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1. 发明授权

US4620945A Mixtures of one or more t-mercapto terpene isomers and .alpha.-terpineol, .beta.-phenylethyl alcohol, 3-methyl-1-phenyl-pentanol-5 and/or butanoyl cyclohexane derivatives, organoleptic uses thereof and process for preparing same 失效
标题翻译：一种或多种t-巯基萜烯异构体和α-萜品醇，β-苯乙醇，3-甲基-1-苯基 - 戊醇-5和/或丁酰基环己烷衍生物的混合物，其感官用途及其制备方法
公开(公告)号：US4620945A
公开(公告)日：1986-11-04
申请号：US644053
申请日：1984-08-24
申请人： Braja D. Mookherjee , Bernard J. Chant , William J. Evers , Richard A. Wilson , Michael J. Zampino , Manfred H. Vock
发明人： Braja D. Mookherjee , Bernard J. Chant , William J. Evers , Richard A. Wilson , Michael J. Zampino , Manfred H. Vock
IPC分类号： C07D331/02 , C11B9/00 , A61K7/46
CPC分类号： C07D331/02 , C11B9/0034
摘要： Described are organoleptic utilities of mixtures of t-mercapto terpene isomers defined according to the generic structure: ##STR1## wherein one of the dashed lines is a carbon-carbon double bond and the other of the dashed lines is a carbon-carbon single bond taken further together with .alpha.-terpineol having the structure: ##STR2## .beta.-phenylethyl alcohol having the structure: ##STR3## 3-methyl-1-phenyl-pentanol-5 having the structure: ##STR4## and/or butanoyl cyclohexane derivatives defined according to the generic structure: ##STR5## wherein one of the dashed lines is a carbon-carbon double bond or two of the dashed lines represent carbon-carbon double bonds but that when two of the dashed lines represent carbon-carbon double bonds, the carbon-carbon double bonds are conjugated.
摘要翻译：描述了根据通用结构定义的t-巯基萜烯异构体混合物的感官效用：其中一条虚线是碳 - 碳双键，另一条虚线是碳 - 碳单键取代进一步与具有以下结构的α-萜品醇结合：具有以下结构的具有以下结构的β-苯乙醇：具有以下结构的3-甲基-1-苯基 - 戊醇-5：具有以下结构的化合物：和/或丁酰基环己烷衍生物涉及通用结构：其中虚线中的一条为碳 - 碳双键，或两条虚线表示碳 - 碳双键，但当虚线中的两条代表碳 - 碳双键时，碳 - 碳双键共轭。

2. 发明授权

US4536583A Process for preparing mixtures containing 8,9-epithio-1-p-menthene 失效
标题翻译：制备含有9,9-环硫-1-对薄荷烯的混合物的方法
公开(公告)号：US4536583A
公开(公告)日：1985-08-20
申请号：US519371
申请日：1983-08-01
申请人： Braja D. Mookherjee , Bernard J. Chant , William J. Evers , Richard A. Wilson , Michael J. Zampino , Manfred H. Vock
发明人： Braja D. Mookherjee , Bernard J. Chant , William J. Evers , Richard A. Wilson , Michael J. Zampino , Manfred H. Vock
IPC分类号： C07D331/02 , C11B9/00 , A61K7/46
CPC分类号： C07D331/02 , C11B9/0034
摘要： Described is a process for preparing a mixture of t-mercapto terpenes defined according to the structure: ##STR1## and .alpha.-terpineol defined according to the structure: ##STR2## including the step of reacting the compound defined according to the structure: ##STR3## with an alkali metal thiocyanate defined according to the structure: ##STR4## wherein M represents alkali metal such as sodium, potassium or lithium in the presence of a phase transfer catalyst. The resulting product is then treated with lithium aluminum hydride followed by aqueous mineral acid to form a mixture of .alpha.-terpineol and the compound defined according to the structure: ##STR5## which mixture is useful for its organoleptic properties.
摘要翻译：描述了根据以下结构定义的t-巯基萜烯的混合物的方法：根据以下结构定义的：ι和α-萜品醇：包括使根据以下结构定义的化合物反应的步骤：碱金属硫氰酸盐根据以下结构定义：其中M在相转移催化剂存在下表示碱金属如钠，钾或锂。然后将所得产物用氢化铝锂处理，然后用无机酸水溶液处理，以形成α-萜烯醇和根据以下结构定义的化合物的混合物：该组合物可用于其感官特性。

3. 发明授权

US4584128A Mixture of one or more t-mercapto terpene isomers and .alpha.-terpineol organoleptic uses thereof 失效
标题翻译：一种或多种t-巯基萜烯异构体和α-萜品醇感官用途的混合物
公开(公告)号：US4584128A
公开(公告)日：1986-04-22
申请号：US644117
申请日：1984-08-24
申请人： Braja D. Mookherjee , Bernard J. Chant , William J. Evers , Richard A. Wilson , Michael J. Zampino , Manfred H. Vock
发明人： Braja D. Mookherjee , Bernard J. Chant , William J. Evers , Richard A. Wilson , Michael J. Zampino , Manfred H. Vock
IPC分类号： C07D331/02 , C11B9/00 , A61K7/46
CPC分类号： C11B9/0034 , C07D331/02
摘要： Described are mixtures of t-mercapto terpene isomers defined according to the generic structure: ##STR1## wherein one of the dashed lines is a carbon-carbon double bond and the other of the dashed lines is a carbon-carbon single bond taken further together with .alpha.-terpineol having the structure: ##STR2##
摘要翻译：描述了根据通用结构定义的t-巯基萜烯异构体的混合物：其中一条虚线是碳 - 碳双键，另一条虚线是碳 - 碳单键，进一步与具有以下结构的α-萜品醇：

4. 发明授权

US4145354A Process for preparing 5-acyl-2-(furfurylthio)dihydro-2,5-dialkyl-3-�2H!furanones 失效
标题翻译：制备5-亚氨基-2-（呋喃硫基）二氢-2,5-二烷基-3-（2H）呋喃酮的方法
公开(公告)号：US4145354A
公开(公告)日：1979-03-20
申请号：US887637
申请日：1978-03-17
申请人： Braja D. Mookherjee , Donald A. Withycombe , Ira Katz , Alfred E. Goossens , Manfred H. Vock , William J. Evers , Joaquin F. Vinals , Jacob Kiwala
发明人： Braja D. Mookherjee , Donald A. Withycombe , Ira Katz , Alfred E. Goossens , Manfred H. Vock , William J. Evers , Joaquin F. Vinals , Jacob Kiwala
IPC分类号： A24B15/40 , C07D307/32 , C07D307/38 , C07D307/42 , C11B9/00 , C07D307/64
CPC分类号： C07D307/32 , A24B15/406 , C07D307/38 , C07D307/42 , C11B9/0076
摘要： Processes and compositions are described for the use in foodstuff, chewing gum, toothpaste and medicinal product flavor and aroma and tobacco flavor and aroma augmenting, modifying, enhancing and imparting compositions and as foodstuff, chewing gum, toothpaste, medicinal product and tobacco aroma and flavor imparting, augmenting, modifying and enhancing materials of one or more 5-acyl-2-(furfurylthio)dihydro-2,5-dialkyl-3-�2H!furanones having the generic structure: ##STR1## wherein R.sub.1 ', R.sub.2 ', R.sub.3 ' and R.sub.4 ' are each the same or different and each represents hydrogen or methyl produced according to the process of reacting one or more alpha, beta diketones containing from 4 up to 6 carbon atoms and having the generic structure: ##STR2## or one or more dimerization products thereof having the generic structure: ##STR3## wherein R.sub.1 ', R.sub.2 ', R.sub.3 ', R.sub.4 ', R.sub.5 ' and R.sub.6 ' are each the same or different and each represents hydrogen or methyl with furfuryl mercaptan having the structure: ##STR4## Addition of one or more 5-acyl-2-(furfurylthio)dihydro-2,5-dialkyl-3-�2H!furanones or "cis" or "trans" isomers thereof to consumable materials is indicated to produce: (A) In flavoring compositions for foodstuffs, chewing gums, toothpastes and medicinal products and in the foodstuffs, chewing gums, toothpastes, and medicinal products per se, coffee, roasted, cocoa-like, caramel-like, licorice and roasted almond aroma and flavor characteristics at levels of greater than or equal to 0.01 parts per million; and (B) In tobacco, flavoring compositions for tobacco, tobacco substitutes and flavoring compositions therefor, wheat, caramel/coffee aroma and taste characteristics prior to and on smoking and nutty/pyrazine-like flavor and aroma characteristics with roasted nut like nuances on smoking.

5. 发明授权

US4143173A Flavoring with 5-acyl-2-(furfurylthio)dihydro-2,5-dialkyl-3-[2H]furanones 失效
标题翻译：用5-亚氨基-2-（呋喃硫基）二氢-2H-二烷基-3-（2H）呋喃酮
公开(公告)号：US4143173A
公开(公告)日：1979-03-06
申请号：US887632
申请日：1978-03-17
申请人： Braja D. Mookherjee , Donald A. Withycombe , Ira Katz , Alfred E. Goossens , Manfred H. Vock , William J. Evers , Joaquin F. Vinals , Jacob Kiwala
发明人： Braja D. Mookherjee , Donald A. Withycombe , Ira Katz , Alfred E. Goossens , Manfred H. Vock , William J. Evers , Joaquin F. Vinals , Jacob Kiwala
IPC分类号： A24B15/40 , C07D307/32 , C07D307/38 , C07D307/42 , C11B9/00 , A23L1/234
CPC分类号： C07D307/32 , A24B15/406 , C07D307/38 , C07D307/42 , C11B9/0076
摘要： Processes and compositions are described for the use in foodstuff, chewing gum, toothpaste and medicinal product flavor and aroma and tobacco flavor and aroma augmenting, modifying, enhancing and imparting compositions and as foodstuff, chewing gum, toothpaste, medicinal product and tobacco aroma and flavor imparting, augmenting, modifying and enhancing materials of one or more 5-acyl-2-(furfurylthio)dihydro-2,5-dialkyl-3-[2H]furanones having the generic structure: ##STR1## wherein R.sub.1 ', R.sub.2 ', R.sub.3 ' and R.sub.4 ' are each the same or different and each represents hydrogen or methyl produced according to the process of reacting one or more alpha, beta diketones containing from 4 up to 6 carbon atoms and having the generic structure: ##STR2## or one or more dimerization products thereof having the generic structure: ##STR3## wherein R.sub.1 ', R.sub.2 ', R.sub.3 ', R.sub.4 ', R.sub.5 ' and R.sub.6 ' are each the same or different and each represents hydrogen or methyl with furfuryl mercaptan having the structure: ##STR4## Addition of one or more 5-acyl-2-(furfurylthio)dihydro-2,5-dialkyl-3-[2H]furanones or "cis" or "trans" isomers thereof to consumable materials is indicated to produce:(A) In flavoring compositions for foodstuffs, chewing gums, toothpastes and medicinal products and in the foodstuffs, chewing gums, toothpastes and medicinal products per se, coffee, roasted, cocoa-like, caramel-like, licorice and roasted almond aroma and flavor characteritics at levels of greater than or equal to 0.01 parts per million; and(B) In tobacco, flavoring compositions for tobacco, tobacco substitutes and flavoring compositions therefor, wheat, caramel/coffee aroma and taste characteristics prior to and on smoking and nutty/pyrazine-like flavor and aroma characteristics with roasted nut like nuances on smoking.

6. 发明授权

US3960860A 2-Methyl-5,7-dihydrothieno-[3,4d]-pyrimidine 失效
标题翻译： 2-甲基-5,7-二氢噻吩并 - {1,8-d]嘧啶
公开(公告)号：US3960860A
公开(公告)日：1976-06-01
申请号：US541259
申请日：1975-01-15
申请人： Ira Katz , Richard A. Wilson , William J. Evers , Manfred H. Vock , Gerrit W. Verhoeve
发明人： Ira Katz , Richard A. Wilson , William J. Evers , Manfred H. Vock , Gerrit W. Verhoeve
IPC分类号： A23L27/20 , A24B15/36 , C11B9/00 , C07D495/04
CPC分类号： C11B9/0069 , A23L27/205 , A24B15/36
摘要： This application relates to 2-methyl-5,7-dihydrothieno-[3,4d]-pyrimidine, which is useful for flavoring foodstuffs or tobacco compositions and altering the fragrance of perfume compositions.
摘要翻译：本申请涉及2-甲基-5,7-二氢噻吩并[3,4d] - 嘧啶，其可用于调味食品或烟草组合物并改变香料组合物的香料。

7. 发明授权

US4126708A Flavoring with 2-acyl-5-substituted thiatetrahydrofuran-4-ones 失效
标题翻译：用2-乙炔基-5-取代的噻唑烷-4-酮洗脱
公开(公告)号：US4126708A
公开(公告)日：1978-11-21
申请号：US887629
申请日：1978-03-17
申请人： Braja D. Mookherjee , William J. Evers , Alfred E. Goossens
发明人： Braja D. Mookherjee , William J. Evers , Alfred E. Goossens
IPC分类号： A24B15/40 , C07D307/32 , C07D307/64 , C11B9/00 , A23L1/226 , A23L1/234
CPC分类号： C07D307/32 , A24B15/406 , C07D307/64 , C11B9/0076
摘要： The 2-acyl-5-substituted thiatetrahydrofuran-4-ones of our invention have organoleptic properties which make them useful for augmenting or enhancing the aroma or flavor of foodstuffs, tobaccos and the aroma of perfumes and perfumed articles.

8. 发明授权

US4623749A Synthesis of triconjugated dienones and novel intermediates used in said process 失效
标题翻译：三氯联二烯酮的合成和所述方法中使用的新型中间体
公开(公告)号：US4623749A
公开(公告)日：1986-11-18
申请号：US620163
申请日：1984-08-17
申请人： William J. Evers , Gilbert Stork , Braja D. Mookherjee , Howard H. Heinsohn, Jr.
发明人： William J. Evers , Gilbert Stork , Braja D. Mookherjee , Howard H. Heinsohn, Jr.
IPC分类号： C07C45/67 , C07C49/203 , C07C69/145 , C07C69/157 , C11B9/00 , C11D3/50
CPC分类号： C11D3/50 , C07C45/673 , C07C45/676 , C07C49/203 , C07C67/293 , C11B9/0015 , C11B9/0061
摘要： Described is a process for preparing triconjugated dienones defined according to the structure: ##STR1## wherein R.sub.1 represents C.sub.1 -C.sub.8 alkyl, phenyl or phenyl methyl and wherein R.sub.2 represents hydrogen or C.sub.1 -C.sub.5 lower alkyl; and wherein the wavy lines are indicative of a "cis" or a "trans" juxtaposition of the R.sub.2, methyl, acyl or vinyl moieties about one or both of the carbon-carbon double bonds which process involves the reaction of an acyl halide with a substituted or unsubstituted prenyl ester having the structure: ##STR2## wherein R.sub.3 represents C.sub.1 -C.sub.5 alkyl in the presence of an aluminum chloride catalyst and a methylene dichloride solvent in order to form a halogen-ester intermediate defined according to the structure: ##STR3## then dehydrohalogenating said halogen-ester intermediate using an alkali metal carbonate and a dimethylformamide solvent in order to form a ketoester having the structure: ##STR4## wherein one of the dashed lines represents a carbon-carbon double bond and the other of the dashed lines represents a carbon-carbon single bond; and then dehydroacyloxylating the ketoester in the presence of an alkali metal carbonate and dimethylformamide solvent in order to form the triconjugated dienone.
摘要翻译：描述了根据以下结构定义的三结合双酮的方法：其中R 1表示C 1 -C 8烷基，苯基或苯基甲基，并且其中R 2表示氢或C 1 -C 5低级烷基; 并且其中波浪线表示R2，甲基，酰基或乙烯基部分在一个或两个碳 - 碳双键上的“顺式”或“反式”并置，该方法涉及酰卤与具有以下结构的取代或未取代的异戊二烯基酯：其中R 3在氯化铝催化剂和二氯甲烷溶剂的存在下代表C 1 -C 5烷基，以形成根据以下结构定义的卤素 - 酯中间体：然后使用碱金属碳酸盐和二甲基甲酰胺溶剂将所述卤代酯中间体脱卤化氢，以形成具有以下结构的酮酯：其中虚线中的一条代表碳 - 碳双键，另一条虚线表示碳 - 碳单键; 然后在碱金属碳酸盐和二甲基甲酰胺溶剂的存在下，使酮酯脱羟基酰化，以形成三羟甲基封端的二烯酮。

9. 发明授权

US4504398A Process for augmenting or enhancing the aroma of perfumed articles by adding thereto triconjugated dienones 失效
标题翻译：通过向其中加入三环酮二烯酮来增强或增强香料制品香气的方法
公开(公告)号：US4504398A
公开(公告)日：1985-03-12
申请号：US551482
申请日：1983-11-14
申请人： William J. Evers , Gilbert Stork , Braja D. Mookherjee , Howard H. Heinsohn, Jr.
发明人： William J. Evers , Gilbert Stork , Braja D. Mookherjee , Howard H. Heinsohn, Jr.
IPC分类号： C07C45/67 , C07C49/203 , C11B9/00 , C11D3/50 , D06M13/20
CPC分类号： C11D3/50 , C07C45/673 , C07C45/676 , C07C49/203 , C07C67/293 , C07C67/297 , C11B9/0015 , C11B9/0061
摘要： Described is a process for augmenting or enhancing the aroma of a perfumed article which is a solid or liquid anionic, cationic, nonionic or zwitterionic detergent or a fabric softener composition or a dryer-added fabric softener article comprising the step of adding to said perfumed article at least one compound having a structure selected from the group consisting of: ##STR1##
摘要翻译：描述了一种用于增强或增强作为固体或液体阴离子，阳离子，非离子或两性离子洗涤剂或织物柔软剂组合物或干衣剂添加的织物柔软剂制品的香料的香气的方法，其包括将所述香料至少一种具有选自以下的结构的化合物：（i）和（iii）（ii）

10. 发明授权

US4560791A Synthesis of triconjugated dienones and intermediates used in said process 失效
标题翻译：在所述方法中使用的三氯联二烯酮和中间体的合成
公开(公告)号：US4560791A
公开(公告)日：1985-12-24
申请号：US551480
申请日：1983-11-14
申请人： William J. Evers , Gilbert Stork , Braja D. Mookherjee , Howard H. Heinsohn, Jr.
发明人： William J. Evers , Gilbert Stork , Braja D. Mookherjee , Howard H. Heinsohn, Jr.
IPC分类号： C07C45/67 , C07C49/203 , C07C69/157 , C11B9/00 , C11D3/50
CPC分类号： C11D3/50 , C07C45/673 , C07C45/676 , C07C49/203 , C07C67/293 , C07C67/297 , C07C69/63 , C11B9/0015 , C11B9/0061
摘要： Described is a process for preparing triconjugated dienones defined according to the structure: ##STR1## wherein R.sub.1 represents C.sub.1 -C.sub.8 alkyl, phenyl or phenyl methyl and wherein R.sub.2 represents hydrogen or C.sub.1 -C.sub.5 lower alkyl; and wherein the wavy lines are indicative of a "cis" or a "trans" juxtaposition of the R.sub.2, methyl, acyl or vinyl moieties about one or both of the carbon-carbon double bonds which process involves the reaction of an acyl halide having the structure: ##STR2## (wherein X represents chloro) with a substituted or unsubstituted prenyl ester having the structure: ##STR3## wherein R.sub.3 represents C.sub.1 -C.sub.5 alkyl in the presence of an aluminum chloride catalyst and a methylene dichloride solvent in order to form the novel intermediate genus defined according to the structure: ##STR4## then dehydrohalogenating the compound defined according to the structure: ##STR5## using an alkali metal carbonate and a dimethylformamide solvent in order to form the novel compound genus having the structure: ##STR6## wherein one of the dashed lines represents a carbon-carbon double bond and the other of the dashed lines represents a carbon-carbon single bond; and then dehydroacyloxylating the compound having the structure: ##STR7## in order to form the compound having the structure: ##STR8## the dehydroacyloxylation step taking place in the presence of an akali metal carbonate and dimethylformamide solvent.
摘要翻译：描述了根据以下结构定义的三结合双酮的方法：其中R 1表示C 1 -C 8烷基，苯基或苯基甲基，并且其中R 2表示氢或C 1 -C 5低级烷基; 并且其中波浪线表示R2，甲基，酰基或乙烯基部分在一个或两个碳 - 碳双键上的“顺式”或“反式”并置，该方法涉及具有结构：其中X表示氯，具有以下结构的取代或未取代的异戊二烯基酯：其中R 3表示C 1 -C 5烷基，在氯化铝催化剂和二氯甲烷溶剂的存在下，形成根据以下结构定义的新型中间体：然后使用碱金属碳酸盐和二甲基甲酰胺溶剂将根据结构定义的化合物脱卤化氢，以形成具有以下结构的新颖化合物：其中虚线中的一条代表碳 - 碳双键，另一条虚线表示碳 - 碳单键; 然后将具有以下结构的化合物脱氢酰化氧化：为了形成具有以下结构的化合物：在碱金属碳酸盐和二甲基甲酰胺溶剂存在下进行脱氢甲酰氧基化步骤。

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