日：2018-08-21
申请号：US12748259
申请日：2010-03-26
申请人： Georgios D. Karles , Shuzhong Zhuang , Yi Zeng
发明人： Georgios D. Karles , Shuzhong Zhuang , Yi Zeng
IPC分类号： A24B15/30 , A24B15/28 , A24B15/18
CPC分类号： A24B15/283 , A24B15/186 , A24B15/30
摘要： Encapsulated tobacco beads and processes of making the encapsulated tobacco beads are disclosed. According to an embodiment, a process of making encapsulated tobacco beads comprises mixing tobacco particles and menthol in an aqueous solution to form a wet mass; extruding the wet mass to form extrudates; spheronizing the extrudates to form tobacco beads; drying the tobacco beads; contacting the beads with a solution comprising a cation; and introducing the contacted tobacco beads into a solution of coating material in a concentration effective to induce ionic gelation of the coating material around the beads, to form encapsulated tobacco beads having gel coatings. According to another embodiment, an encapsulated tobacco bead comprises a core comprising tobacco particles and encapsulated menthol, an inner coating layer comprising hydroxypropyl methylcellulose or pectin, and an outer coating layer comprising an ionically-crosslinked gel.

6. 发明申请

US20110232657A1 CONTROLLED RELEASE MENTHOLATED TOBACCO BEADS 审中-公开
标题翻译：受控释放的迷迭香珠
公开(公告)号：US20110232657A1
公开(公告)日：2011-09-29
申请号：US12748259
申请日：2010-03-26
申请人： Georgios D. Karles , Shuzhong Zhuang , Yi Zeng
发明人： Georgios D. Karles , Shuzhong Zhuang , Yi Zeng
IPC分类号： A24B15/30 , A24B13/00
CPC分类号： A24B15/283 , A24B15/186 , A24B15/30
摘要： Encapsulated tobacco beads and processes of making the encapsulated tobacco beads are disclosed. According to an embodiment, a process of making encapsulated tobacco beads comprises mixing tobacco particles and menthol in an aqueous solution to form a wet mass; extruding the wet mass to form extrudates; spheronizing the extrudates to form tobacco beads; drying the tobacco beads; contacting the beads with a solution comprising a cation; and introducing the contacted tobacco beads into a solution of coating material in a concentration effective to induce ionic gelation of the coating material around the beads, to form encapsulated tobacco beads having gel coatings. According to another embodiment, an encapsulated tobacco bead comprises a core comprising tobacco particles and encapsulated menthol, an inner coating layer comprising hydroxypropyl methylcellulose or pectin, and an outer coating layer comprising an ionically-crosslinked gel.
摘要翻译：公开了包封的烟草珠和制备包封的烟草珠的方法。根据一个实施方案，制备包封的烟草珠的方法包括将烟草颗粒和薄荷醇混合在水溶液中以形成湿团块; 挤出湿物质以形成挤出物; 使挤出物成球形成烟丝珠; 烘干烟草珠; 使珠粒与包含阳离子的溶液接触; 并将接触的烟草珠引入到涂层材料的溶液中，浓度有效地诱导珠粒周围涂层材料的离子凝胶化，形成具有凝胶涂层的包封的烟草珠粒。根据另一个实施方案，封装的烟草珠包含包含烟草颗粒和包封的薄荷醇的核，包含羟丙基甲基纤维素或果胶的内包衣层和包含离子交联凝胶的外包衣层。

7. 发明授权

US08235056B2 Smoking article with concentric hollow core in tobacco rod and capsule containing flavorant and aerosol forming agents in the filter system 有权
标题翻译：吸烟制品在烟草棒中具有同心中空芯，并且在过滤系统中含有食用香料和烟雾剂形成剂
公开(公告)号：US08235056B2
公开(公告)日：2012-08-07
申请号：US12000863
申请日：2007-12-18
申请人： Shuzhong Zhuang , Georgios D. Karles , Raquel M. Olegario
发明人： Shuzhong Zhuang , Georgios D. Karles , Raquel M. Olegario
IPC分类号： A24D3/06
CPC分类号： A24D1/00 , A24D3/061
摘要： A smoking article having a cylinder of smoking material and a central tube within the cylinder of the smoking material wherein heat is convectively transferred with smoke from a lit end of the cylinder of smoking material through the central tube to a mouth end of the cylinder of smoking material in each puff. A filter system is attached to the cylinder of smoking material, and includes a plurality of segments, wherein at least one of the plurality of segments contains flavorant and aerosol forming agents encapsulated in at least one breakable capsule.
摘要翻译：一种具有吸烟材料圆筒和吸烟材料圆筒内的中心管的吸烟制品，其中热量通过烟雾从吸烟材料筒的点燃端部通过中心管对流传播到吸烟筒的嘴端每个泡芙的材料。过滤系统连接到吸烟材料的圆筒，并且包括多个部分，其中多个部分中的至少一个部分包含密封在至少一个可破裂胶囊中的香味剂和烟雾形成剂。

8. 发明申请

US20110104218A1 METHODS AND COMPOSITIONS FOR PRODUCING HYDROGEL CAPSULES COATED FOR LOW PERMEABILITY AND PHYSICAL INTEGRITY 有权
标题翻译：生产用于低渗透性和物理完整性的水凝胶囊剂的方法和组合物
公开(公告)号：US20110104218A1
公开(公告)日：2011-05-05
申请号：US12612881
申请日：2009-11-05
申请人： Georgios D. Karles , Daqing Wu , Shuzhong Zhuang
发明人： Georgios D. Karles , Daqing Wu , Shuzhong Zhuang
IPC分类号： A61K8/11 , B05D3/00 , A24B15/00 , A24D1/00 , A24D3/04 , A61K9/48
CPC分类号： A24B15/186 , A23L27/72 , A23P10/30 , A23V2002/00 , A24B13/00 , A24B15/283 , A24D3/061 , A61K8/11 , A61K8/31 , A61K8/731 , A61K8/733 , A61K8/8152 , A61K9/5026 , A61K9/5036 , A61K9/5073 , A61Q19/00 , B01J13/22 , C09B67/0097 , A23V2200/224 , A23V2250/5026 , A23V2250/5036 , A23V2250/5072
摘要： Methods and compositions for producing hydrogel capsules enveloped with at least one coating layer is disclosed. The coating formulations deposited on the surface of the capsules can improve the physical integrity and the water-retention properties of the alginate beads. The coating formulations can be sequentially applied in various combinations to obtain desirable properties, such as improved physical integrity, mechanical strength, and low permeability, that can extend the shelf-life of the capsules when incorporated into various consumer products.
摘要翻译：公开了用至少一个涂层包裹的生产水凝胶胶囊的方法和组合物。沉积在胶囊表面上的涂料制剂可以改善藻酸盐珠的物理完整性和保水性。涂层制剂可以以各种组合顺序施用以获得所需的性能，例如改善的物理完整性，机械强度和低渗透性，当将其并入各种消费品时可延长胶囊的保存期限。

9. 发明申请

US20080110470A1 Immobilized diluents for smoking articles 有权
标题翻译：用于吸烟制品的固定化稀释剂
公开(公告)号：US20080110470A1
公开(公告)日：2008-05-15
申请号：US11812028
申请日：2007-06-14
申请人： Shuzhong Zhuang , Georgios D. Karles
发明人： Shuzhong Zhuang , Georgios D. Karles
IPC分类号： A24D3/06
CPC分类号： A24B15/283 , A24B15/245 , A24B15/246 , A24B15/28 , A24B15/287 , A24C5/472 , A24D3/06 , A24F47/008 , B01J20/20 , B01J20/28004 , B01J20/28019 , B01J20/28061 , B01J20/28064 , B01J20/28071 , B01J20/28073 , B01J20/28076
摘要： Immobilized diluents in a smoking article are provided, wherein diluents can be immobilized through absorption and/or adsorption of the diluents into immobilizing materials, such as sorbents like silica gels. By immobilizing diluents, the diluents can be available for vaporization, while still being protected from migration and/or loss of the diluents in a smoking article.
摘要翻译：提供了吸烟制品中的固定化稀释剂，其中稀释剂可以通过将稀释剂吸收和/或吸附到诸如硅胶等吸附剂的固定材料中来固定。通过固定稀释剂，稀释剂可用于蒸发，同时仍然保护免受吸烟制品中稀释剂的迁移和/或损失。

10. 发明授权

US08393333B2 Immobilized diluents for smoking articles 有权
标题翻译：用于吸烟制品的固定化稀释剂
公开(公告)号：US08393333B2
公开(公告)日：2013-03-12
申请号：US11812028
申请日：2007-06-14
申请人： Shuzhong Zhuang , Georgios D. Karles
发明人： Shuzhong Zhuang , Georgios D. Karles
IPC分类号： A24D3/04
CPC分类号： A24B15/283 , A24B15/245 , A24B15/246 , A24B15/28 , A24B15/287 , A24C5/472 , A24D3/06 , A24F47/008 , B01J20/20 , B01J20/28004 , B01J20/28019 , B01J20/28061 , B01J20/28064 , B01J20/28071 , B01J20/28073 , B01J20/28076
摘要： Immobilized diluents in a smoking article are provided, wherein diluents can be immobilized through absorption and/or adsorption of the diluents into immobilizing materials, such as sorbents like silica gels. By immobilizing diluents, the diluents can be available for vaporization, while still being protected from migration and/or loss of the diluents in a smoking article.
摘要翻译：提供了吸烟制品中的固定化稀释剂，其中稀释剂可以通过将稀释剂吸收和/或吸附到诸如硅胶等吸附剂的固定材料中来固定。通过固定稀释剂，稀释剂可用于蒸发，同时仍然保护免受吸烟制品中稀释剂的迁移和/或损失。

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