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1. 发明授权

US06734322B1 Method for producing o-chloromethyl benzenecarbonyl chlorides 失效
标题翻译：邻苯甲酰氯的制备方法
公开(公告)号：US06734322B1
公开(公告)日：2004-05-11
申请号：US10130826
申请日：2002-05-23
申请人： Armin Stamm , Roland Götz , Norbert Götz , Jochem Henkelmann , Heinz-Josef Kneuper , Bernd Wolf
发明人： Armin Stamm , Roland Götz , Norbert Götz , Jochem Henkelmann , Heinz-Josef Kneuper , Bernd Wolf
IPC分类号： C07C5158
CPC分类号： C07C51/09 , C07C63/04
摘要： The invention relates to a method for producing o-choromethyl benzenecarbonyl chlorides of formula (I), wherein R1-R4 can be the same or different and stand for hydrogen, C1-C4-alkyl, halogen or trifluoromnethyl, by converting benzocondensed lactones of formula (II), wherein R1-R4 have the aforementioned meaning, with gaseous or liquid phosgene and the dimers or trimers thereof. The inventive method is characterized in that the conversion is carried out in the presence of catalytical amounts of a Lewis acid and catalytical amounts of a phosgenation catalyst
摘要翻译：本发明涉及一种制备式（I）的邻氯甲基苯甲酰氯的方法，其中R 1 -R 4可以相同或不同，代表氢，C 1 -C 4 - 烷基，卤素或三氟甲基，通过用气态或液体光气及其二聚体或三聚体转化其中R 1 -R 4具有上述含义的式（II）的苯并二化内酯。本发明的方法的特征在于转化在催化量的路易斯酸和催化量的光气化催化剂

2. 发明授权

US07034181B1 Method for producing o-chloromethyl benzoic acid chlorides 失效
标题翻译：邻氯甲基苯甲酸氯化物的生产方法
公开(公告)号：US07034181B1
公开(公告)日：2006-04-25
申请号：US10130821
申请日：2000-11-27
申请人： Roland Götz , Norbert Götz , Michael Keil , Bernd Wolf , Adrian Steinmetz , Armin Stamm , Jochem Henkelmann
发明人： Roland Götz , Norbert Götz , Michael Keil , Bernd Wolf , Adrian Steinmetz , Armin Stamm , Jochem Henkelmann
IPC分类号： C07C51/58
CPC分类号： C07C51/60 , C07C63/10
摘要： The invention relates to a method for producing o-chloromethyl benzoic acid chlorides of formula (I), in which R1 to R4 can be the same or different and represent hydrogen C1–C4 alkyl, halogen or trifluoromethyl, by reaction benzo condensed lactones of formula (II), in which R1 to R4 have the above-mentioned meaning, with thionyl chloride. The inventive method is characterized in that the reaction is carried out in the presence of catalytic quantities of a Lewis acid and in the presence of catalytic quantities of a phosphine derivative.
摘要翻译：本发明涉及一种制备式（I）的邻氯甲基苯甲酰氯的方法，其中R 1至R 4可以相同或不同，表示氢 C 1 -C 4烷基，卤素或三氟甲基，通过反应式（II）的苯并稠合内酯，其中R 1至R 4， SUP> 4 具有上述含义，与亚硫酰氯。本发明的方法的特征在于反应在催化量的路易斯酸存在下和在催化量的膦衍生物的存在下进行。

3. 发明授权

US06727385B1 Method for producing o-chloromethyl benzoic acid chlorides 失效
标题翻译：邻氯甲基苯甲酸氯化物的生产方法
公开(公告)号：US06727385B1
公开(公告)日：2004-04-27
申请号：US10130825
申请日：2002-08-12
申请人： Roland Götz , Norbert Götz , Michael Keil , Bernd Wolf , Adrian Steinmetz , Armin Stamm , Jochem Henkelmann
发明人： Roland Götz , Norbert Götz , Michael Keil , Bernd Wolf , Adrian Steinmetz , Armin Stamm , Jochem Henkelmann
IPC分类号： C07C5536
CPC分类号： C07C51/60 , C07C63/04 , C07C63/10
摘要： A process for preparing o-chloromethylbenzoyl chlorides of the formula I, in which R1 to R4 can be identical or different and are hydrogen, C1-C4-alkyl, halogen or trifluoromethyl, by reacting benzo-fused lactones of the formula II, in which R1 to R4 are as defined above, with thionyl chloride, which comprises carrying out the reaction in the presence of catalytic amounts of boric acid, boric anhydride, borate, boronic acid or boronic acid esters and catalytic amounts of a quaternary ammonium salt is described.
摘要翻译：制备式I的邻氯甲基苯甲酰氯的方法，其中R 1至R 4可以相同或不同，并且是氢，C 1 -C 4 - 烷基，卤素或三氟甲基，通过使苯并稠合的内酯与其中R 1至R 4如上所定义的式II与亚硫酰氯反应，其包括在催化量的硼酸，硼酸酐，硼酸盐，硼酸或硼酸的存在下进行反应描述了酯和催化量的季铵盐。

4. 发明授权

US08541611B2 Bifunctional phenyl iso(thio)cyanates, processes and intermediates products for their preparation 失效
标题翻译：双官能苯基异（硫代）氰酸酯，其制备方法和中间体产品
公开(公告)号：US08541611B2
公开(公告)日：2013-09-24
申请号：US13535544
申请日：2012-06-28
申请人： Gerhard Hamprecht , Michael Puhl , Bernd Wolf , Norbert Götz , Michael Keil , Robert Reinhard , Ingo Sagasser , Werner Seitz
发明人： Gerhard Hamprecht , Michael Puhl , Bernd Wolf , Norbert Götz , Michael Keil , Robert Reinhard , Ingo Sagasser , Werner Seitz
IPC分类号： C07C331/28
CPC分类号： C07D213/76 , C07C303/34 , C07C307/06 , C07C331/28 , C07C2601/14 , C07D207/20 , C07D211/18 , C07D211/70 , C07D295/26 , C07D307/52 , C07D319/06 , C07D333/20
摘要： A process for preparing phenyl iso(thio)cyanates of the formula I in which a compound of the formula II or its HCl adduct is reacted with a phosgenating agent where W is oxygen or sulfur and Ar and A are as defined in claim 1 is described. Moreover, the invention relates to the use of the phenyl iso(thio)cyanates for preparing crop protection agents.
摘要翻译：描述式I的苯基异（硫代）氰酸酯的方法，其中将式II化合物或其HCl加合物与W是氧或硫的光气反应剂和Ar和A如权利要求1中所定义的相同。此外，本发明涉及苯基异（硫代）氰酸酯用于制备作物保护剂的用途。

5. 发明授权

US07820846B2 Bifunctional phenyliso(thio)cyanates, processes and intermediates products for their preparation 有权
标题翻译：双官能苯基（硫代）氰酸酯，其制备方法和中间体产品
公开(公告)号：US07820846B2
公开(公告)日：2010-10-26
申请号：US10532931
申请日：2003-10-29
申请人： Gerhard Hamprecht , Michael Puhl , Bernd Wolf , Norbert Götz , Michael Keil , Robert Reinhard , Ingo Sagasser , Werner Seitz
发明人： Gerhard Hamprecht , Michael Puhl , Bernd Wolf , Norbert Götz , Michael Keil , Robert Reinhard , Ingo Sagasser , Werner Seitz
IPC分类号： C07C255/50
CPC分类号： C07D213/76 , C07C303/34 , C07C307/06 , C07C331/28 , C07C2601/14 , C07D207/20 , C07D211/18 , C07D211/70 , C07D295/26 , C07D307/52 , C07D319/06 , C07D333/20
摘要： A process for preparing phenyl iso(thio)cyanates of the formula I in which a compound of the formula II or its HCl adduct is reacted with a phosgenating agent where W is oxygen or sulfur and Ar and A are as defined in claim 1 is described. Moreover, the invention relates to the use of the phenyl iso(thio)cyanates for preparing crop protection agents.
摘要翻译：描述式I的苯基异（硫代）氰酸酯的方法，其中将式II化合物或其HCl加合物与W是氧或硫的光气反应剂和Ar和A如权利要求1中所定义的相同。此外，本发明涉及苯基异（硫代）氰酸酯用于制备作物保护剂的用途。

6. 发明申请

US20120271049A1 BIFUNCTIONAL PHENYL ISO (THIO) CYANATES, PROCESSES AND INTERMEDIATES PRODUCTS FOR THEIR PREPARATION 失效
标题翻译：双功能PHENYL ISO（THIO）氰化物，工艺和中间体产品的制备
公开(公告)号：US20120271049A1
公开(公告)日：2012-10-25
申请号：US13535544
申请日：2012-06-28
申请人： Gerhard Hamprecht , Michael Puhl , Bernd Wolf , Norbert Götz , Michael Keil , Robert Reinhard , Ingo Sagasser , Werner Seitz
发明人： Gerhard Hamprecht , Michael Puhl , Bernd Wolf , Norbert Götz , Michael Keil , Robert Reinhard , Ingo Sagasser , Werner Seitz
IPC分类号： C07C303/34 , C07D317/28 , C07D307/52 , C07C331/28 , C07D213/76 , C07D295/26 , C07D207/48 , C07D211/96 , C07C307/06 , C07D333/20
CPC分类号： C07D213/76 , C07C303/34 , C07C307/06 , C07C331/28 , C07C2601/14 , C07D207/20 , C07D211/18 , C07D211/70 , C07D295/26 , C07D307/52 , C07D319/06 , C07D333/20
摘要： A process for preparing phenyl iso(thio)cyanates of the formula I in which a compound of the formula II or its HCl adduct is reacted with a phosgenating agent where W is oxygen or sulfur and Ar and A are as defined in claim 1 is described.Moreover, the invention relates to the use of the phenyl iso(thio)cyanates for preparing crop protection agents.
摘要翻译：描述式I的苯基异（硫代）氰酸酯的方法，其中将式II化合物或其HCl加合物与W是氧或硫的光气反应剂和Ar和A如权利要求1中所定义的相同。此外，本发明涉及苯基异（硫代）氰酸酯用于制备作物保护剂的用途。

7. 发明申请

US20110009640A1 BIFUNCTIONAL PHENYL ISO (THIO) CYANATES, PROCESSES AND INTERMEDIATES FOR THEIR PREPARATION 有权
标题翻译：双功能苯乙烯（THIO）氰化物，其制备方法和中间体
公开(公告)号：US20110009640A1
公开(公告)日：2011-01-13
申请号：US12886986
申请日：2010-09-21
申请人： Gerhard Hamprecht , Michael Puhl , Bernd Wolf , Norbert Götz , Michael Keil , Robert Reinhard , Ingo Sagasser , Werner Seitz
发明人： Gerhard Hamprecht , Michael Puhl , Bernd Wolf , Norbert Götz , Michael Keil , Robert Reinhard , Ingo Sagasser , Werner Seitz
IPC分类号： C07D249/14 , C07C263/10 , C07C331/28 , C07C265/12 , C07D249/12 , C07C307/02
CPC分类号： C07D213/76 , C07C303/34 , C07C307/06 , C07C331/28 , C07C2601/14 , C07D207/20 , C07D211/18 , C07D211/70 , C07D295/26 , C07D307/52 , C07D319/06 , C07D333/20
摘要： A process for preparing phenyl iso(thio)cyanates of the formula I in which a compound of the formula II or its HCl adduct is reacted with a phosgenating agent where W is oxygen or sulfur and Ar and A are as defined in claim 1 is described.Moreover, the invention relates to the use of the phenyl iso(thio)cyanates for preparing crop protection agents.
摘要翻译：描述式I的苯基异（硫代）氰酸酯的方法，其中将式II化合物或其HCl加合物与W是氧或硫的光气反应剂和Ar和A如权利要求1中所定义的相同。此外，本发明涉及苯基异（硫代）氰酸酯用于制备作物保护剂的用途。

8. 发明授权

US08232421B2 Bifunctional phenyl ISO (THIO) cyanates, processes and intermediates for their preparation 有权
标题翻译：双官能苯基ISO（THIO）氰酸酯，其制备方法和中间体
公开(公告)号：US08232421B2
公开(公告)日：2012-07-31
申请号：US12886986
申请日：2010-09-21
申请人： Gerhard Hamprecht , Michael Puhl , Bernd Wolf , Norbert Götz , Michael Keil , Robert Reinhard , Ingo Sagasser , Werner Seitz
发明人： Gerhard Hamprecht , Michael Puhl , Bernd Wolf , Norbert Götz , Michael Keil , Robert Reinhard , Ingo Sagasser , Werner Seitz
IPC分类号： C07C263/10 , C07C249/14 , C07C331/28 , C07C265/12 , C07D249/12
CPC分类号： C07D213/76 , C07C303/34 , C07C307/06 , C07C331/28 , C07C2601/14 , C07D207/20 , C07D211/18 , C07D211/70 , C07D295/26 , C07D307/52 , C07D319/06 , C07D333/20
摘要： A process for preparing phenyl iso(thio)cyanates of the formula I in which a compound of the formula II or its HCl adduct is reacted with a phosgenating agent where W is oxygen or sulfur and Ar and A are as defined in claim 1 is described. Moreover, the invention relates to the use of the phenyl iso(thio)cyanates for preparing crop protection agents.
摘要翻译：描述式I的苯基异（硫代）氰酸酯的方法，其中将式II化合物或其HCl加合物与W是氧或硫的光气反应剂和Ar和A如权利要求1中所定义的相同。此外，本发明涉及苯基异（硫代）氰酸酯用于制备作物保护剂的用途。

9. 发明授权

US06680410B2 Method for producing oxime ethers 失效
标题翻译：生产肟醚的方法
公开(公告)号：US06680410B2
公开(公告)日：2004-01-20
申请号：US10257327
申请日：2002-10-10
申请人： Roland Götz , Bernd Wolf , Michael Rack
发明人： Roland Götz , Bernd Wolf , Michael Rack
IPC分类号： C07C25156
CPC分类号： C07C249/12 , C07C251/38
摘要： A process for preparing oxime ethers of the formula I, in which the substituents R1 and R2 can be identical or different and can each be cyano, alkyl, haloalkyl, cycloalkyl, phenyl and naphthyl, and R3 can be alkyl, by alkylation of oximes of the formula II under basic conditions with an alkylating agent from the group of alkyl halides, dialkyl sulfates and dialkyl carbonates, wherein the reaction is carried out in a mixture consisting of 5 to 25% by weight of polar aprotic solvents selected from the group of nitrites, N-alkylpyrrolidones, cyclic urea derivatives, dimethylformamide and dimethylacetamide, 55 to 95% by weight of nonpolar solvents selected from the group of aliphatic hydrocarbons, aromatic hydrocarbons, alkyl alkylcarboxylates and ethers, and 0 to 25% by weight of water, the contents thereof totaling 100%.
摘要翻译：制备式I的肟醚的方法，其中取代基R 1和R 2可以相同或不同，并且各自可以是氰基，烷基，卤代烷基，环烷基，苯基和萘基，R 3，可以通过烷基化剂从烷基卤化物，二烷基硫酸盐和碳酸二烷基酯在碱性条件下将式II的肟烷基化，其中该反应以5至25重量％的极性非质子选自亚硝酸盐，N-烷基吡咯烷酮，环脲衍生物，二甲基甲酰胺和二甲基乙酰胺的溶剂，55至95重量％的选自脂族烃，芳烃，烷基烷基羧酸盐和醚的非极性溶剂，和0至25％水重量，总含量为100％。

10. 发明授权

US06441236B1 Method for preparing trion-bis(oxime ether) derivatives andrion-mono and trion-bis(oxime ether) derivatives obtained therewith 有权
标题翻译：制备得到的三 - 双（肟醚）衍生物和单 - 和三 - 双（肟醚）衍生物的方法
公开(公告)号：US06441236B1
公开(公告)日：2002-08-27
申请号：US09787950
申请日：2001-03-23
申请人： Thomas Grote , Bernd Wolf , Michael Rack , Roland Götz , Andreas Gypser , Adrian Steinmetz , Hubert Sauter , Michael Keil , Horst Mayer
发明人： Thomas Grote , Bernd Wolf , Michael Rack , Roland Götz , Andreas Gypser , Adrian Steinmetz , Hubert Sauter , Michael Keil , Horst Mayer
IPC分类号： C07C24900
CPC分类号： C07C251/38 , C07C249/08 , C07D317/28 , C07D319/06
摘要： The present invention relates to a method for the production of trion-bis(oxime ether) derivatives of formula (I), wherein the substituents have the following meaning: R1, R3 represent unsubstituted, partially or totally halogenated C1-C6-alkyl or C3-C6-cycloalkyl; R2, R4 represent C1-C4-alkyl or a methyl substituted by C2-C4-alkenyl, C2-C4-alkinyl or phenyl and X represents oxygen or N—OH. The invention also relates to the intermediate products obtained with said method.
摘要翻译：本发明涉及制备式（I）的三 - 双（肟醚）衍生物的方法，其中取代基具有以下含义：R 1，R 3表示未取代的，部分或全部卤代的C 1 -C 6烷基或C 3 -C 6-环烷基 R 2，R 4表示C 1 -C 4 - 烷基或被C 2 -C 4 - 烯基，C 2 -C 4 - 炔基或苯基取代的甲基，X表示氧或N-OH。本发明还涉及用所述方法获得的中间产物。

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