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    • 8. 发明授权
    • Ion sputter removal from thin microscopy samples with ions extracted from an RF generated plasma
    • 从RF产生的等离子体中提取离子从薄型显微镜样品中离子溅射去除
    • US08288737B1
    • 2012-10-16
    • US12108353
    • 2008-04-23
    • Scott D. Walck
    • Scott D. Walck
    • G21K5/08
    • H01J37/32082H01J37/20H01J2237/2007H01J2237/31745
    • A plasma system for changing a microscopy material sample comprises a microscopy material sample holder for holding a microscopy material sample in place in a desired orientation, and a receptacle holder for receiving the sample holder and an RF antenna. The microscopy sample is positioned relative to the antenna so that no point on the antenna is in direct line-of-sight contact with the microscopy sample. This feature of avoiding direct line-of-sight contact between the antenna and the sample assists in preventing, or at least minimizing, ion sputtering of system component material onto the specimen or sample 10 that is being trimmed. Moreover, portions of the system which are in direct line-of-sight contact with the sample are comprised of material having a low sputtering yield, preferably carbon. The material may comprise graphite, and may be in the form of a carbon coating or a carbon paint.
    • 用于改变显微镜材料样品的等离子体系统包括用于将显微镜材料样品保持在期望取向的显微镜材料样品保持器,以及用于接收样品架和RF天线的容器保持器。 显微镜样品相对于天线定位,使得天线上的任何点与显微镜样品直接接触。 避免天线和样品之间的直接视线接触的这一特征有助于防止或至少最小化将系统组分材料离子溅射到待修剪的样品或样品10上。 此外,与样品直接视线接触的系统的部分由具有低溅射产率,优选碳的材料构成。 该材料可以包括石墨,并且可以是碳涂层或碳涂料的形式。
    • 10. 发明授权
    • Specimen preservation systems and methods
    • 标本保存系统和方法
    • US07723701B1
    • 2010-05-25
    • US11495294
    • 2006-07-28
    • Scott D. Walck
    • Scott D. Walck
    • G01F23/00G21K5/08G21K5/10B65D6/00B65D8/14
    • G01N1/28A01N1/0263B01L3/508B01L2200/141B01L2200/185B01L2300/049B01L2300/10B01L2300/14G01N1/44
    • A two-part container for preserving material samples during storage and transport is separable and can be sealed with the presence of an elastomeric O-ring and internal threads on each part of the container. In the configuration at which the threads first engage between the two halves of the container, there is a small hole in the outer top part just above the O-ring of the bottom mating part. When the two container parts are mated and the sealing O-ring is below the small hole, inert gas can be made to flow through an inlet valve, into the container, and out through the small hole. In this configuration, the inert gas flows through the container and purges the atmospheric gas, replacing it with inert gas. After a period of time, the two container parts are rotated so that the sealing O-ring moves above the small hole. This will stop the flow into and out of the container. After this, the gas inlet valve is closed to seal the inert gas in the container. After the valve is closed, the pressure in the container is increased by screwing the two parts of the container in relation to each other such that the volume of the container is decreased. Prior to opening, the efficacy of the container can be checked by releasing the gas while the container is in the compressed state.
    • 在储存和运输过程中用于保存材料样品的两部分容器是可分离的,并且可以在容器的每个部分上存在橡胶O形环和内螺纹的情况下被密封。 在螺纹首先接合在容器的两个半部之间的构型中,在外部顶部部分中恰好在底部配合部件的O形环上方的小孔。 当两个容器部件配合并且密封O形环位于小孔下面时,惰性气体可以通过入口阀流入容器,并通过小孔流出。 在这种结构中,惰性气体流过容器并清除大气气体,用惰性气体代替。 一段时间后,两个容器部分旋转,使得密封O形环在小孔上移动。 这将阻止流入和流出容器。 之后,气体入口阀关闭以密封容器中的惰性气体。 在关闭阀门之后,通过将容器的两部分相对于彼此拧紧以减小容器的容积,增加了容器中的压力。 在打开之前,可以通过在容器处于压缩状态时释放气体来检查容器的功效。