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1. 发明授权

US06277917B1 Powder coating compositions and coated substrates with multilayered coatings 失效
标题翻译：粉末涂料组合物和具有多层涂层的涂布基材
公开(公告)号：US06277917B1
公开(公告)日：2001-08-21
申请号：US09326921
申请日：1999-06-07
申请人： Anton Jurgetz , Karen B. Allen , John M. Furar , Kurt A. Humbert , Charles M. Kania , Stephen G. McQuown , Karen S. Rechenberg
发明人： Anton Jurgetz , Karen B. Allen , John M. Furar , Kurt A. Humbert , Charles M. Kania , Stephen G. McQuown , Karen S. Rechenberg
IPC分类号： C09D13314
CPC分类号： B05D7/532 , B05D7/534 , B05D7/572 , C08L33/068 , C08L73/02 , C08L2205/02 , C09D133/068 , Y10S525/934 , Y10T428/31504 , C08L2666/04 , C08L2666/28 , C08L2666/02
摘要： Curable powder clear coating composition and coated substrate with multilayered coatings have as the predominant film-forming polymer in the coating at least one epoxy acrylic copolymer in an amount from 60 to 99.99 percent by weight and 10 to 40 percent by weight of a polycarboxylic acid crosslinking agent. The percentages by weight are based on solids of the curable coating composition. A single predominant film-forming epoxy acrylic copolymer has a number average molecular weight in the range of about 1000 to 5500; a calculated Tg in the range of 50 to 85° C.; epoxy content in the range of 35 to 85, and a styrene content resulting from an amount of styrene monomer in the range of up to about 25 weight percent based on the weight percent of the monomers to form the copolymer. The blend of epoxy acrylic copolymer has one polymer which is the single epoxy acrylic copolymer or one having a number average molecular weight in the range of about 1000 to about 10,000, a calculated Tg in the range of about 40° C. to 85° C., and an epoxy content from 40 to 60 weight percent of the total weight of the monomers to prepare the epoxy acrylic copolymer. The other polymer of the blend has a number average molecular weight in the range of about 500 to about 3000, a calculated Tg in the range of about 35° C. to about 125° C., and an epoxy content from glycidyl functional ethylenically unsaturated monomer that is higher than that of the first epoxy functional acrylic copolymer of the blend and in the range of about 50 to about 100.
摘要翻译：可固化的粉末透明涂料组合物和具有多层涂料的涂布基材在涂层中具有作为主要成膜聚合物的至少一种环氧丙烯酸共聚物，其量为60至99.99重量％，10至40重量％的多元羧酸交联代理商重量百分比是基于可固化涂料组合物的固体。单一主要的成膜环氧丙烯酸共聚物的数均分子量在约1000至5500的范围内; 计算的Tg在50至85℃的范围内。环氧含量在35至85范围内，苯乙烯含量由苯乙烯单体的量的至多约25重量％范围内，基于形成共聚物的单体的重量百分数。环氧丙烯酸共聚物的共混物具有一种聚合物，其是单环氧丙烯酸共聚物或具有数均分子量在约1000至约10,000范围内的聚合物，计算的Tg在约40℃至85℃的范围内，并且环氧树脂含量为单体总重量的40至60重量％，以制备环氧丙烯酸共聚物。共混物的其它聚合物的数均分子量在约500至约3000的范围内，计算的Tg在约35℃至约125℃的范围内，并且来自缩水甘油基官能烯属不饱和的环氧基含量单体，高于共混物的第一环氧官能丙烯酸共聚物的单体，并且在约50至约100的范围内。

2. 发明授权

US06863982B2 Curable film-forming composition exhibiting improved yellowing resistance 失效
标题翻译：具有改善耐黄变性的可固化成膜组合物
公开(公告)号：US06863982B2
公开(公告)日：2005-03-08
申请号：US10269389
申请日：2002-10-11
申请人： Masayuki Nakajima , Charles M. Kania , Stephen G. McQuown , Karen S. Rechenberg , Susan A. Campbell , Kurt A. Humbert , Karen A. Barkac
发明人： Masayuki Nakajima , Charles M. Kania , Stephen G. McQuown , Karen S. Rechenberg , Susan A. Campbell , Kurt A. Humbert , Karen A. Barkac
IPC分类号： C08G59/30 , C08G59/32 , C08G59/42 , C09D5/03 , C09D7/12 , C09D163/00 , B32B27/38
CPC分类号： C09D163/00 , C08G59/304 , C08G59/3254 , C08G59/4284 , C09D5/036 , C09D7/63 , Y10T428/31511 , C08L2666/02
摘要： A curable film-forming composition of 5 to 95 weight percent (based on the total resin solids weight in the composition) of a crosslinking agent; 5 to 95 weight percent ot a polymer containing functional groups reactive with the crosslinking agent; and 0.01 to 15 weight percent of at least one additive selected from a reaction product of phosporous acid and: at least one diepoxide; at least one diepoxide and at least one anhydride; at least one diepoxide and at least one anhydride, chain extended with at least one diol; at least one monoepoxide and at least one anhydride, chain extended with at least one diepoxide; and mixtures thereof. The additives in the composition prevent thermal oxidation, minimizing visual effects (i.e., yellowing). A multi-component composite coating includes a base coat and a top coat which may be derived from the above curable film-forming composition.
摘要翻译：交联剂为5〜95重量％（基于组合物中树脂固体重量的总量）的可固化成膜组合物; 5至95重量％的含有与交联剂反应的官能团的聚合物; 和0.01至15重量％的至少一种选自磷酸和：至少一种二环氧化物的反应产物的添加剂; 至少一种二环氧化物和至少一种酸酐; 至少一种二环氧化物和至少一种酸酐，链与至少一种二醇延伸; 至少一种单环氧化物和至少一种酸酐，链与至少一种二环氧化物延伸; 及其混合物。组合物中的添加剂防止热氧化，使视觉效果最小化（即变黄）。多组分复合涂层包括底涂层和可以由上述可固化成膜组合物衍生的面漆。

3. 发明授权

US07132477B2 Powder coating compositions 失效
标题翻译：粉末涂料组合物
公开(公告)号：US07132477B2
公开(公告)日：2006-11-07
申请号：US10928902
申请日：2004-08-27
申请人： Kurt A. Humbert , Karen S. Rechenberg , Edward R. Coleridge , Charles M. Kania , Paul H. Lamers
发明人： Kurt A. Humbert , Karen S. Rechenberg , Edward R. Coleridge , Charles M. Kania , Paul H. Lamers
IPC分类号： C08F8/00
CPC分类号： C09D5/033 , B05D1/007 , B05D3/0209 , B05D3/067 , B05D7/53 , B05D7/57 , C08F8/00 , C08F210/10 , C08F220/06 , C08F220/10 , C08F220/32 , C08F290/046 , C08G18/6229 , C08G18/6254 , C08G18/792 , C08G18/798 , C08G18/8025 , C08G18/807 , C08G18/8074 , C08G59/4261 , C08G2150/20 , C08L33/02 , C08L33/04 , C08L33/068 , C08L2312/00 , C09D123/22 , C09D133/062 , C09D133/068 , C09D133/08 , C09D163/00 , Y10T428/31855 , C08L2666/04 , C08F220/00 , C08F2500/26 , C08F220/12 , C08F210/00 , C08L2666/28 , C08L2666/02 , C08F212/00 , C08F222/00 , C08F214/18 , C08F2500/03 , C08F2500/02
摘要： A thermosetting composition that includes a co-reactable solid, particulate mixture of a film forming material having functional groups, a crosslinking agent having at least two functional groups that are reactive with the functional groups in the film forming material, and a monocarboxylic acid. Multi-component composite coatings, coated substrates, and related methods are also provided.
摘要翻译：一种热固性组合物，其包含可共反应的固体，具有官能团的成膜材料的颗粒混合物，具有至少两个与成膜材料中的官能团反应的官能团的交联剂和一元羧酸。还提供了多组分复合涂层，涂覆的基材和相关方法。

4. 发明授权

US08901198B2 UV-curable coating compositions, multi-component composite coatings, and related coated substrates 有权
标题翻译：紫外光固化涂料组合物，多组分复合涂料和相关的涂布基材
公开(公告)号：US08901198B2
公开(公告)日：2014-12-02
申请号：US12940168
申请日：2010-11-05
申请人： Charles M. Kania , Kenneth T. Phelps , Kurt A. Humbert , Todd M. Roper , Jiping Shao , David C. Martin
发明人： Charles M. Kania , Kenneth T. Phelps , Kurt A. Humbert , Todd M. Roper , Jiping Shao , David C. Martin
IPC分类号： C08F2/50 , C08J3/28 , C08F2/48 , C08F2/46 , C08G18/79 , C09D175/16 , C08G18/67 , C08G18/32
CPC分类号： C08G18/792 , C08F2/48 , C08G18/3206 , C08G18/672 , C09D175/16
摘要： Disclosed herein are solventborne liquid UV-curable coating compositions comprising: a radiation curable compound comprising an acrylate-terminated compound having greater than two unsaturated sites, wherein the acrylate-terminated compound comprises a reaction product of reactants comprising: an adduct of a polyisocyanate, wherein the adduct of a polyisocyanate comprises a reaction product of reactants comprising a polyisocyanate comprising greater than two isocyanate groups and a compound having groups reactive with the isocyanate groups of the polyisocyanate; and an active hydrogen-containing acrylate; and a photoinitiator composition that includes a first photoinitiator composition for providing surface cure and a second photoinitiator composition for providing through cure of the resultant coating layer. Also disclosed are related multi-component composite coatings, coated substrates, and methods for coating a substrate.
摘要翻译：本文公开了溶剂型液体UV可固化涂料组合物，其包含：包含具有大于两个不饱和位点的丙烯酸酯封端的化合物的可辐射固化化合物，其中所述丙烯酸酯封端的化合物包含反应物的反应产物，其包含：多异氰酸酯的加合物，其中多异氰酸酯的加成物包括包含多于两个异氰酸酯基的多异氰酸酯和具有与多异氰酸酯的异氰酸酯基反应的基团的化合物的反应物的反应产物; 和含活性氢的丙烯酸酯; 以及光引发剂组合物，其包括用于提供表面固化的第一光引发剂组合物和用于通过固化所得涂层提供的第二光引发剂组合物。还公开了相关的多组分复合涂层，涂覆的基底和用于涂覆基底的方法。

5. 发明申请

US20120115975A1 UV-Curable Coating Compositions, Multi-Component Composite Coatings, and Related Coated Substrates 有权
标题翻译： UV可固化涂料组合物，多组分复合涂料和相关涂层基材
公开(公告)号：US20120115975A1
公开(公告)日：2012-05-10
申请号：US12940168
申请日：2010-11-05
申请人： Charles M. Kania , Kenneth T. Phelps , Kurt A. Humbert , Todd M. Roper , Jiping Shao , David C. Martin
发明人： Charles M. Kania , Kenneth T. Phelps , Kurt A. Humbert , Todd M. Roper , Jiping Shao , David C. Martin
IPC分类号： C09D175/00 , C08F2/46
CPC分类号： C08G18/792 , C08F2/48 , C08G18/3206 , C08G18/672 , C09D175/16
摘要： Disclosed herein are solventborne liquid UV-curable coating compositions comprising: a radiation curable compound comprising an acrylate-terminated compound having greater than two unsaturated sites, wherein the acrylate-terminated compound comprises a reaction product of reactants comprising: an adduct of a polyisocyanate, wherein the adduct of a polyisocyanate comprises a reaction product of reactants comprising a polyisocyanate comprising greater than two isocyanate groups and a compound having groups reactive with the isocyanate groups of the polyisocyanate; and an active hydrogen-containing acrylate; and a photoinitiator composition that includes a first photoinitiator composition for providing surface cure and a second photoinitiator composition for providing through cure of the resultant coating layer. Also disclosed are related multi-component composite coatings, coated substrates, and methods for coating a substrate.
摘要翻译：本文公开了溶剂型液体UV可固化涂料组合物，其包含：包含具有大于两个不饱和位点的丙烯酸酯封端的化合物的可辐射固化化合物，其中所述丙烯酸酯封端的化合物包含反应物的反应产物，其包含：多异氰酸酯的加合物，其中多异氰酸酯的加成物包括包含多于两个异氰酸酯基的多异氰酸酯和具有与多异氰酸酯的异氰酸酯基反应的基团的化合物的反应物的反应产物; 和含活性氢的丙烯酸酯; 以及光引发剂组合物，其包括用于提供表面固化的第一光引发剂组合物和用于通过固化所得涂层提供的第二光引发剂组合物。还公开了相关的多组分复合涂层，涂覆的基底和用于涂覆基底的方法。

6. 发明授权

US5939195A Color-plus-clear composite coating and process and coated article for improved properties 失效
标题翻译：彩色 - 透明复合涂层和工艺和涂层制品，以提高性能
公开(公告)号：US5939195A
公开(公告)日：1999-08-17
申请号：US803568
申请日：1997-02-20
申请人： Karen B. Allen , Kurt A. Humbert , Kurt G. Olson , Edward R. Coleridge , Roxalana L. Martin
发明人： Karen B. Allen , Kurt A. Humbert , Kurt G. Olson , Edward R. Coleridge , Roxalana L. Martin
IPC分类号： B05D7/00 , C09D163/00 , C09D201/02 , B32B27/38
CPC分类号： B05D7/534 , C09D163/00 , C09D201/02 , Y10T428/31511
摘要： A composite coating of a water-borne basecoat and an epoxy-acid clearcoat has improved performance characteristics of reduced yellowing or reduced tendency to chip through the formulation of the composite coating and the process for its application. The process comprises applying to the substrate a film-forming composition to form a basecoat and applying to the basecoat an epoxy-acid clear film-forming composition to form a transparent topcoat over the basecoat. The basecoat is a coating composition comprising a polymeric film-forming resin, aminoplast crosslinking agent and a pigment wherein the crosslinking agent is a partially or fully alkylated aminoplast and has a lower or higher imino content. The lower imino content promotes reduced yellowing of the clearcoat and the higher imino content promotes improved chip resistance when the pigment of the water-borne basecoat reduces yellowing effects. The transparent topcoat, or clearcoat, has an epoxy film forming resin and a polycarboxylic acid crosslinking agent.
摘要翻译：水性底涂层和环氧 - 酸性透明涂层的复合涂层具有改善的性能特征，其通过复合涂层的配方及其应用的方法减少黄化或降低芯片的趋势。该方法包括将成膜组合物施用到基底上以形成底涂层，并向底漆涂布环氧树脂透明成膜组合物，以在底涂层上形成透明的面漆。底漆是包含聚合物成膜树脂，氨基塑料交联剂和颜料的涂料组合物，其中交联剂是部分或全部烷基化的氨基塑料并具有较低或更高的亚氨基含量。较低的亚氨基含量促进透明涂层的减少黄化，当水性底漆的颜料降低黄变效应时，较高的亚氨基含量促进改善的耐碎屑性。透明面漆或透明涂料具有环氧树脂成膜树脂和多元羧酸交联剂。

7. 发明授权

US06265489B1 Thermosetting compositions containing carboxylic acid functional polymers prepared by atom transfer radical polymerization 失效
标题翻译：含有通过原子转移自由基聚合制备的羧酸官能聚合物的热固性组合物
公开(公告)号：US06265489B1
公开(公告)日：2001-07-24
申请号：US09375017
申请日：1999-08-16
申请人： Karen A. Barkac , Simion Coca , James R. Franks , Kurt A. Humbert , Paul H. Lamers , Roxalana L. Martin , James B. O'Dwyer , Kurt G. Olson , Daniela White
发明人： Karen A. Barkac , Simion Coca , James R. Franks , Kurt A. Humbert , Paul H. Lamers , Roxalana L. Martin , James B. O'Dwyer , Kurt G. Olson , Daniela White
IPC分类号： C08L3302
CPC分类号： C09D133/02 , C08L63/00 , C09D133/064 , C08L2666/14
摘要： A thermosetting composition comprising a co-reactable solid, particulate mixture of (a) polycarboxylic acid functional polymer, and (b) epoxide functional crosslinking agent having at least two epoxide groups, e.g., triglycidyl isocyanurate (TGIC), is described. The polycarboxylic acid functional polymer is prepared by atom transfer radical polymerization and has well defined polymer chain architecture and polydispersity index of less than 2.0. The thermosetting compositions of the present invention have utility as powder coatings compositions.
摘要翻译：描述了包含（a）多元羧酸官能聚合物和（b）具有至少两个环氧基团的环氧官能交联剂例如三缩水甘油基异氰脲酸酯（TGIC）的共反应固体，颗粒混合物的热固性组合物。聚羧酸官能聚合物通过原子转移自由基聚合制备，并且具有良好的聚合物链结构和小于2.0的多分散指数。本发明的热固性组合物可用作粉末涂料组合物。

8. 发明申请

US20120148848A1 POLYMERIC SUBSTRATES HAVING A THIN METAL FILM AND FINGERPRINT RESISTANT CLEAR COATING DEPOSITED THEREON AND RELATED METHODS 审中-公开
标题翻译：具有薄金属薄膜和指纹电阻透明涂层的聚合物基板及其相关方法
公开(公告)号：US20120148848A1
公开(公告)日：2012-06-14
申请号：US13050118
申请日：2011-03-17
申请人： David C. Martin , Kurt A. Humbert , Brian K. Rearick
发明人： David C. Martin , Kurt A. Humbert , Brian K. Rearick
IPC分类号： B05D7/00 , B32B27/28 , B05D1/36 , B32B15/00
CPC分类号： B05D5/067 , B05D5/083 , B05D2350/65 , Y10T428/3154 , Y10T428/31678
摘要： Disclosed are methods of coating a polymeric substrate. The methods include (a) depositing a thin metal film onto the polymeric substrate, and (b) depositing a transparent radiation curable film-forming composition onto a thin metal film, wherein the transparent radiation curable film-forming composition comprises a fluorine-containing radiation curable compound.
摘要翻译：公开了涂覆聚合物基材的方法。所述方法包括：（a）在所述聚合物基材上沉积薄金属膜，和（b）将透明的可辐射固化成膜组合物沉积到薄金属膜上，其中所述透明可辐射固化膜形成组合物包含含氟辐射可固化化合物。

9. 发明授权

US06313224B1 Coating of film-forming resin and functional flow control copolymer 失效
标题翻译：成膜树脂和功能流动控制共聚物的涂层
公开(公告)号：US06313224B1
公开(公告)日：2001-11-06
申请号：US09437891
申请日：1999-11-09
申请人： Debra L. Singer , Kurt G. Olson , Kurt A. Humbert , Karen A. Barkac , Mark E. Wozniak
发明人： Debra L. Singer , Kurt G. Olson , Kurt A. Humbert , Karen A. Barkac , Mark E. Wozniak
IPC分类号： C08L2304
CPC分类号： C09D201/00 , C09D7/47 , Y10T428/31692 , C08L2666/04
摘要： Curable coating compositions comprising either a liquid or particulate curable film-forming resinous material, a flow control agent which is a copolymer and optionally a carrier for the liquid resinous material. The copolymer is from at least one non-amino, non-hydroxyl and non-acid functional alkyl acrylate or methacrylate containing from 1 to 20 carbon atoms in the alkyl group, and functional monomer of either (i) amino functional acrylates and methacrylates in an effective amount to give the copolymer an amine value in the range from 2 to 70, or (ii) acid functional acrylate and methacrylate in an effective amount to give the copolymer an acid value in the range of from 10 to 30. Additionally, with either functional monomer (i) or (ii) another functional comonomer (iii) can be present in the copolymer which is hydroxyalkyl acrylate and/or hydroxyalkyl methacrylate and/or caprolactone polyol monomer. Comonomer (iii) can be present in the copolymer in an effective amount to give the copolymer a hydroxyl number is in the range of about 0 to 100.
摘要翻译：可固化的涂料组合物包括液体或颗粒状可固化成膜树脂材料，流动控制剂，其是共聚物和任选的液体树脂材料的载体。该共聚物来自烷基中至少一个含有1-20个碳原子的非氨基，非羟基和非酸官能的丙烯酸酯或甲基丙烯酸烷基酯，和（i）氨基官能的丙烯酸酯和甲基丙烯酸酯的官能单体有效量使得共聚物的胺值在2-70范围内，或（ii）酸官能丙烯酸酯和甲基丙烯酸酯有效量，以使共聚物的酸值在10至30的范围内。另外，在丙烯酸羟烷基酯和/或甲基丙烯酸羟烷基酯和/或己内酯多元醇单体的共聚物中可以存在官能单体（i）或（ii）另一功能性共聚单体（iii）。共聚单体（iii）可以以有效的量存在于共聚物中，得到共聚物，羟值在约0-100范围内。

10. 发明授权

US06251999B1 Tin carboxylate catalysts for epoxy-acid coating compositions 失效
标题翻译：用于环氧酸涂料组合物的羧酸锡催化剂
公开(公告)号：US06251999B1
公开(公告)日：2001-06-26
申请号：US09339394
申请日：1999-06-23
申请人： Daniel E. Rardon , Kurt A. Humbert , Karen A. Barkac , Peter Kamarchik, Jr. , Mark E. Wozniak
发明人： Daniel E. Rardon , Kurt A. Humbert , Karen A. Barkac , Peter Kamarchik, Jr. , Mark E. Wozniak
IPC分类号： C08F800
CPC分类号： C09D163/00 , C07F7/2224 , C08G59/42 , C08G59/685 , C08L2666/04 , C08L2666/18
摘要： A catalytic tin carboxylate adduct, which is useful as a catalyst in epoxy-acid coating compositions, is the reaction product of (A) a mono-, di-, or poly-carboxylic acid functional compound and (B) an organotin compound containing one to three aryl groups and at least one halogen or hydroxyl group attached to the tin atom. There is also provided an epoxy-acid coating composition, which incorporates this catalytic tin carboxylate adduct. The epoxy-acid coating composition is advantageous as an automotive topcoat, particularly as a clear coat composition because it exhibits good appearance, durability, stability and generates no, or extremely low levels of benzene during the curing process.
摘要翻译：可用作环氧 - 酸性涂料组合物中的催化剂的催化锡羧酸盐加合物是（A）单羧酸官能化合物，二羧酸或多羧酸官能化合物与（B）含有一个或多个羧酸官能化合物的有机锡化合物的反应产物至三个芳基和至少一个与锡原子连接的卤素或羟基。还提供了一种环氧酸涂料组合物，其包含该催化性羧酸锡加合物。环氧酸涂料组合物作为汽车面漆是特别有利的，特别是作为透明涂料组合物，因为它在固化过程中表现出良好的外观，耐久性，稳定性和不产生或极低的苯含量。

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