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1. 发明申请

US20080108777A1 POLYCARBONATES WITH FLUOROALKYLENE CARBONATE END GROUPS 有权
标题翻译：聚碳酸酯与氟亚甲基碳酸酯末端组
公开(公告)号：US20080108777A1
公开(公告)日：2008-05-08
申请号：US12013141
申请日：2008-01-11
申请人： Gary Davis , Dibakar Dhara , Brian Mullen , Joshua Stone
发明人： Gary Davis , Dibakar Dhara , Brian Mullen , Joshua Stone
IPC分类号： C08G64/10
CPC分类号： C08G64/10 , C08G63/64 , C08G63/6826 , C08G64/186 , C08K5/42 , C08L67/00 , C08L69/00 , C08L79/08 , C08L2666/18 , C08L2666/20
摘要： Polycarbonate compositions having an aromatic polycarbonate resin with 90% or greater fluoroalkylene carbonate end-groups are formed from a partially fluorinated alcohol or a partially fluorinated polymeric alcohol, and a bisphenol and a carbonate source using melt or interfacial polymerization methods. Copolymers and blends with a variety of other bisphenols and other thermoplastics are also described. The polycarbonate compositions show high water contact angles, fluorine enrichment on the surface layer of molded articles, and good flame retardant properties and are useful in a variety of applications including medical, automotive, telecommunication and weatherable applications.
摘要翻译：具有90％或更多氟代亚烷基碳酸酯端基的芳族聚碳酸酯树脂的聚碳酸酯组合物由部分氟化的醇或部分氟化的聚合物醇和使用熔体或界面聚合方法的双酚和碳酸酯源形成。还描述了与各种其它双酚和其它热塑性塑料的共聚物和共混物。聚碳酸酯组合物显示出高的接触角，在模制品的表面层上富集氟，并具有良好的阻燃性能，并且可用于各种应用，包括医疗，汽车，电信和耐候性应用。

2. 发明申请

US20060135737A1 Polycarbonates with fluoroalkylene carbonate end groups 审中-公开
公开(公告)号：US20060135737A1
公开(公告)日：2006-06-22
申请号：US11022535
申请日：2004-12-22
申请人： Gary Davis , Dibakar Dhara , Brian Mullen , Joshua Stone
发明人： Gary Davis , Dibakar Dhara , Brian Mullen , Joshua Stone
IPC分类号： C08G63/68
CPC分类号： C08G64/10 , C08G63/64 , C08G63/6826 , C08G64/186 , C08K5/42 , C08L67/00 , C08L69/00 , C08L79/08 , C08L2666/18 , C08L2666/20
摘要： Polycarbonate compositions having an aromatic polycarbonate resin with 90% or greater fluoroalkylene carbonate end-groups are formed from a partially fluorinated alcohol or a partially fluorinated polymeric alcohol, and a bisphenol and a carbonate source using melt or interfacial polymerization methods. Copolymers and blends with a variety of other bisphenols and other thermoplastics are also described. The polycarbonate compositions show high water contact angles, fluorine enrichment on the surface layer of molded articles, and good flame retardant properties and are useful in a variety of applications including medical, automotive, telecommunication and weatherable applications.

3. 发明申请

US20070122627A1 WEATHERABLE, THERMOSTABLE POLYMERS HAVING IMPROVED FLOW COMPOSITION 有权
标题翻译：具有改进流动性组合物的耐热可聚合聚合物
公开(公告)号：US20070122627A1
公开(公告)日：2007-05-31
申请号：US11627828
申请日：2007-01-26
申请人： Gary Davis , Brian Mullen , Paul Sybert
发明人： Gary Davis , Brian Mullen , Paul Sybert
IPC分类号： B32B27/36 , C08F20/00
CPC分类号： B32B27/365 , B32B27/06 , B32B27/08 , B32B27/20 , B32B27/283 , B32B27/36 , B32B2307/584 , B32B2307/71 , B32B2307/712 , B32B2419/00 , B32B2605/00 , C08F293/00 , C08G63/19 , C08G63/64 , C08G63/676 , C08G63/6956 , C08G63/79 , C08J7/047 , C08J2467/00 , C08J2469/00 , C08L53/00 , C08L2666/02 , C09D153/00 , C09D167/03 , C09J153/00 , F02B61/045 , Y10T428/31504 , Y10T428/31507
摘要： A copolymer composition comprises an arylate polyester unit, an aromatic carbonate unit, and a soft-block moiety, wherein individual occurrences of the soft block moiety are linked by a spacer unit comprising one or more of the arylate polyester units, one or more of the aromatic carbonate units, or a combination comprising each of these. In one embodiment, a soft block moiety comprises a polysiloxane unit. A film of the composition has a percent transmittance of greater than or equal to 60% as determined according to ASTM D1003-00. A method of forming a copolymer composition is disclosed, comprising substantially forming the bis-haloformates of a dihydroxy compound comprising an arylate polyester unit, and a dihydroxy compound comprising a soft-block moiety, and reacting the bis haloformates with a dihydroxy aromatic compound. In an embodiment, a multilayer article comprises the thermostable, weatherable polymer.
摘要翻译：共聚物组合物包含芳基化聚酯单元，芳族碳酸酯单元和软嵌段部分，其中软嵌段部分的单独出现由包含一个或多个芳基化聚酯单元的间隔单元连接，一个或多个芳族碳酸酯单元，或包含这些中的每一个的组合。在一个实施方案中，软嵌段部分包含聚硅氧烷单元。根据ASTM D1003-00测定，该组合物的透光率百分比大于或等于60％。公开了一种形成共聚物组合物的方法，其包括基本上形成包含芳基化聚酯单元的二羟基化合物的双卤代甲酸酯和包含软嵌段部分的二羟基化合物，并使双卤代甲酸酯与二羟基芳族化合物反应。在一个实施方案中，多层制品包含耐热耐候性聚合物。

4. 发明申请

US20070027271A1 WEATHERABLE, THERMOSTABLE POLYMERS HAVING IMPROVED FLOW COMPOSITION 有权
标题翻译：具有改进流动性组合物的耐热可聚合聚合物
公开(公告)号：US20070027271A1
公开(公告)日：2007-02-01
申请号：US11426680
申请日：2006-06-27
申请人： Gary Davis , Brian Mullen , Paul Sybert
发明人： Gary Davis , Brian Mullen , Paul Sybert
IPC分类号： C08L83/10 , C08L83/14
CPC分类号： C08G64/186 , C08G63/64 , C08G63/6956 , C08G77/448 , C08L69/00 , C08L83/10 , C08L2666/02
摘要： A copolymer composition comprises a polysiloxane block of Formula XIX or XXII, having 4 to 50 siloxane units, and a polyarylate-polycarbonate block consisting essentially of 50 to 99 mol % arylate polyester units and 1 to 50 mol % aromatic carbonate units, wherein 1 to 30 mole percent of the aromatic carbonate units are resorcinol carbonates, and 0 to 35 mol % of the aromatic carbonate units are bisphenol carbonates; wherein the sum of mole percentages of arylate polyester units, and aromatic carbonate units is 100 mol %; the polysiloxane blocks connect to an arylate ester unit, and/or an aromatic carbonate unit; the siloxane units of the polysiloxane block are present at 0.2 to 10 wt % based on weight of the copolymer composition; and a molded article of 3.2±0.12 millimeters thickness and consisting of the copolymer composition has a percent transmittance greater than or equal to 70%, according to ASTM D1003-00.
摘要翻译：共聚物组合物包含具有4至50个硅氧烷单元的式XIX或XXII的聚硅氧烷嵌段和基本上由50至99mol％芳基化聚酯单元和1至50mol％芳族碳酸酯单元组成的聚芳酯 - 聚碳酸酯嵌段，其中1至 30摩尔％的芳族碳酸酯单元是间苯二酚碳酸酯，0-35摩尔％的芳族碳酸酯单元是双酚碳酸酯; 其中芳基化聚酯单元和芳族碳酸酯单元的摩尔百分比之和为100摩尔％。聚硅氧烷嵌段连接到芳基酯单元和/或芳族碳酸酯单元; 聚硅氧烷嵌段的硅氧烷单元以基于共聚物组合物的重量计为0.2-10重量％存在; 并且根据ASTM D1003-00，由共聚物组合物组成的3.2±0.12毫米厚的模制品具有百分比透射率大于或等于70％。

5. 发明申请

US20070129492A1 POLYSILOXANE COPOLYMERS, THERMOPLASTIC COMPOSITION, AND ARTICLES FORMED THEREFROM 有权
标题翻译：聚硅氧烷共聚物，热塑性组合物及其形成的制品
公开(公告)号：US20070129492A1
公开(公告)日：2007-06-07
申请号：US11537154
申请日：2006-09-29
申请人： Robert Colborn , Gary Davis , Jianbo Di , Constantin Donea , Irene Dris , Katherine Jackson , Brian Mullen , Laura Schultz , Moitreyee Sinha , Paul Sybert
发明人： Robert Colborn , Gary Davis , Jianbo Di , Constantin Donea , Irene Dris , Katherine Jackson , Brian Mullen , Laura Schultz , Moitreyee Sinha , Paul Sybert
IPC分类号： C08L83/10
CPC分类号： C08G63/64 , B64C1/1492 , C08G63/19 , C08G63/605 , C08G63/6956 , C08L83/10 , Y10T428/31663
摘要： A polysiloxane copolymer composition comprises: a polysiloxane unit comprising 4 to 50 siloxane units, and a polyester-polycarbonate unit consisting of 50 to 100 mole percent of arylate ester units, less than 50 mole percent aromatic carbonate units, less than 30 mole percent resorcinol carbonate units, and less than 35 mole percent bisphenol carbonate units, wherein the siloxane units are present in the polysiloxane unit in an amount of 0.2 to 10 wt % of the total weight of the polysiloxane copolymer composition, and wherein the polysiloxane copolymer composition has a 2 minute integrated heat release rate of less than or equal to 65 kilowatt-minutes per square meter (kW-min/m2) and a peak heat release rate of less than 65 kilowatts per square meter (kW/m2) as measured using the method of FAR F25.4, in accordance with Federal Aviation Regulation FAR 25.853 (d). A window article for an aircraft, comprising the polysiloxane copolymer composition, is also disclosed.
摘要翻译：聚硅氧烷共聚物组合物包括：包含4至50个硅氧烷单元的聚硅氧烷单元和由50至100摩尔％的芳基酯单元，小于50摩尔％的芳族碳酸酯单元，小于30摩尔％的间苯二酚碳酸酯组成的聚酯 - 聚碳酸酯单元单体和小于35摩尔％的双酚碳酸酯单元，其中硅氧烷单元以聚硅氧烷共聚物组合物总重量的0.2-10重量％的量存在于聚硅氧烷单元中，并且其中聚硅氧烷共聚物组合物具有2 小于或等于65千瓦 - 分钟/平方米（kW-min / m 2）的每分钟集成放热速率和小于65千瓦/平方米的峰值放热率（kW / 根据FAR F25.4的方法，根据联邦航空法规FAR 25.853（d）测量。还公开了一种包含聚硅氧烷共聚物组合物的飞机用窗构件。

6. 发明申请

US20050159577A1 Weatherable, thermostable polymers having improved flow composition 有权
标题翻译：具有改善流动组成的耐候性耐热聚合物
公开(公告)号：US20050159577A1
公开(公告)日：2005-07-21
申请号：US11025635
申请日：2004-12-29
申请人： Gary Davis , Brian Mullen , Paul Sybert
发明人： Gary Davis , Brian Mullen , Paul Sybert
IPC分类号： B32B27/06 , B32B27/08 , B32B27/18 , C08G63/19 , C08G63/64 , C08G63/676 , C08G63/695 , C08G63/79 , C08J7/04 , C09D167/03 , F02B61/04 , C08G64/00
CPC分类号： B32B27/365 , B32B27/06 , B32B27/08 , B32B27/20 , B32B27/283 , B32B27/36 , B32B2307/584 , B32B2307/71 , B32B2307/712 , B32B2419/00 , B32B2605/00 , C08F293/00 , C08G63/19 , C08G63/64 , C08G63/676 , C08G63/6956 , C08G63/79 , C08J7/047 , C08J2467/00 , C08J2469/00 , C08L53/00 , C08L2666/02 , C09D153/00 , C09D167/03 , C09J153/00 , F02B61/045 , Y10T428/31504 , Y10T428/31507
摘要： A copolymer composition comprises an arylate polyester unit, an aromatic carbonate unit, and a soft-block moiety, wherein individual occurrences of the soft block moiety are linked by a spacer unit comprising one or more of the arylate polyester units, one or more of the aromatic carbonate units, or a combination comprising each of these. In one embodiment, a soft block moiety comprises a polysiloxane unit. A film of the composition has a percent transmittance of greater than or equal to 60% as determined according to ASTM D1003-00. A method of forming a copolymer composition is disclosed, comprising substantially forming the bis-haloformates of a dihydroxy compound comprising an arylate polyester unit, and a dihydroxy compound comprising a soft-block moiety, and reacting the bis haloformates with a dihydroxy aromatic compound.
摘要翻译：共聚物组合物包含芳基化聚酯单元，芳族碳酸酯单元和软嵌段部分，其中软嵌段部分的单独出现由包含一个或多个芳基化聚酯单元的间隔单元连接，一个或多个芳族碳酸酯单元，或包含这些中的每一个的组合。在一个实施方案中，软嵌段部分包含聚硅氧烷单元。根据ASTM D1003-00测定，该组合物的透光率百分比大于或等于60％。公开了一种形成共聚物组合物的方法，其包括基本上形成包含芳基化聚酯单元的二羟基化合物的双卤代甲酸酯和包含软嵌段部分的二羟基化合物，并使双卤代甲酸酯与二羟基芳族化合物反应。

7. 发明授权

US07709581B2 Polycarbonate-polysiloxane copolymer compositions and articles formed therefrom 有权
标题翻译：聚碳酸酯 - 聚硅氧烷共聚物组合物和由其形成的制品
公开(公告)号：US07709581B2
公开(公告)日：2010-05-04
申请号：US11537056
申请日：2006-09-29
申请人： Katherine Glasgow , Jan-Pleun Lens , Brian Mullen , Vandita Pai-Paranjape
发明人： Katherine Glasgow , Jan-Pleun Lens , Brian Mullen , Vandita Pai-Paranjape
IPC分类号： C08L69/00 , C08G81/00
CPC分类号： C08G77/448 , C08L83/10
摘要： A thermoplastic composition comprises a copolycarbonate comprising 25 to 100 mole percent of a first carbonate unit derived from a dihydroxy aromatic compound having the formula wherein Ra′ and Rb′ are C1-12 alkyl, T is a C5-16 cycloalkylene, a C5-16 cylcloalkylidene, a C1-5 alkylene, a C1-5 alkylidene, a C6-13 arylene, a C7-12 arylalkylene, C7-12 arylalkylidene, a C7-12 alkylarylene, or a C7-12 arylenealkyl, and r and s are each independently 1 to 4, and r and s are 1 to 4; and 0 to 75 mole percent of a second carbonate unit, wherein the first carbonate unit and second carbonate unit are not identical; a polysiloxane-polycarbonate copolymer comprising 0.15 to 30 weight percent of a polysiloxane block comprising siloxane units of the formula wherein E is on average of 4 to 60 units, and 70 to 99.85 weight percent of a third carbonate unit, wherein an article having a thickness of 3.2 mm and molded from the thermoplastic composition has a Dynatup total energy of greater than 50 Joules, as measured at a constant speed of 3.3 to 3.6 m/sec at 23° C. according to ASTM D3763-02. A method of making and articles prepared therefrom are also disclosed.
摘要翻译：热塑性组合物包括共聚碳酸酯，其包含25至100摩尔％的衍生自具有下式的二羟基芳族化合物的第一碳酸酯单元：其中R a'和R b'为C 1-12烷基，T为C 5-6亚环烷基，C 5-16 C 1 -C 5亚烷基，C 1-5亚烷基，C 6-13亚芳基，C 7-12芳基亚烷基，C 7-12芳烷基亚烷基，C 7-12烷基亚芳基或C 7-12亚芳基烷基，r和s分别为独立地1至4，r和s为1至4; 和0至75摩尔％的第二碳酸酯单元，其中所述第一碳酸酯单元和第二碳酸酯单元不相同; 聚硅氧烷 - 聚碳酸酯共聚物，其包含0.15至30重量％的包含下式的硅氧烷单元的聚硅氧烷嵌段，其中E平均为4至60个单元，和70至99.85重量％的第三个碳酸酯单元，其中具有厚度根据ASTM D3763-02，由热塑性组合物模塑的Dynatup总能量大于50焦耳，其在23℃下以3.3至3.6m /秒的恒定速度测量。还公开了一种制备方法和由其制备的制品。

8. 发明授权

US07671169B2 Polycarbonate-polyester block copolymer compositions, methods, and articles 有权
标题翻译：聚碳酸酯 - 聚酯嵌段共聚物组合物，方法和制品
公开(公告)号：US07671169B2
公开(公告)日：2010-03-02
申请号：US11755817
申请日：2007-05-31
申请人： Brian Mullen , Tara Mullen
发明人： Brian Mullen , Tara Mullen
IPC分类号： C08G63/00 , C08G64/00
CPC分类号： C08G63/64 , C08G63/08 , C08G63/823 , C08G63/912 , C08G64/18 , C08G2261/126 , C08L69/00 , C08L69/005 , C08L2666/18
摘要： A polycarbonate-polyester block copolymer includes a polycarbonate block and a polyester block, each having specific structures. The block copolymer can be prepared, at least in part, from renewable feedstocks. In some forms, the block copolymer includes biodegradable segments that facilitate structural breakdown of objects molded from the block copolymer. Methods of preparing the block copolymer are described as are compositions that include it and articles prepared from it.
摘要翻译：聚碳酸酯 - 聚酯嵌段共聚物包括具有特定结构的聚碳酸酯嵌段和聚酯嵌段。该嵌段共聚物可至少部分由可再生原料制备。在一些形式中，嵌段共聚物包括促进由嵌段共聚物模制的物体的结构分解的可生物降解的链段。制备嵌段共聚物的方法描述为包括它的组合物和由其制备的制品。

9. 发明申请

US20090119979A1 CATALYSTS FOR PRODUCTION OF BIODIESEL FUEL AND GLYCEROL 审中-公开
标题翻译：生物柴油燃料和甘油的生产催化剂
公开(公告)号：US20090119979A1
公开(公告)日：2009-05-14
申请号：US11937271
申请日：2007-11-08
申请人： Brian Mullen
发明人： Brian Mullen
IPC分类号： C10L1/18 , C01B21/082 , C01B25/02
CPC分类号： C11C3/003 , B01J31/0239 , B01J31/0268 , B01J2231/49 , C10G2300/1011 , C10L1/026 , C10L1/19 , Y02E50/13 , Y02P30/20
摘要： A method of producing biodiesel through the trans-esterification of a triglyceride, comprising mixing a triglyceride, an alcohol, and a catalyst to form a mixture, where said catalyst is non-metal quaternary ammonium hydroxide or non-metal quaternary phosphonium hydroxide, removing volatile components from said mixture, and allowing the remaining mixture to separate into a biodiesel-rich layer and a glycerol-rich layer.
摘要翻译：通过甘油三酯的酯交换生产生物柴油的方法，包括将甘油三酯，醇和催化剂混合以形成混合物，其中所述催化剂是非金属季铵氢氧化物或非金属季铵氢氧化物，除去挥发性来自所述混合物的组分，并且允许剩余的混合物分离成富含生物柴油层和富含甘油的层。

10. 发明授权

US07524919B2 Polycarbonate-polysiloxane copolymers, method of making, and articles formed therefrom 有权
标题翻译：聚碳酸酯 - 聚硅氧烷共聚物，制造方法和由其形成的制品
公开(公告)号：US07524919B2
公开(公告)日：2009-04-28
申请号：US11537135
申请日：2006-09-29
申请人： James Franklin Hoover , Jan-Pleun Lens , Brian Mullen
发明人： James Franklin Hoover , Jan-Pleun Lens , Brian Mullen
IPC分类号： C08G64/00 , C08G63/02
CPC分类号： C08G64/186 , C08G77/448 , C08L69/00 , C08L83/04 , Y10T428/31504 , Y10T428/31507 , C08L83/00 , C08L2666/18
摘要： A polycarbonate copolymer comprising90 to 100 mol % of units derived from a cyclohexylidene bisphenol of the formula wherein Ra′ and Rb′ are each independently C1-12 alkyl, T is a C5-16 cycloalkylene, a C5-16 cylcloalkylidene, a C1-5 alkylene, a C1-5 alkylidene, a C6-13 arylene, a C7-12 arylalkylene, C7-12 arylalkylidene, a C7-12 alkylarylene, or a C7-12 arylenealkyl, and r and s are each independently 1 to 4; 2 to 35 wt % of units derived from a polysiloxane diol of the formulas or a combination thereof, wherein Ar is a substituted or unsubstituted C6-36 arylene group, each R is the same or different C1-13 monovalent organic group, each R6 is the same or different divalent C1-C30 organic group, and E is an integer from 2 to 100; and 0 to 10 mol % of units derived from a dihydroxy aromatic compound of formula (3) wherein Ra and Rb are each independently halogen, p and q are each independently integers of 0 to 4, and the dihydroxy aromatic compound of formula (3) is not the same as the cyclohexylidene bisphenol or the polysiloxane diols.
摘要翻译：一种聚碳酸酯共聚物，其包含90-100摩尔％的衍生自下式的亚环己基双酚的单元：其中Ra'和Rb'各自独立地为C1-12烷基，T为C5-16亚环烷基，C5-16亚烷基亚烷基，C1- 5亚烷基，C 1-5亚烷基，C 6-13亚芳基，C 7-12芳基亚烷基，C 7-12芳烷基亚烷基，C 7-12烷基亚芳基或C 7-12亚芳基烷基，r和s各自独立地为1至4; 2〜35重量％衍生自下式的聚硅氧烷二醇或其组合的单元，其中Ar为取代或未取代的C 6〜36亚芳基，各R为相同或不同的C 1-11一价有机基团，各R6为相同或不同的二价C1-C30有机基团，E为2至100的整数; 和0〜10摩尔％的衍生自式（3）的二羟基芳族化合物的单元，其中Ra和Rb各自独立地为卤素，p和q各自独立地为0至4的整数，并且式（3）的二羟基芳族化合物与亚环己基双酚或聚硅氧烷二醇不同。

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