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1. 发明授权

US4143173A Flavoring with 5-acyl-2-(furfurylthio)dihydro-2,5-dialkyl-3-[2H]furanones 失效
标题翻译：用5-亚氨基-2-（呋喃硫基）二氢-2H-二烷基-3-（2H）呋喃酮
公开(公告)号：US4143173A
公开(公告)日：1979-03-06
申请号：US887632
申请日：1978-03-17
申请人： Braja D. Mookherjee , Donald A. Withycombe , Ira Katz , Alfred E. Goossens , Manfred H. Vock , William J. Evers , Joaquin F. Vinals , Jacob Kiwala
发明人： Braja D. Mookherjee , Donald A. Withycombe , Ira Katz , Alfred E. Goossens , Manfred H. Vock , William J. Evers , Joaquin F. Vinals , Jacob Kiwala
IPC分类号： A24B15/40 , C07D307/32 , C07D307/38 , C07D307/42 , C11B9/00 , A23L1/234
CPC分类号： C07D307/32 , A24B15/406 , C07D307/38 , C07D307/42 , C11B9/0076
摘要： Processes and compositions are described for the use in foodstuff, chewing gum, toothpaste and medicinal product flavor and aroma and tobacco flavor and aroma augmenting, modifying, enhancing and imparting compositions and as foodstuff, chewing gum, toothpaste, medicinal product and tobacco aroma and flavor imparting, augmenting, modifying and enhancing materials of one or more 5-acyl-2-(furfurylthio)dihydro-2,5-dialkyl-3-[2H]furanones having the generic structure: ##STR1## wherein R.sub.1 ', R.sub.2 ', R.sub.3 ' and R.sub.4 ' are each the same or different and each represents hydrogen or methyl produced according to the process of reacting one or more alpha, beta diketones containing from 4 up to 6 carbon atoms and having the generic structure: ##STR2## or one or more dimerization products thereof having the generic structure: ##STR3## wherein R.sub.1 ', R.sub.2 ', R.sub.3 ', R.sub.4 ', R.sub.5 ' and R.sub.6 ' are each the same or different and each represents hydrogen or methyl with furfuryl mercaptan having the structure: ##STR4## Addition of one or more 5-acyl-2-(furfurylthio)dihydro-2,5-dialkyl-3-[2H]furanones or "cis" or "trans" isomers thereof to consumable materials is indicated to produce:(A) In flavoring compositions for foodstuffs, chewing gums, toothpastes and medicinal products and in the foodstuffs, chewing gums, toothpastes and medicinal products per se, coffee, roasted, cocoa-like, caramel-like, licorice and roasted almond aroma and flavor characteritics at levels of greater than or equal to 0.01 parts per million; and(B) In tobacco, flavoring compositions for tobacco, tobacco substitutes and flavoring compositions therefor, wheat, caramel/coffee aroma and taste characteristics prior to and on smoking and nutty/pyrazine-like flavor and aroma characteristics with roasted nut like nuances on smoking.

2. 发明授权

US4145354A Process for preparing 5-acyl-2-(furfurylthio)dihydro-2,5-dialkyl-3-�2H!furanones 失效
标题翻译：制备5-亚氨基-2-（呋喃硫基）二氢-2,5-二烷基-3-（2H）呋喃酮的方法
公开(公告)号：US4145354A
公开(公告)日：1979-03-20
申请号：US887637
申请日：1978-03-17
申请人： Braja D. Mookherjee , Donald A. Withycombe , Ira Katz , Alfred E. Goossens , Manfred H. Vock , William J. Evers , Joaquin F. Vinals , Jacob Kiwala
发明人： Braja D. Mookherjee , Donald A. Withycombe , Ira Katz , Alfred E. Goossens , Manfred H. Vock , William J. Evers , Joaquin F. Vinals , Jacob Kiwala
IPC分类号： A24B15/40 , C07D307/32 , C07D307/38 , C07D307/42 , C11B9/00 , C07D307/64
CPC分类号： C07D307/32 , A24B15/406 , C07D307/38 , C07D307/42 , C11B9/0076
摘要： Processes and compositions are described for the use in foodstuff, chewing gum, toothpaste and medicinal product flavor and aroma and tobacco flavor and aroma augmenting, modifying, enhancing and imparting compositions and as foodstuff, chewing gum, toothpaste, medicinal product and tobacco aroma and flavor imparting, augmenting, modifying and enhancing materials of one or more 5-acyl-2-(furfurylthio)dihydro-2,5-dialkyl-3-�2H!furanones having the generic structure: ##STR1## wherein R.sub.1 ', R.sub.2 ', R.sub.3 ' and R.sub.4 ' are each the same or different and each represents hydrogen or methyl produced according to the process of reacting one or more alpha, beta diketones containing from 4 up to 6 carbon atoms and having the generic structure: ##STR2## or one or more dimerization products thereof having the generic structure: ##STR3## wherein R.sub.1 ', R.sub.2 ', R.sub.3 ', R.sub.4 ', R.sub.5 ' and R.sub.6 ' are each the same or different and each represents hydrogen or methyl with furfuryl mercaptan having the structure: ##STR4## Addition of one or more 5-acyl-2-(furfurylthio)dihydro-2,5-dialkyl-3-�2H!furanones or "cis" or "trans" isomers thereof to consumable materials is indicated to produce: (A) In flavoring compositions for foodstuffs, chewing gums, toothpastes and medicinal products and in the foodstuffs, chewing gums, toothpastes, and medicinal products per se, coffee, roasted, cocoa-like, caramel-like, licorice and roasted almond aroma and flavor characteristics at levels of greater than or equal to 0.01 parts per million; and (B) In tobacco, flavoring compositions for tobacco, tobacco substitutes and flavoring compositions therefor, wheat, caramel/coffee aroma and taste characteristics prior to and on smoking and nutty/pyrazine-like flavor and aroma characteristics with roasted nut like nuances on smoking.

3. 发明授权

US4260641A Mixtures containing isobutyl substituted heterocyclic compounds and flavor use thereof 失效
标题翻译：含有异丁基取代的杂环化合物的混合物及其风味用途
公开(公告)号：US4260641A
公开(公告)日：1981-04-07
申请号：US67370
申请日：1979-08-17
申请人： Donald A. Withycombe , Braja D. Mookherjee , Manfred H. Vock , Joaquin F. Vinals
发明人： Donald A. Withycombe , Braja D. Mookherjee , Manfred H. Vock , Joaquin F. Vinals
IPC分类号： A23L27/20 , A23L27/28 , A23L1/234
CPC分类号： A23L27/28 , A23L27/2056
摘要： Foodstuff flavor and aroma augmenting and enhancing compositions are described containing compositions of matter which include a mixture of (i) 2,4,6-triisobutyl-1,3,5-trioxane and (ii) two 2-isobutyl dialkyloxazolines having the generic structure: ##STR1## wherein R.sub.1 and R.sub.2 are different and each represents ethyl or methyl. Addition of such mixtures to foodstuffs produces chocolate-like, nutty, green, burnt, roasted aromas and tastes. The above-mentioned mixture can only properly be defined by its process for producing same. That is, admixing aqueous ammonia with isovaleraldehyde at a temperature in the range of from about 0.degree. C. up to about 10.degree. C. whereby the reaction of aqueous ammonia with isovaleraldehyde is carried out, using a mole ratio of isovaleraldehyde: ammonia of from 0.5:1 up to 2:1 thereby producing an imine; then reacting the resulting imine with 2-hydroxy-3-pentanone 3-hydroxy-2-pentanone or a mixture thereof at a temperature in the range of from about 30.degree. C. up to about 50.degree. C. over a period of time of from 1 up to 10 hours.
摘要翻译：描述了包含（i）2,4,6-三异丁基-1,3,5-三恶烷和（ii）具有通用结构的两个2-异丁基二烷基恶唑啉的混合物的物质组合物的食品香料增香和增强组合物：其中R 1和R 2不同并且各自表示乙基或甲基。将这样的混合物加入到食品中产生巧克力，坚果，绿色，烧焦，烘烤的香气和口味。上述混合物只能通过其制备方法适当地定义。也就是说，将氨水与异戊醛混合在约0℃至约10℃的温度范围内，由此氨水与异戊醛的反应是使用异戊醛：氨的摩尔比来进行的 0.5：1至2：1，从而产生亚胺; 然后将所得亚胺与2-羟基-3-戊酮3-羟基-2-戊酮或其混合物在约30℃至约50℃的温度下反应一段时间，从1到10小时。

4. 发明授权

US4207905A Isobutyl substituted heterocyclic compounds for augmenting or enhancing the organoleptic properties of smoking tobaccos and smoking tobacco articles 失效
标题翻译：异丁基取代的杂环化合物，用于增强或增强吸烟烟草和烟草制品的感官特性
公开(公告)号：US4207905A
公开(公告)日：1980-06-17
申请号：US887627
申请日：1978-03-17
申请人： Donald A. Withycombe , Braja D. Mookherjee , Manfred H. Vock , Joaquin F. Vinals
发明人： Donald A. Withycombe , Braja D. Mookherjee , Manfred H. Vock , Joaquin F. Vinals
IPC分类号： A23G4/00 , A23G4/06 , A23L27/20 , A24B15/36 , A24B15/40 , C07D263/12 , C07D323/04 , A24B3/12
CPC分类号： A23G4/06 , A23L27/2052 , A23L27/2056 , A24B15/36 , A24B15/403 , C07D263/12 , C07D323/04
摘要： Processes and compositions are described for the use in smoking tobacco flavor and aroma augmenting, modifying, enhancing and imparting compositions and as smoking tobacco aroma or flavor imparting, augmenting or enhancing materials of a mixture of compounds having the generic structure: ##STR1## wherein X is a moiety selected from the group consisting of: ##STR2## and wherein R.sub.1 and R.sub.2 are different, one of R.sub.1 or R.sub.2 being methyl, and the other of R.sub.1 or R.sub.2 being ethyl, or mixtures of same, including (i) 2,4,6-triisobutyl-1,3,5-trioxane and (ii) 2-isobutyl dialkyloxazolines.
摘要翻译：描述了用于吸烟烟草风味和香气增强，改性，增强和赋予组合物以及吸烟烟草香气或风味赋予，增强或增强具有以下通用结构的化合物的混合物的方法和组合物：其中X 是选自以下的部分：其中R 1和R 2不同，R 1或R 2中的一个为甲基，R 1或R 2中的另一个为乙基，或其混合物，包括（i）2， 4,6-三异丁基-1,3,5-三恶烷和（ii）2-异丁基二烷基恶唑啉。

5. 发明授权

US4191785A Flavoring with mixtures of 2,4,6-triisobutyl-1,3,5-trioxane and 2-isobutyl-dialkyl oxazolines 失效
标题翻译：用2,4,6-三异丁基-1,3,5-三恶烷和2-异丁基 - 二烷基恶唑啉的混合物进行调味
公开(公告)号：US4191785A
公开(公告)日：1980-03-04
申请号：US928716
申请日：1978-07-27
申请人： Donald A. Withycombe , Braja D. Mookherjee , Manfred H. Vock , Joaquin F. Vinals
发明人： Donald A. Withycombe , Braja D. Mookherjee , Manfred H. Vock , Joaquin F. Vinals
IPC分类号： A23G1/00 , A23G1/56 , A23L27/20 , A23L27/28 , A24B15/36 , A24B15/40 , C07D263/12 , C07D323/04 , A23L1/226 , A23L1/234
CPC分类号： C07D323/04 , A23G1/56 , A23L27/2052 , A23L27/2056 , A23L27/28 , A24B15/36 , A24B15/403 , C07D263/12 , A23G2200/00
摘要： Processes and compositions are described for the use in foodstuffs, chewing gums, toothpastes and medicinal product flavor and aroma augmenting, modifying, enhancing and imparting compositions and as foodstuff, chewing gum, toothpaste and medicinal product imparting, augmenting or enhancing materials of a mixture of compounds having the structures: ##STR1## wherein R.sub.1 and R.sub.2 are different and each represents ethyl or methyl. Addition of such mixtures to foodstuffs, foodstuff flavorings, chewing gums, toothpastes and medicinal products produces therein sweet, dark chocolate and cocoa powder-like aroma characteristics with dark chocolate, cocoa powder-like, and spicey flavor characteristics and bitter chocolate aftertastes.
摘要翻译：描述的方法和组合物用于食品，口香糖，牙膏和药用产品香料以及香气增强，改性，增强和赋予组合物以及作为食品，口香糖，牙膏和赋予，增加或增强混合物的材料的药用产品具有以下结构的化合物：其中R1和R2不同，并且各自表示乙基或甲基。向食品，食品调味品，口香糖，牙膏和药用产品中加入这种混合物产生具有黑巧克力，可可粉和类似风味特征的苦味巧克力和可可粉样香气特征以及苦味巧克力味道。

6. 发明授权

US4170236A Isobutyl substituted heterocyclic compounds and uses for augmenting or enhancing the organoleptic properties of smoking compositions 失效
标题翻译：异丁基取代的杂环化合物和用于增强或增强吸烟组合物的感官特性的用途
公开(公告)号：US4170236A
公开(公告)日：1979-10-09
申请号：US887625
申请日：1978-03-17
申请人： Donald A. Withycombe , Braja D. Mookherjee , Manfred H. Vock , Joaquin F. Vinals
发明人： Donald A. Withycombe , Braja D. Mookherjee , Manfred H. Vock , Joaquin F. Vinals
IPC分类号： A23G4/00 , A23G4/06 , A23L27/20 , A24B15/40 , A24B3/12 , A24D1/18
CPC分类号： A23G4/06 , A23L27/2052 , A23L27/2056 , A24B15/403
摘要： Process and product for use in augmenting or enhancing the aroma and taste of smoking compositions comprising the addition of 2,4,6-triisobutyl-1,3,5-trioxane.
摘要翻译：用于增强或增强吸烟组合物的香气和味道的方法和产品，包括加入2,4,6-三异丁基-1,3,5-三恶烷。

7. 发明授权

US4360032A Use of hydrogenated derivatives of 2,6,6-trimethyl-cyclohexene derivatives in augmenting or enhancing the aroma or taste of smoking tobacco and smoking tobacco articles 失效
标题翻译：使用2,6,6-三甲基 - 环己烯衍生物的氢化衍生物来增强或增强吸烟烟草和烟草制品的香气或味道
公开(公告)号：US4360032A
公开(公告)日：1982-11-23
申请号：US239052
申请日：1981-02-27
申请人： Robert W. Trenkle , Braja D. Mookherjee , Frederick L. Schmitt , Manfred H. Vock , Joaquin F. Vinals , Jacob Kiwala
发明人： Robert W. Trenkle , Braja D. Mookherjee , Frederick L. Schmitt , Manfred H. Vock , Joaquin F. Vinals , Jacob Kiwala
IPC分类号： A24B15/34 , C07C45/62 , C07C49/303 , C07C49/543 , C11B9/00 , A24B3/12 , A24B15/30
CPC分类号： C11B9/0034 , A24B15/34 , C07C45/62 , C07C49/303 , C07C49/543
摘要： Described is the use of augmenting or enhancing the aroma or taste of smoking tobacco or smoking tobacco articles comprising the step of intimately admixing with smoking tobacco or a portion of a smoking tobacco article at least one substance selected from the group consisting of:(i) the compound having the structure: ##STR1## (ii) the compound having the structure: ##STR2## (iii) a mixture of compounds having the structures: ##STR3## (iv) a mixture of compounds having the structures: ##STR4##
摘要翻译：描述了增加或增强吸烟烟草或吸烟烟草制品的香味或味道的用途，其包括与吸烟烟草或吸烟烟草制品的一部分紧密混合的步骤至少一种选自以下的物质：（i）具有以下结构的化合物：（ii）具有以下结构的化合物：（iii）具有以下结构的化合物的混合物：（i）具有以下结构的化合物的混合物： + TR

8. 发明授权

US4228026A 3-Hydroxy-1-(2,6,6-trimethyl-1,3-cyclohexadien-1-yl)-1-butanone in detergents 失效
标题翻译： 3-羟基-1-（2,6,6-三甲基-1,3-环己二烯-1-基）-1-丁酮的洗涤剂
公开(公告)号：US4228026A
公开(公告)日：1980-10-14
申请号：US39116
申请日：1979-05-15
申请人： Braja D. Mookherjee , Richard A. Wilson , Manfred H. Vock , Joaquin F. Vinals , Jacob Kiwala , Frederick L. Schmitt , Edward J. Granda
发明人： Braja D. Mookherjee , Richard A. Wilson , Manfred H. Vock , Joaquin F. Vinals , Jacob Kiwala , Frederick L. Schmitt , Edward J. Granda
IPC分类号： C11B9/00 , C11D3/50 , C11D9/44
CPC分类号： C11B9/0034 , C11D3/50
摘要： Processes and compositions are described for the use as detergent aroma imparting, augmenting or enhancing materials of 3-hydroxy-1-(2,6,6-trimethyl-1,3-cyclohexadien-1-yl)-1-butanone having the structure: ##STR1## and perfume compositions containing same.
摘要翻译：描述了用作洗涤剂香气赋予，增强或增强具有结构的3-羟基-1-（2,6,6-三甲基-1,3-环己二烯-1-基）-1-丁酮的材料的方法和组合物：＆lt; IMAGE＆gt;和含有它们的香水组合物。

9. 发明授权

US4335002A Compositions of matter containing cis-3-hexenal 失效
标题翻译：含有顺式-3-己烯醛的物质组成
公开(公告)号：US4335002A
公开(公告)日：1982-06-15
申请号：US169678
申请日：1980-07-17
申请人： Cynthia J. Mussinan , Braja D. Mookherjee , Manfred H. Vock , Frederick L. Schmitt , Edward J. Granda , Joaquin F. Vinals , Jacob Kiwala
发明人： Cynthia J. Mussinan , Braja D. Mookherjee , Manfred H. Vock , Frederick L. Schmitt , Edward J. Granda , Joaquin F. Vinals , Jacob Kiwala
IPC分类号： A23L27/20 , A24B15/32 , C11B9/00 , A23L1/226 , A23L2/26 , A61K7/46
CPC分类号： C11B9/0015 , A23L27/2024 , A24B15/32
摘要： Described are cis-3-hexenyl derivatives having the generic structure: ##STR1## wherein R is one of the moieties: ##STR2## which are useful in foodstuffs, flavorings, fragrances, perfumed articles (e.g. anionic, cationic or nonionic detergents, dryer-added fabric softener articles and cosmetic powders) and smoking tobacco flavorings; processes for producing such cis-3-hexenyl derivatives and products produced according to such processes which include chemical compounds in addition to said cis-3-hexenyl derivatives.
摘要翻译：描述了具有以下通用结构的顺式-3-己烯基衍生物：其中R是部分之一：可用于食品，调味品，香料，加香制品（例如阴离子，阳离子或非离子型洗涤剂，干燥剂添加织物柔软剂制品和化妆品粉末）和吸烟烟草调味剂; 制备这种顺式-3-己烯基衍生物的方法和根据这些方法生产的产物，除了所述顺式-3-己烯基衍生物外，还包括化学化合物。

10. 发明授权

US4324704A Process for hydrogenation of damascenone, products produced thereby and organoleptic uses of said products 失效
标题翻译：大马士革氢化方法，由此生产的产品和所述产品的感官用途
公开(公告)号：US4324704A
公开(公告)日：1982-04-13
申请号：US238680
申请日：1981-02-27
申请人： Robert W. Trenkle , Braja D. Mookherjee , Frederick L. Schmitt , Manfred H. Vock , Joaquin F. Vinals , Jacob Kiwala
发明人： Robert W. Trenkle , Braja D. Mookherjee , Frederick L. Schmitt , Manfred H. Vock , Joaquin F. Vinals , Jacob Kiwala
IPC分类号： A24B15/34 , C07C45/62 , C07C49/303 , C07C49/543 , C11B9/00 , C11D3/50 , A61K7/46
CPC分类号： C07C403/16 , A24B15/34 , C07C45/62 , C07C49/303 , C07C49/543 , C11B9/0034 , C11D3/50 , C07C2101/16
摘要： Described is a process for preparing hydrogenated derivatives of 2,6,6-trimethyl cyclohexene derivatives by means of treating said derivatives with hydrogen in the presence of a supported palladium catalyst such as palladium-on-calcium carbonate or palladium-on-barium sulfate in the presence of a quinoline activator. The resulting products are useful for their organoleptic properties as foodstuff flavorants and flavor enhancers, perfume composition ingredients, perfumed article ingredients and tobacco flavorants and flavor enhancers.
摘要翻译：描述了通过在负载的钯催化剂如碳酸钯/钯/硫酸钡的存在下用氢处理所述衍生物来制备2,6,6-三甲基环己烯衍生物的氢化衍生物的方法，其中喹啉激活剂的存在。所得到的产品对于其感官特性可用作食品香料和风味增强剂，香料组合物成分，香料制品成分和烟草香料以及风味增强剂。

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