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    • 2. 发明授权
    • Apparatus and method for matrix coating fibres with metal vapour
    • 用金属蒸气基质涂覆纤维的装置和方法
    • US6129951A
    • 2000-10-10
    • US142086
    • 1998-09-01
    • Charles M. Ward-CloseLakshman Chandrasekaran
    • Charles M. Ward-CloseLakshman Chandrasekaran
    • C23C14/56C23C14/24
    • C23C14/562
    • A physical vapour deposition apparatus for pre-coating fibres of a reinforcement material with a predetermined thickness of matrix metal prior to consolidation to yield a metal matrix composite material comprises: at least one evaporation crucible; a heater for heating a charge of metal in the at least one evaporation crucible to a temperature at which an appreciable vapour pressure is generated and a flux of metal vapour is evolved; a powered take-up device for drawing the reinforcement through the apparatus, and a guide mechanism for guiding the reinforcement repeatedly through the vapour flux, and to effect twisting of the reinforcement about its longitudinal axis after each successive pass through the vapour flux by an amount which is a fraction of 180.degree.. The guide mechanism comprises a pair of multi-pass transfer rollers each having a multiplicity of concentric fibre-receiving grooves formed on its surface. The transfer rollers are positioned above the evaporation crucible or crucibles and spaced apart from each other with their rotational axes parallel. At least one of the transfer rollers comprises a plurality of independently-rotatable sub-rollers.
    • PCT No.PCT / GB97 / 00793 Sec。 371日期:1998年9月1日 102(e)1998年9月1日PCT 1997年3月24日PCT公布。 第WO94 / 36021号公报 日期1997年10月2日用于在固结之前预先涂覆具有预定厚度的基质金属的增强材料的纤维以产生金属基质复合材料的物理气相沉积设备包括:至少一个蒸发坩埚; 加热器,用于将所述至少一个蒸发坩埚中的金属电荷加热到产生明显的蒸汽压的温度和金属蒸汽的流量; 用于通过该装置拉伸加强件的动力收紧装置和用于通过蒸气通量反复引导加强件的引导机构,并且在每次连续通过蒸气通量之后使加强件围绕其纵向轴线扭转一定量 这是180度的分数。 引导机构包括一对多遍转印辊,每个多遍转印辊在其表面上形成有多个同心光纤接收槽。 转印辊位于蒸发坩埚或坩埚上方并且彼此间隔开并且其旋转轴线平行。 至少一个转印辊包括多个可独立旋转的副辊。
    • 4. 发明授权
    • Titanium-based alloy produced by vapor quenching
    • 通过气相淬火制备的钛基合金
    • US5421917A
    • 1995-06-06
    • US107843
    • 1993-10-12
    • Peter G. PartridgeCharles M. Ward-Close
    • Peter G. PartridgeCharles M. Ward-Close
    • C22C1/00C22C14/00C22C45/10C23C14/16C23C14/30C22C21/00
    • C23C14/30C22C1/00C22C14/00C22C45/10C23C14/16
    • An alloy based on titanium and containing 0.5 to 30% by weight of magnesium, calcium or lithium is produced by vapor quenching to yield a metastable solid solution of solute in titanium. Exemplified alloys containing magnesium have age hardening or solution strengthening characteristics. Vapor quenching enables these alloys to be produced despite the differences in melting temperature between solute and solvent by separate vaporization of each of the species and mixing in the vapor phase. This method provides a route to achieving rapid solidification microstructures unobtainable by other rapid solidification methods. Preferred alloys comprise Ti with 1-15% or 3-7% by weight of magnesium. The alloys may contain other strengthening ingredients currently used in titanium alloys.
    • PCT No.PCT / GB92 / 00326 Sec。 371日期:1993年10月12日 102(e)日期1993年10月12日PCT提交1992年2月24日PCT公布。 出版物WO92 / 14852 日本9月3日,1992年。通过气相淬火产生基于钛并含有0.5至30重量%镁,钙或锂的合金,以产生固溶于钛的亚稳固溶体。 含镁的示例合金具有时效硬化或溶液强化特性。 蒸气淬火使得这些合金能够生产,尽管溶质和溶剂之间的熔融温度的差异通过单个蒸发每种物质并在气相中混合而产生。 该方法提供了通过其他快速固化方法获得的快速凝固微结构的途径。 优选的合金包括具有1-15%或3-7重量%镁的Ti。 合金可能含有目前用于钛合金的其他强化成分。
    • 5. 发明授权
    • Method of making precursors and articles of ceramic-reinforced metal
matrix composites
    • 制备陶瓷增强金属基复合材料前体和制品的方法
    • US5378500A
    • 1995-01-03
    • US25382
    • 1993-03-02
    • Charles M. Ward-ClosePeter G. Partridge
    • Charles M. Ward-ClosePeter G. Partridge
    • B22F7/06C22C47/00C22C47/02C22C47/04C22C47/06C22C47/14C23C14/18C23C16/06D04H1/42C23C16/00
    • C23C16/06C22C47/04C22C47/14C23C14/18D04H1/42Y02T50/67
    • Precursors for metal matrix composites are produced by coating a long fibre ceramic reinforcement with alternating layers of dissimilar species of matrix materials to an aggregate thickness sufficient to yield the intended matrix volume fraction in a consolidated product without additional material. This duplex coating of fibres is performed by vapor phase deposition comprising vapor condensation, sputtering or chemical vapor reaction. The precursor includes an aggregate coating of at least 5% of fibre diameter, preferably at least 20%. Various duplex systems are disclosed, each having one component significantly more frangible than the other to render damage tolerant properties to the resultant metal composite.Product materials are produced from the duplex matrix coated fibres by consolidation of an assembly of coated fibres under conditions of elevated temperature and pressure to cause inter-fibre matrix flow and bonding of matrix materials.
    • 金属基质复合材料的前体是通过将具有交替的不同种类的基质材料的交替层的长纤维陶瓷增强材料涂覆到足以在没有附加材料的情况下产生固结产品中的预期基体体积分数的骨料厚度来制备的。 纤维的这种双相涂层通过包括蒸气冷凝,溅射或化学气相反应的气相沉积进行。 前体包括纤维直径的至少5%,优选至少20%的聚集体涂层。 公开了各种双相系统,每个具有一个组分比另一组分明显更易破碎,以使所得金属复合材料具有耐损伤性能。 通过在升高的温度和压力的条件下固化涂覆的纤维的组件以产生纤维间基质流动和基质材料的结合,从双重基质涂覆的纤维生产产品材料。