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1. 发明授权

US3641085A Oxidation of aluminum alkyls 失效
标题翻译：氧化铝的氧化
公开(公告)号：US3641085A
公开(公告)日：1972-02-08
申请号：US3641085D
申请日：1969-05-01
申请人： CONTINENTAL OIL CO
发明人： LUNDEEN ALLAN J , YATES JAMES E
IPC分类号： C07C29/54 , C07F5/06
CPC分类号： C07C29/54 , C07C31/125
摘要： IN THE OXIDATION OF ALUMINUM ALKYLS IN THE PREPARATION OF ALCHOLS VIA ALUMINUM CHEMISTRY, HIGHER QUALITY AND YIELDS OF DESIRED ALCHOL ARE OBTAINED IF THE RATE OF OXADATION IS MATERIALLY REDUCED WHEN THE OXYGEN IN THE OXIDATION REACTOR APPROACHES THE MAXIMUM ALLOWABLE AND CONTINUING THE OXIDATION TO SUBSTANTIAL COMPLETION AT THE LOWER RATE OF OXYGEN FLOW.

2. 发明授权

US3862994A Process for condensation of alcohols 失效
标题翻译：醇缩合方法
公开(公告)号：US3862994A
公开(公告)日：1975-01-28
申请号：US36769073
申请日：1973-06-06
申请人： CONTINENTAL OIL CO
发明人： YATES JAMES E
IPC分类号： C07C29/00 , C07C31/02
CPC分类号： Y10S585/906
摘要： A process for producing higher molecular weight alcohols by forming a reaction mixture of at least one lower molecular weight primary alkanol having a methylene group adjacent the hydroxylated carbon atom, an alkali catalyst and a palladium salt of a Beta -diketone, and heating the reaction mixture to effect condensation of the alkanol while simultaneously removing water as it forms.
摘要翻译：通过形成具有邻近羟基化碳原子的亚甲基的至少一种低分子量伯烷醇，β-二酮的碱金属催化剂和钯盐的反应混合物生产高分子量醇的方法，并加热反应混合物以实现链烷醇的缩合，同时在形成时除去水。

3. 发明授权

US3600417A Method of removing secondary aluminum alkoxides from primary aluminum alkoxides 失效
标题翻译：从主要的铝氧化物中除去二级的铝氧化物的方法
公开(公告)号：US3600417A
公开(公告)日：1971-08-17
申请号：US3600417D
申请日：1968-10-21
申请人： CONTINENTAL OIL CO
发明人： LUNDEEN ALLAN J , YATES JAMES E
IPC分类号： C07C29/54 , C07F5/06
CPC分类号： C07C29/54 , C07C31/12 , C07C31/125
摘要： A METHOD FOR REMOVING SECONDARY ALUMINUM ALKOXIDES FROM PRIMARY ALUMINUM ALKOXIDES BY HEATING A MIXTURE CONTAINING BOTH TYPES OF COMPOUNDS TO SELECTIVELY CONVERT THE SECONDARY ALKOXIDES TO OLEFINIC COMPOUNDS WITHOUT SUBSTANTIAL MOLECULAR CHANGE OF THE PRIMARY ALKOXIDE. THE METHOD IS FURTHER DEVELOPED TO EITHER REMOVE FROM THE MIXTURE, THE OLEFINIC PRODUCTS OF THERMAL DECOMPOSITION OF THE SECONDARY ALKOXIDES, OR, WHERE SUCH PRODUCTS ARE DERIVED FROM DIALUMINUM ALKOXIDES CONTAINING BOTH PRIMARY AND SECONDARY SUBSTITUTION OF THE ALKYL GROUP, TO HYDROLYZE THEM TO PRIMARY ALCOHOLS. IN EITHER PROCEDURE, THE STARTING MIXTURE IS IMPROVED AS A SOURCE MATERIAL OF ALCOHOL SULFATES USEFUL AS DETERGENTS.

4. 发明授权

US3916015A Process for condensation of alcohols 失效
标题翻译：醇缩合方法
公开(公告)号：US3916015A
公开(公告)日：1975-10-28
申请号：US52459974
申请日：1974-11-18
申请人： CONTINENTAL OIL CO
发明人： YATES JAMES E
IPC分类号： C07C29/34 , C07C29/00
CPC分类号： C07C29/34 , C07C31/125
摘要： A process for producing higher molecular weight alcohols by condensing at least one lower molecular weight primary alkanol having a methylene group adjacent the hydroxylated carbon atom in liquid phase in the presence of an alkali catalyst and an organic zinc compound, said alkali catalyst being an alkali metal alcoholate or a precursor thereof which forms the alcoholate in the reaction system and said organic zinc compound being defined by

WHEREIN R'', R'''' and R'''''' are each, independently, saturated or unsaturated, cyclic or acyclic, branch or straight chain hydrocarbon groups, while simultaneously removing water as it forms.
摘要翻译：一种通过在碱催化剂和有机锌化合物的存在下将具有邻近羟基化碳原子的亚甲基的至少一种低分子量伯烷醇缩合成液相来生产较高分子量醇的方法，所述碱催化剂是碱金属醇化物或其在反应体系中形成醇化物的前体，所述有机锌化合物由O PARALLEL [I]（R'-CO）2 Zn，OHR“PARALLEL” - [II]（R“-C = CO）2 Zn或[III]（R“' - SO 3）2 Zn WHEREIN R'，R”和R“'各自独立地为饱和或不饱和的，环状或非环状，支链或直链烃同时在形成时同时去除水分。

5. 发明授权

US3862993A Process for condensation of alcohols 失效
标题翻译：醇缩合方法
公开(公告)号：US3862993A
公开(公告)日：1975-01-28
申请号：US36768873
申请日：1973-06-06
申请人： CONTINENTAL OIL CO
发明人： YATES JAMES E , MOTZ KAYE L
IPC分类号： C07C31/02
摘要： A process for producing higher molecular weight alcohols by condensing at least one lower molecular weight primary alkanol having a methylene group adjacent the hydroxylated carbon atom at elevated temperatures in the presence of an alkali catalyst and a copper salt of a Beta -diketone while simultaneously removing water as it forms.
摘要翻译：通过在碱催化剂和β-二酮的铜盐的存在下，在升高的温度下将具有亚甲基的至少一种低分子量伯烷醇与β-二酮缩合而生成高分子量醇的方法，同时除去水因为它形成。

6. 发明授权

US3860664A Process for condensation of alcohols 失效
标题翻译：酒精浓缩方法
公开(公告)号：US3860664A
公开(公告)日：1975-01-14
申请号：US36768973
申请日：1973-06-06
申请人： CONTINENTAL OIL CO
发明人： YATES JAMES E
IPC分类号： C07C29/00 , C07C31/02
CPC分类号： Y10S585/906
摘要： A process for producing higher molecular weight alcohols by forming a reaction mixture of at least one lower molecular weight primary or secondary alkanol having a methylene group adjacent the hydroxylated carbon atom, an alkali catalyst and a palladium (II) compound, said palladium compound being mixed with the alkanol prior to dissolution of the alkali catalyst therein, and heating the reaction mixture to effect condensation of the alkanol while simultaneously removing water as it forms.
摘要翻译：通过形成至少一种具有邻近羟基化碳原子的亚甲基的低分子量伯或仲链烷醇，碱催化剂和钯（II）化合物的反应混合物来生产较高分子量醇的方法，所述钯化合物混合与烷醇溶解之前，碱催化剂在其中，并加热反应混合物以实现链烷醇的缩合，同时同时除去水形成。

7. 发明授权

US3917722A Process for condensation of alcohols 失效
标题翻译：醇缩合方法
公开(公告)号：US3917722A
公开(公告)日：1975-11-04
申请号：US52460074
申请日：1974-11-18
申请人： CONTINENTAL OIL CO
发明人： YATES JAMES E
IPC分类号： C07C29/34 , C07C29/00
CPC分类号： C07C29/34 , C07C31/125
摘要： A process for producing higher molecular weight alcohols by condensing at least one lower molecular weight primary alkanol having a methylene group adjacent the hydroxylated carbon atom in liquid phase in the presence of an alkali catalyst and an organic zinc compound, said alkali catalyst being an alkali metal alcoholate or a precursor thereof which forms the alcoholate in the reaction system and said organic zinc compound being defined by

WHEREIN R'', R'''' and R'''''' are each, independently, saturated or unsaturated, cyclic or acyclic, branch or straight chain hydrocarbon groups, while simultaneously removing water as it forms.
摘要翻译：一种通过在碱催化剂和有机锌化合物的存在下将具有邻近羟基化碳原子的亚甲基的至少一种低分子量伯烷醇缩合成液相来生产较高分子量醇的方法，所述碱催化剂是碱金属醇化物或其在反应体系中形成醇化物的前体，所述有机锌化合物由O-PARALLEL [I]（R'-CO）2 Zn，OHR“PARALLEL”，[II]（R“-C = CO）2 Zn或者WHEREIN R'，R“和R”'各自独立地是饱和或不饱和的，环状或非环状，支链或直链烃基，同时同时除去水形成。

8. 发明授权

US3883362A Friable compositions and process for producing same 失效
标题翻译：易碎组合物及其生产方法
公开(公告)号：US3883362A
公开(公告)日：1975-05-13
申请号：US46595074
申请日：1974-05-01
申请人： CONTINENTAL OIL CO
发明人： YATES JAMES E , WASHECHECK PAUL H
IPC分类号： C08J5/00 , C08L91/06 , C08L91/08 , C08L101/00 , C08H9/06 , C08H17/36
CPC分类号： C08L101/00 , C08J5/00 , C08K3/22 , C08K5/09 , C08L27/06 , C08L91/06 , C08L91/08
摘要： Friable compositions suitable for use as extrusion aids in polymeric extrusion formulations are prepared by a process which comprises mixing a paraffinic hydrocarbon wax, calcium hydroxide and a fatty acid while heating to a temperature of at least 150*C and thereafter cooling to recover a solid, glass-like, friable composition, said paraffinic hydrocarbon wax having a drop melting point of at least 110*F, an oil content of not greater than 50 percent by weight and a needle penetration value (77*F) in the range of 1 mm to 20 mm, and said fatty acid being a C16C24 aliphatic hydrocarbon monocarboxylic acid or mixtures thereof.
摘要翻译：适合用作聚合物挤出制剂中的挤出助剂的易碎组合物通过包括将石蜡烃蜡，氢氧化钙和脂肪酸混合同时加热至至少150℃的温度并随后冷却以回收固体的方法制备，玻璃状易碎组合物，所述石蜡烃蜡的熔点至少为110°F，油含量不大于50wt％，针刺度（77°F）在1mm范围内至20mm，所述脂肪酸为C16-C24脂族烃单羧酸或其混合物。

9. 发明授权

US3450735A Production of aluminum trialkoxide and aliphatic alcohols 失效
标题翻译：生产三聚氰酸铝和脂肪醇
公开(公告)号：US3450735A
公开(公告)日：1969-06-17
申请号：US3450735D
申请日：1966-11-14
申请人： CONTINENTAL OIL CO
发明人： LUNDEEN ALLAN J , YATES JAMES E
IPC分类号： C07C29/54 , C07F5/06
CPC分类号： C07C29/54 , C07C31/125

10. 发明授权

US3883363A Friable composition and process 失效
标题翻译：脆弱的组成和过程
公开(公告)号：US3883363A
公开(公告)日：1975-05-13
申请号：US46578974
申请日：1974-05-01
申请人： CONTINENTAL OIL CO
发明人： YATES JAMES E , PINTO WILFRED M
IPC分类号： C08J5/00 , C08K5/098 , C08L91/06 , C08L91/08 , C08L101/00 , C08H9/06 , C08H17/36
CPC分类号： C08L101/00 , C08J5/00 , C08K5/09 , C08K5/098 , C08L27/06 , C08L91/06 , C08L91/08
摘要： Friable compositions suitable for use as extrusion aids in polymeric extrusion formulations are prepared by a process which comprises mixing a paraffinic hydrocarbon wax and calcium salt of a fatty acid while heating to a temperature of at least 150*C and thereafter cooling to recover a solid, glass-like, friable composition, said paraffinic hydrocarbon wax having a drop melting point of at least 110*F, an oil content of not greater than 50 percent by weight and a needle penetration value at 77*F in the range of 1 mm to 20 mm, and said fatty acid being a C16C24 aliphatic hydrocarbon monocarboxylic acid or mixtures thereof.
摘要翻译：适合用作聚合物挤出配方中的挤出助剂的微小组合物通过以下方法制备，该方法包括将石蜡烃蜡和脂肪酸的钙盐混合，同时加热至至少150℃的温度，然后冷却以回收固体，玻璃状，易碎组合物，所述链烷烃烃蜡的熔点至少为110°F，油含量不大于50％（重量），针刺度在77°F的范围为1mm至 20mm，所述脂肪酸是C16-C24脂族烃单羧酸或其混合物。

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