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    • 2. 发明申请
    • Method for manufacturing microporous CMP materials having controlled pore size
    • 具有可控孔径的微孔CMP材料的制造方法
    • US20060052040A1
    • 2006-03-09
    • US11265607
    • 2005-11-02
    • Abaneshwar Prasad
    • Abaneshwar Prasad
    • B24B1/00
    • B24B37/24B24D3/32B24D11/001
    • A method of manufacturing a chemical-mechanical polishing (CMP) pad comprises the steps of (a) forming a layer of a polymer resin liquid solution (i.e., a polymer resin dissolved in a solvent); (b) inducing a phase separation in the layer of polymer solution to produce an interpenetrating polymeric network comprising a continuous polymer-rich phase interspersed with a continuous polymer-depleted phase in which the polymer-depleted phase constitutes about 20 to about 90 percent of the combined volume of the phases; (c) solidifying the continuous polymer-rich phase to form a porous polymer sheet; (d) removing at least a portion of the polymer-depleted phase from the porous polymer sheet; and (e) forming a CMP pad therefrom. The method provides for microporous CMP pads having a porosity and pore size that can be readily controlled by selecting the concentration polymer resin in the polymer solution, selecting the solvent based on the solubility parameters of the polymer in the solvent polarity of solvent, selecting the conditions for phase separation, and the like.
    • 一种制造化学机械抛光(CMP)垫的方法包括以下步骤:(a)形成聚合物树脂液体溶液层(即溶解在溶剂中的聚合物树脂); (b)在聚合物溶液层中诱导相分离以产生互穿聚合物网络,其包含富含连续聚合物的相连续的聚合物贫化相,其中聚合物贫化相构成约20至约90% 相的组合体积; (c)固化连续富聚合物相以形成多孔聚合物片; (d)从所述多孔聚合物片中除去所述聚合物贫化相的至少一部分; 和(e)从其形成CMP垫。 该方法提供具有孔隙率和孔径的微孔CMP垫,其可以通过选择聚合物溶液中的聚合物树脂浓度来容易地控制,基于聚合物在溶剂的溶剂极性中的溶解度参数选择溶剂,选择条件 用于相分离等。
    • 7. 发明授权
    • Method for manufacturing microporous CMP materials having controlled pore size
    • 具有可控孔径的微孔CMP材料的制造方法
    • US07311862B2
    • 2007-12-25
    • US11265607
    • 2005-11-02
    • Abaneshwar Prasad
    • Abaneshwar Prasad
    • C08J9/28
    • B24B37/24B24D3/32B24D11/001
    • A method of manufacturing a chemical-mechanical polishing (CMP) pad comprises the steps of (a) forming a layer of a polymer resin liquid solution (i.e., a polymer resin dissolved in a solvent); (b) inducing a phase separation in the layer of polymer solution to produce an interpenetrating polymeric network comprising a continuous polymer-rich phase interspersed with a continuous polymer-depleted phase in which the polymer-depleted phase constitutes about 20 to about 90 percent of the combined volume of the phases; (c) solidifying the continuous polymer-rich phase to form a porous polymer sheet; (d) removing at least a portion of the polymer-depleted phase from the porous polymer sheet; and (e) forming a CMP pad therefrom. The method provides for microporous CMP pads having a porosity and pore size that can be readily controlled by selecting the concentration polymer resin in the polymer solution, selecting the solvent based on the solubility parameters of the polymer in the solvent polarity of solvent, selecting the conditions for phase separation, and the like.
    • 一种制造化学机械抛光(CMP)垫的方法包括以下步骤:(a)形成聚合物树脂液体溶液层(即溶解在溶剂中的聚合物树脂); (b)在聚合物溶液层中诱导相分离以产生互穿聚合物网络,其包含富含连续聚合物的相连续的聚合物贫化相,其中聚合物贫化相构成约20至约90% 相的组合体积; (c)固化连续富聚合物相以形成多孔聚合物片; (d)从所述多孔聚合物片中除去所述聚合物贫化相的至少一部分; 和(e)从其形成CMP垫。 该方法提供具有孔隙率和孔径的微孔CMP垫,其可以通过选择聚合物溶液中的聚合物树脂浓度来容易地控制,基于聚合物在溶剂的溶剂极性中的溶解度参数选择溶剂,选择条件 用于相分离等。
    • 9. 发明申请
    • Polishing pad with microporous regions
    • 具有微孔区域的抛光垫
    • US20060046622A1
    • 2006-03-02
    • US10931908
    • 2004-09-01
    • Abaneshwar Prasad
    • Abaneshwar Prasad
    • B24B1/00
    • B24B37/26
    • The invention provides a polishing pad for chemical-mechanical polishing comprising a polymeric material comprising two or more adjacent regions, wherein the regions have the same polymer formulation and the transition between the regions does not include a structurally distinct boundary. In a first embodiment, a first region and a second adjacent region have a first and second non-zero void volume, respectively, wherein the first void volume is less than the second void volume. In a second embodiment, a first non-porous region is adjacent to a second adjacent porous region, wherein the second region has an average pore size of about 50 μm or less. In a third embodiment, at least two of an optically transmissive region, a first porous region, and an optional second porous region, are adjacent. The invention further provides methods of polishing a substrate comprising the use of the polishing pads and a method of producing the polishing pads.
    • 本发明提供了一种用于化学机械抛光的抛光垫,其包括包含两个或更多个相邻区域的聚合物材料,其中所述区域具有相同的聚合物配方,并且所述区域之间的转变不包括结构上不同的边界。 在第一实施例中,第一区域和第二相邻区域分别具有第一和第二非零空隙体积,其中第一空隙体积小于第二空隙体积。 在第二实施方案中,第一非多孔区域与第二相邻的多孔区域相邻,其中第二区域的平均孔径为约50μm或更小。 在第三实施例中,光学透射区域,第一多孔区域和任选的第二多孔区域中的至少两个相邻。 本发明还提供了抛光包括使用抛光垫的衬底的方法以及制造抛光垫的方法。