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1. 发明授权

US5965671A Modified phenolic resin toughened by poly (alkylene oxide) and preparation thereof 失效
标题翻译：通过聚（环氧烷）增韧的改性酚醛树脂及其制备
公开(公告)号：US5965671A
公开(公告)日：1999-10-12
申请号：US35486
申请日：1998-03-05
申请人： Chen-Chi Martin Ma , Hew-Der Wu , Chih-Tsung Lee
发明人： Chen-Chi Martin Ma , Hew-Der Wu , Chih-Tsung Lee
IPC分类号： C08G65/331 , C08L71/02 , G08G65/32
CPC分类号： C08G65/3317 , C08L71/02
摘要： Modified resole and novolac type phenolic resins which are toughened by poly(alkylene oxide) are disclosed. The modified resole type phenolic resin is prepared by the following steps: mixing a poly(alkylene oxide) having a weight average molecular weight of 100,000.about.8,000,000 and phenol in a weight ratio of poly(alkylene oxide): phenol=1.5:1.about.1:1 at an elevated temperature to form a glutinous mixture; mixing the glutinous mixture with an acid catalyst to obtain a viscous mixture having a relatively low viscosity compared to the glutinous mixture; and mixing the viscose mixture with a resole type phenolic resin. The modified novolac type phenolic resin is prepared by directly mixing the glutinous mixture with a liquid novolac type phenolic resin. The amount of the poly(alkylene oxide) mixed is 2.about.10 wt % based on the phenolic resin.
摘要翻译：公开了通过聚（环氧烷）增韧的改性甲阶酚醛树脂和酚醛清漆型酚醛树脂。通过以下步骤制备改性甲阶酚醛树脂：将聚（环氧烷）：苯酚= 1.5:1的重量比混合重均分子量为100,000,000,000,000,000,000的聚（环氧烷烃）：1在升高的温度下形成糯混合物; 将糯混合物与酸催化剂混合以获得与糯混合物相比具有相对低粘度的粘性混合物; 并将粘胶混合物与酚醛树脂酚醛树脂混合。通过将糯混合物与液体酚醛清漆型酚醛树脂直接混合来制备改性酚醛清漆型酚醛树脂。混合的聚（环氧烷）的量相对于酚醛树脂为2％（重量）。

2. 发明授权

US07955654B2 Method of preparation of a MWCNT/polymer composite having electromagnetic interference shielding effectiveness 有权
标题翻译：具有电磁干扰屏蔽效能的MWCNT /聚合物复合材料的制备方法
公开(公告)号：US07955654B2
公开(公告)日：2011-06-07
申请号：US12081517
申请日：2008-04-17
申请人： Chen-Chi Martin Ma , Siu-Ming Yuen , Chia-Yi Chuang , Kuo-Chi Yu , Sheng Yen Wu
发明人： Chen-Chi Martin Ma , Siu-Ming Yuen , Chia-Yi Chuang , Kuo-Chi Yu , Sheng Yen Wu
IPC分类号： B05D3/02
CPC分类号： H05K9/0092 , B82Y30/00 , C08J5/005 , C08J7/047 , C08J2300/12 , C08J2333/12 , C08J2367/02 , C08J2433/00
摘要： A method of preparing carbon nanotube/polymer composite having electromagnetic interference (EMI) shielding effectiveness is disclosed, which includes: dispersing multi-walled carbon nanotubes (MWCNT) in an organic solvent such as N,N-Dimethylacetamide (DMAc); dissolving monomers such as methyl methacrylate (MMA) and an initiator such as 2,2-azobisisobutyronitrile (AIBN) in the MWCNT dispersion; and polymerizing the monomers in the resulting mixture at an elevated temperature such as 120° C. to form a MWCNT/PMMA composite. The composite is coated onto a PET film, and the coated PET film alone or a stack of multiple coated PET films can be applied as an EMI shielding material.
摘要翻译：公开了一种制备具有电磁干扰（EMI）屏蔽效能的碳纳米管/聚合物复合材料的方法，其包括：将多壁碳纳米管（MWCNT）分散在有机溶剂如N，N-二甲基乙酰胺（DMAc）中; 在MWCNT分散体中溶解单体如甲基丙烯酸甲酯（MMA）和引发剂如2,2-偶氮二异丁腈（AIBN）; 并在升高的温度如120℃下将所得混合物中的单体聚合以形成MWCNT / PMMA复合材料。复合材料涂覆在PET膜上，单独涂覆的PET膜或多层涂覆的PET膜的堆叠可以用作EMI屏蔽材料。

3. 发明授权

US07883650B2 Fabrication of carbon nanotubes reinforced polymer composite bipolar plates for fuel cell 有权
标题翻译：用于燃料电池的碳纳米管增强聚合物复合双极板的制造
公开(公告)号：US07883650B2
公开(公告)日：2011-02-08
申请号：US12289046
申请日：2008-10-20
申请人： Chen-Chi Martin Ma , Chih-Hung Hung , Shu-Hang Liao , Chuan-Yu Yen , Jeng-Chih Weng , Yu-Feng Lin
发明人： Chen-Chi Martin Ma , Chih-Hung Hung , Shu-Hang Liao , Chuan-Yu Yen , Jeng-Chih Weng , Yu-Feng Lin
IPC分类号： C04B35/00
CPC分类号： H01B1/24 , H01M8/0213 , H01M8/0221 , H01M8/0226 , Y10S977/745 , Y10S977/748
摘要： A composite bipolar plate for a polymer electrolyte membrane fuel cell (PEMFC) is prepared as follows: a) compounding vinyl ester and graphite powder to form bulk molding compound (BMC) material, the graphite powder content ranging from 60 wt % to 95 wt % based on the total weight of the graphite powder and vinyl ester, wherein carbon nanotubes together with a polyether amine dispersant or modified carbon nanotubes 0.05-10 wt %, based on the weight of the vinyl ester resin, are added during the compounding; b) molding the BMC material from step a) to form a bipolar plates having a desired shaped at 80-200° C. and 500-4000 psi.
摘要翻译：用于聚合物电解质膜燃料电池（PEMFC）的复合双极板如下制备：a）将乙烯基酯和石墨粉末混合以形成本体模塑料（BMC）材料，石墨粉末含量为60重量％至95重量％基于石墨粉末和乙烯基酯的总重量，其中在配混期间加入碳纳米管与聚醚胺分散剂或基于乙烯基酯树脂重量0.05-10重量％的改性碳纳米管; b）将步骤a）中的BMC材料模制成在80-200℃和500-4000psi下具有所需成形的双极板。

4. 发明申请

US20080242785A1 TiO2-coated CNT, TiO2-coated CNT reinforced polymer composite and methods of preparation thereof 审中-公开
标题翻译： TiO 2涂覆的CNT，TiO 2涂覆的CNT增强聚合物复合材料及其制备方法
公开(公告)号：US20080242785A1
公开(公告)日：2008-10-02
申请号：US11812405
申请日：2007-06-19
申请人： Chen-Chi Martin Ma , Siu-Ming Yuen , Chia-Yi Chuang
发明人： Chen-Chi Martin Ma , Siu-Ming Yuen , Chia-Yi Chuang
IPC分类号： C08L23/02 , B29D22/00
CPC分类号： C08J5/005 , B82Y30/00 , C08J2363/00 , C08K9/02 , C08L63/00 , Y10T428/13 , Y10T428/249948 , C08L2666/54
摘要： A method of preparing carbon nanotube/polymer composite is disclosed, which includes: forming a layer of TiO2 on carbon nanotubes (CNTs) with a precursor of TiO2 by a sol-gel or hydrothermal method, a weight ratio of the TiO2 precursor to CNT being 0.3:1 to 30:1; modifying the TiO2-coated CNTs with a coupling agent to improve the affinity thereof to a polymer; and mixing a polymer with the resulting modified TiO2-coated CNTs to form a TiO2-coated CNT reinforced polymer composite. The mechanical properties of the polymer composite can be enhanced by using an additional fiber reinforcement material.
摘要翻译：公开了一种制备碳纳米管/聚合物复合材料的方法，其包括：在具有TiO 2前体的碳纳米管（CNT）上通过溶胶形成一层TiO 2 凝胶或水热法，TiO 2前体与CNT的重量比为0.3:1至30:1; 用偶联剂改性TiO 2 2涂层的CNT以提高其对聚合物的亲和力; 并将聚合物与所得改性的TiO 2涂层CNT混合以形成TiO 2纳层CNT增强聚合物复合材料。聚合物复合材料的机械性能可以通过使用额外的纤维增强材料来提高。

5. 发明申请

US20100154871A1 Composite substrate for counter electrode of dye-sensitized solar cell 有权
标题翻译：染料敏化太阳能电池对电极复合基片
公开(公告)号：US20100154871A1
公开(公告)日：2010-06-24
申请号：US12588379
申请日：2009-10-14
申请人： Chen-Chi Martin Ma , Chuan-Yu Yen , Shu-Hang Liao , Ming-Yu Yen , Min-Chien Hsiao
发明人： Chen-Chi Martin Ma , Chuan-Yu Yen , Shu-Hang Liao , Ming-Yu Yen , Min-Chien Hsiao
IPC分类号： H01L31/02 , C08J5/00 , B29B13/00
CPC分类号： H01G9/2022 , B82Y10/00 , B82Y30/00 , C08J3/203 , C08J5/005 , C08J5/04 , C08J2367/02 , H01G9/2031 , H01G9/2059 , H01L51/444 , Y02E10/542
摘要： A substrate for counter electrode of dye-sensitized solar cell is made of a composite material, which is prepared by: a) compounding vinyl ester and graphite powder to form bulk molding compound (BMC) material, the graphite powder content ranging from 60 wt % to 95 wt % based on the total weight of the graphite powder and vinyl ester, wherein 0.01-10 wt % of an electrically conductive filler, based on the weight of the vinyl ester resin, is optionally added during the compounding; b) molding the BMC material from step a) to form a substrate for the counter electrode having a desired shaped at 80-200° C. and 500-4000 psi.
摘要翻译：染料敏化太阳能电池对电极基板由复合材料制成，该复合材料通过以下方法制备：a）将乙烯基酯和石墨粉末复合以形成批量模塑料（BMC）材料，石墨粉末含量为60wt％相对于石墨粉末和乙烯基酯的总重量为95重量％，其中在配混期间任选加入基于乙烯基酯树脂重量的0.01-10重量％的导电填料; b）从步骤a）模制BMC材料，以形成在80-200℃和500-4000psi下具有所需成型的对电极的基材。

6. 发明申请

US20100127424A1 Fabrication of metal meshes/carbon nanotubes/polymer composite bipolar plates for fuel cell 审中-公开
标题翻译：用于燃料电池的金属网/碳纳米管/聚合物复合双极板的制造
公开(公告)号：US20100127424A1
公开(公告)日：2010-05-27
申请号：US12457353
申请日：2009-06-09
申请人： Chen-Chi Martin Ma , Min-Chien Hsiao , Shu-Hang Liao , Ming-Yu Yen , Chaun-Yu Yen , Jeng-Chin Weng , Shuo-Jen Lee
发明人： Chen-Chi Martin Ma , Min-Chien Hsiao , Shu-Hang Liao , Ming-Yu Yen , Chaun-Yu Yen , Jeng-Chin Weng , Shuo-Jen Lee
IPC分类号： B29C51/42
CPC分类号： H01M8/0234 , H01M8/0239 , H01M8/0243 , H01M2008/1095
摘要： A reinforced mesh structure containing bipolar plate for a polymer electrolyte membrane fuel cell (PEMFC) is prepared as follows: a) compounding vinyl ester and graphite powder to form bulk molding compound (BMC) material, the graphite powder content ranging from 60 wt % to 95 wt % based on the total weight of the graphite powder and vinyl ester, wherein 0.05-10 wt % reactive carbon nanotubes modified by acyl chlorination-amidization reaction, based on the weight of the vinyl ester resin, are added during the compounding; b) molding the BMC material from step a) with a metallic net being embedded in the molded BMC material to form a bipolar plates having a desired shaped at 80-200° C. and 500-4000 psi.
摘要翻译：含有用于聚合物电解质膜燃料电池（PEMFC）的双极板的增强网格结构如下制备：a）将乙烯基酯和石墨粉末混合以形成本体模塑料（BMC）材料，石墨粉末含量范围为60wt％至基于石墨粉末和乙烯基酯的总重量为95重量％，其中在配混期间加入基于乙烯基酯树脂的重量，通过酰基氯化酰胺化反应改性的0.05-10重量％的反应性碳纳米管; b）将来自步骤a）的BMC材料模制成金属网嵌入到模制的BMC材料中以形成在80-200℃和500-4000psi下具有所需成形的双极板。

7. 发明授权

US07378484B2 Toughness-increased phenolic resin and preparation thereof 有权
标题翻译：韧性增加的酚醛树脂及其制备
公开(公告)号：US07378484B2
公开(公告)日：2008-05-27
申请号：US11094176
申请日：2005-03-31
申请人： Jeng-Chang Yang , Chen-Chi Martin Ma , Hon-Bin Chen , Chin-Yih Chen
发明人： Jeng-Chang Yang , Chen-Chi Martin Ma , Hon-Bin Chen , Chin-Yih Chen
IPC分类号： C08G8/02 , C08G8/00
CPC分类号： C08G8/28
摘要： A phenolic resin that increases its toughness by polydimethylsiloxane and a process of preparing the same is provided. Polydimethylsiloxane is added as a coupling agent in a γ-glycidoxypropyltrimethoxysilane-modified phenolic resin to improve the compatibility between polydimethylsiloxane and the phenolic resin. Then, tetraethoxysilane is added to conduct hydrolysis condensation and obtain tougher and thermally stable phenolic resin.
摘要翻译：提供了一种通过聚二甲基硅氧烷增加其韧性的酚醛树脂及其制备方法。将聚二甲基硅氧烷作为偶联剂加入到γ-环氧丙氧基丙基三甲氧基硅烷改性酚醛树脂中，以改善聚二甲基硅氧烷和酚醛树脂之间的相容性。然后加入四乙氧基硅烷进行水解缩合，得到更坚韧，热稳定的酚醛树脂。

8. 发明授权

US06841646B2 Process for preparing poly(urea-urethane) 有权
标题翻译：制备聚（尿素 - 氨基甲酸酯）
公开(公告)号：US06841646B2
公开(公告)日：2005-01-11
申请号：US10453649
申请日：2003-06-04
申请人： Jeng-Cheng Yang , Chen-Chi Martin Ma , Hon-Bin Chen , Chin-Yih Chen
发明人： Jeng-Cheng Yang , Chen-Chi Martin Ma , Hon-Bin Chen , Chin-Yih Chen
IPC分类号： C08G18/10 , C08G18/61 , C08G18/32
CPC分类号： C08G18/61 , C08G18/10 , C08G18/348 , C08G18/3228 , C08G18/3206
摘要： A poly(urea-ureathane) based on polydimethyl siloxane is prepared by reacting an amino-terminated polydimethyl siloxane with polyisocyanate to form a prepolymer of poly(urea-urethane), and reacting the prepolymer and a chain extender in the presence of a catalyst. The resulting poly(urea-urethane) contains about 5-65 wt % of hard segments, and has a surface resistance of about 10-150 MΩ at high relative humidity, so that it can be used in anti-static electricity and electrostatic discharge shielding.
摘要翻译：通过使氨基封端的聚二甲基硅氧烷与多异氰酸酯反应以形成聚（脲 - 氨基甲酸酯）的预聚物，并在催化剂存在下使预聚物和扩链剂反应，制备基于聚二甲基硅氧烷的聚（脲 - 脲）。所得的聚（尿素 - 氨基甲酸酯）含有约5-65重量％的硬链段，并且在高相对湿度下具有约10-150摩尔％的表面电阻，因此可用于抗静电和静电放电屏蔽。

9. 发明授权

US09202635B2 Composite substrate for counter electrode of dye-sensitized solar cell 有权
标题翻译：染料敏化太阳能电池对电极复合基片
公开(公告)号：US09202635B2
公开(公告)日：2015-12-01
申请号：US12588379
申请日：2009-10-14
申请人： Chen-Chi Martin Ma , Chuan-Yu Yen , Shu-Hang Liao , Ming-Yu Yen , Min-Chien Hsiao
发明人： Chen-Chi Martin Ma , Chuan-Yu Yen , Shu-Hang Liao , Ming-Yu Yen , Min-Chien Hsiao
IPC分类号： H01L31/02 , H01G9/20 , B82Y10/00 , B82Y30/00 , C08J3/20 , C08J5/00 , C08J5/04 , H01L51/44
CPC分类号： H01G9/2022 , B82Y10/00 , B82Y30/00 , C08J3/203 , C08J5/005 , C08J5/04 , C08J2367/02 , H01G9/2031 , H01G9/2059 , H01L51/444 , Y02E10/542
摘要： A substrate for counter electrode of dye-sensitized solar cell is made of a composite material, which is prepared by: a) compounding vinyl ester and graphite powder to form bulk molding compound (BMC) material, the graphite powder content ranging from 60 wt % to 95 wt % based on the total weight of the graphite powder and vinyl ester, wherein 0.01-10 wt % of an electrically conductive filler, based on the weight of the vinyl ester resin, is optionally added during the compounding; b) molding the BMC material from step a) to form a substrate for the counter electrode having a desired shaped at 80-200° C. and 500-4000 psi.
摘要翻译：染料敏化太阳能电池对电极基板由复合材料制成，该复合材料通过以下方法制备：a）将乙烯基酯和石墨粉末复合以形成批量模塑料（BMC）材料，石墨粉末含量为60wt％相对于石墨粉末和乙烯基酯的总重量为95重量％，其中在配混期间任选加入基于乙烯基酯树脂重量的0.01-10重量％的导电填料; b）从步骤a）模制BMC材料，以形成在80-200℃和500-4000psi下具有所需成型的对电极的基材。

10. 发明申请

US20100136327A1 Method of preparation of a MWCNT/polymer composite having electromagnetic interference shielding effectiveness 审中-公开
标题翻译：具有电磁干扰屏蔽效能的MWCNT /聚合物复合材料的制备方法
公开(公告)号：US20100136327A1
公开(公告)日：2010-06-03
申请号：US12654331
申请日：2009-12-17
申请人： Chen-Chi Martin Ma , Siu-Ming Yuen , Chia-Yi Chuang , Kuo-Chi Yu , Sheng Yen Wu
发明人： Chen-Chi Martin Ma , Siu-Ming Yuen , Chia-Yi Chuang , Kuo-Chi Yu , Sheng Yen Wu
IPC分类号： B32B27/00 , C07C53/00 , C07C43/03 , C08K3/04 , B05D3/00 , B32B38/00 , B05D5/12
CPC分类号： C08J7/047 , B82Y30/00 , C08J5/005 , C08J2367/02 , C08J2433/00 , H05K9/0092 , Y10T428/263 , Y10T428/264
摘要： The present invention provides a modified carbon nanotube having —C(O)—R′ or —C(O)—R—COOH covalently bounded to a surface of carbon nanotube, wherein R′ is C1-C26 alkyl or C2-C26 alkenyl, and R is C1-C26 alkylene or C2-C26 alkenylene. The present invention also discloses a carbon nanotubes/polymer composite having electromagnetic interference shielding effectiveness, which contains 0.1-10% of modified carbon nanotubes, based on the weight of the polymer. The present invention further provides methods for preparing the modified carbon nanotubes and the composite.
摘要翻译：本发明提供了具有与碳纳米管表面共价结合的-C（O）-R'或-C（O）-R-COOH的改性碳纳米管，其中R'为C 1 -C 26烷基或C 2 -C 26烯基，且R为C 1 -C 26亚烷基或C 2 -C 26亚烯基。本发明还公开了一种具有电磁干扰屏蔽效能的碳纳米管/聚合物复合材料，其基于聚合物的重量含有0.1-10％的改性碳纳米管。本发明还提供了制备改性碳纳米管和复合材料的方法。

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