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1. 发明授权

US09193666B2 Process for preparing alkanolamines by homogeneously catalyzed alcohol amination 有权
标题翻译：通过均匀催化醇胺化制备链烷醇胺的方法
公开(公告)号：US09193666B2
公开(公告)日：2015-11-24
申请号：US13415409
申请日：2012-03-08
申请人： Thomas Schaub , Boris Buschhaus , Marion Kristina Brinks , Mathias Schelwies , Rocco Paciello , Johann-Peter Melder , Martin Merger
发明人： Thomas Schaub , Boris Buschhaus , Marion Kristina Brinks , Mathias Schelwies , Rocco Paciello , Johann-Peter Melder , Martin Merger
IPC分类号： C07C209/66 , C07F15/00 , C07C209/16 , C07C213/02 , C07D207/02 , C07D207/20 , C07D295/027 , C07D307/52
CPC分类号： C07C209/16 , C07C213/02 , C07D207/02 , C07D207/20 , C07D295/027 , C07D307/52 , C07C211/09 , C07C215/08 , C07C217/08 , C07C211/10 , C07C211/12
摘要： Process for preparing alkanolamines which have a primary amino group (—NH2) and a hydroxyl group (—OH) by alcohol amination of diols having two hydroxyl groups (—OH) by means of ammonia with elimination of water, wherein the reaction is carried out homogeneously catalyzed in the presence of at least one complex catalyst comprising at least one element selected from groups 8, 9 and 10 of the Periodic Table and also at least one donor ligand.
摘要翻译：制备具有伯氨基（-NH 2）和羟基（-OH）的链烷醇胺的方法，其通过用氨除去水而具有两个羟基（-OH）的二醇醇胺化，其中反应进行在包含至少一种选自元素周期表第8,9和10族的元素的复合催化剂的存在下，以及至少一种供体配体均匀催化。

2. 发明申请

US20120232292A1 PROCESS FOR THE PREPARATION OF PRIMARY AMINES BY HOMOGENEOUSLY CATALYZED ALCOHOL AMINATION 有权
标题翻译：通过均相催化的醇醇胺化制备主要胺的方法
公开(公告)号：US20120232292A1
公开(公告)日：2012-09-13
申请号：US13415412
申请日：2012-03-08
申请人： Thomas SCHAUB , Boris BUSCHHAUS , Marion Kristina BRINKS , Mathias SCHELWIES , Rocco PACIELLO , Johann-Peter MELDER , Martin MERGER
发明人： Thomas SCHAUB , Boris BUSCHHAUS , Marion Kristina BRINKS , Mathias SCHELWIES , Rocco PACIELLO , Johann-Peter MELDER , Martin MERGER
IPC分类号： C07D307/52 , C07C209/16
CPC分类号： C07C209/16 , C07C213/02 , C07D207/04 , C07D207/20 , C07D295/023 , C07D307/52 , C07C211/07 , C07C211/09 , C07C215/08 , C07C217/08
摘要： Process for the preparation of primary amines which have at least one functional group of the formula (—CH2—NH2) by alcohol amination of starting materials which have at least one functional group of the formula (—CH2—OH), with ammonia, with the elimination of water, where the alcohol amination is carried out under homogeneous catalysis in the presence of at least one complex catalyst which comprises at least one element selected from groups 8 and 9 of the Periodic Table of the Elements, and also at least one phosphorus donor ligand of the general formula (I).
摘要翻译：具有至少一个式（-CH 2 -NH 2）官能团的伯胺的方法，其通过具有至少一个式（-CH 2 -OH）官能团的起始原料与氨进行醇胺化反应，与消除水，其中在均相催化下，在至少一种包含至少一种选自元素周期表第8和9族的元素的复合催化剂的存在下进行醇胺化，以及至少一种磷通式（I）的供体配体。

3. 发明申请

US20110319657A1 Process for the Preparation of Formic Acid 有权
标题翻译：制备甲酸的方法
公开(公告)号：US20110319657A1
公开(公告)日：2011-12-29
申请号：US13171598
申请日：2011-06-29
申请人： Daniel Schneider , Klaus-Dieter Mohl , Martin Schäfer , Karin Pickenäcker , Stefan Rittinger , Thomas Schaub , Joaquim Henrique Teles , Rocco Paciello , Gerd Kaibel
发明人： Daniel Schneider , Klaus-Dieter Mohl , Martin Schäfer , Karin Pickenäcker , Stefan Rittinger , Thomas Schaub , Joaquim Henrique Teles , Rocco Paciello , Gerd Kaibel
IPC分类号： C07C53/02
CPC分类号： C07C51/09 , C07C51/44 , C07C53/02
摘要： Process for obtaining formic acid by thermal separation of a stream comprising formic acid and a tertiary amine (I), in which a liquid stream comprising formic acid and a tertiary amine (I) in a molar ratio of from 0.5 to 5 is produced by combining tertiary amine (I) and a formic acid source, from 10 to 100% by weight of the secondary components present therein are separated off and formic acid is removed by distillation in a distillation apparatus at a bottom temperature of from 100 to 300° C. and a pressure of from 30 to 3000 hPa abs from the liquid stream obtained, the bottom discharge from the distillation apparatus being separated into two liquid phases and the upper liquid phase being recycled to the formic acid source and the lower liquid phase being recycled for separating off the secondary components and/or to the distillation apparatus.
摘要翻译：通过热分离包含甲酸和叔胺（I）的流来获得甲酸的方法，其中包含摩尔比为0.5至5的甲酸和叔胺（I）的液体流通过组合分离叔胺（I）和甲酸源，10至100重量％存在于其中的次要组分，并在蒸馏装置中在100-300℃的底部温度下蒸馏除去甲酸。从得到的液体流中的压力为30〜3000hPa abs，将来自蒸馏装置的底部排出物分离成两液相，将上液相再循环至甲酸源，将下液相回收分离脱离第二组分和/或蒸馏装置。

4. 发明申请

US20110294977A1 POLYALKYLENEPOLYAMINES BY HOMOGENEOUSLY CATALYZED ALCOHOL AMINATION 有权
标题翻译：聚丙烯酰胺通过均相催化的醇醇胺化
公开(公告)号：US20110294977A1
公开(公告)日：2011-12-01
申请号：US13116649
申请日：2011-05-26
申请人： Thomas SCHAUB , Boris BUSCHHAUS , Johann-Peter MELDER , Rocco PACIELLO , Stephan HUEFFER , Helmut WITTELER
发明人： Thomas SCHAUB , Boris BUSCHHAUS , Johann-Peter MELDER , Rocco PACIELLO , Stephan HUEFFER , Helmut WITTELER
IPC分类号： C08G73/02 , C07C211/22 , C07C209/16
CPC分类号： C07C209/16 , C07C213/02 , C08G73/0213 , C07C211/14 , C07C215/14
摘要： The invention relates to a process for the preparation of polyalkylenepolyamines by catalyzed alcohol amination, in which(i) aliphatic aminoalcohols are reacted with one another or (ii) aliphatic diamines or polyamines are reacted with aliphatic diols or polyols with the elimination of water in the presence of a catalyst.
摘要翻译：本发明涉及通过催化醇胺化制备聚亚烷基多胺的方法，其中（i）脂肪族氨基醇彼此反应，或（ii）脂族二胺或多胺与脂族二元醇或多元醇反应，在存在催化剂。

5. 发明申请

US20050137946A1 Use of separate rib ledgers in a computerized enterprise resource planning system 有权
标题翻译：在计算机化企业资源规划系统中使用单独的分类帐
公开(公告)号：US20050137946A1
公开(公告)日：2005-06-23
申请号：US10740558
申请日：2003-12-22
申请人： Thomas Schaub , Andreas Schaefer , Horst Schnoerer
发明人： Thomas Schaub , Andreas Schaefer , Horst Schnoerer
IPC分类号： G06Q10/00 , G06F17/60
CPC分类号： G06Q10/06 , G06Q40/00 , G06Q40/12
摘要： Enterprise management applications perform a “revenues increasing the budget” (RIB) operation on general ledger data and store elements of the general ledger data that have a RIB effect in another ledger, called the “RIB ledger”. RIB ledgers may include sets of RIB rules, storage for documents reflecting all relevant delta values together with the corresponding links to the underlying original transaction documents as well as storage for all relevant aggregated data. Accordingly, when audit operations are performed for RIB budget increases, relevant transaction data is readily available in the RIB ledger. Such copies of the data are more easily accessed than through a search of the larger set of general ledger data, thus facilitating and accelerating use of the RIB techniques in an online system.
摘要翻译：企业管理应用程序对总帐数据执行“收入增加预算”（RIB）操作，并在另一个分类帐（RIB分类帐）中存储具有RIB效应的总分类帐数据的元素。 RIB分类帐可能包括一组RIB规则，用于反映所有相关增量值的文档的存储，以及与底层原始交易文档的相应链接以及所有相关聚合数据的存储。因此，当执行RIB预算增加的审计操作时，相关的交易数据在RIB分类帐中容易获得。数据的这种副本比通过搜索较大的总分类帐数据的集合更容易地访问，从而有助于和加速在线系统中的RIB技术的使用。

6. 发明申请

US20050131807A1 Balanced budget update in the presence of rib rules 审中-公开
标题翻译：在肋骨规则的存在下平衡预算更新
公开(公告)号：US20050131807A1
公开(公告)日：2005-06-16
申请号：US10730948
申请日：2003-12-10
申请人： Andreas Schaefer , Horst Schnoerer , Thomas Schaub
发明人： Andreas Schaefer , Horst Schnoerer , Thomas Schaub
IPC分类号： G06Q40/00 , G06F17/60 , G06F17/00
CPC分类号： G06Q40/02 , G06Q20/10
摘要： A budgetary control system is described that maintains balance between revenue and expenditure budgets even when the expenditure budgets increase due to “revenues increasing the budget” (RIB) effects. RIB increases to an expenditure budget may be recorded in parallel to a revenue budget. Doing so maintains balance between the two budget data structures. During auditing operations or other control checks that examine the budget data structures for balance, RIB increases to the expenditure budget are counter-balanced by corresponding increases to the revenue budget. In the revenue budget, RIB increases may be isolated from a ‘base’ budget to ensure that the RIB increases do not effect other budgetary controls unintentionally.
摘要翻译：描述了一种预算控制系统，即使在由于“收入增加预算”（RIB）影响而导致的支出预算增加时，也会在收支预算之间保持平衡。 RIB增加到支出预算可能与收入预算并行记录。这样做在两个预算数据结构之间保持平衡。在审计业务或其他控制检查中，检查预算数据结构的余额，RIB增加到支出预算将通过相应增加收入预算来平衡。在收入预算中，RIB增加可能与“基数”预算隔离，以确保RIB增加不会无意中影响其他预算控制。

7. 发明授权

US08877965B2 Process for preparing formic acid by reaction of carbon dioxide with hydrogen 有权
标题翻译：通过二氧化碳与氢气反应制备甲酸的方法
公开(公告)号：US08877965B2
公开(公告)日：2014-11-04
申请号：US13171928
申请日：2011-06-29
申请人： Thomas Schaub , Donata Maria Fries , Rocco Paciello , Klaus-Dieter Mohl , Martin Schäfer , Stefan Rittinger , Daniel Schneider
发明人： Thomas Schaub , Donata Maria Fries , Rocco Paciello , Klaus-Dieter Mohl , Martin Schäfer , Stefan Rittinger , Daniel Schneider
IPC分类号： C07C51/15 , C07F15/00 , C07C53/00 , C07C51/44 , C07C51/48
CPC分类号： C07C51/44 , C07C51/15 , C07C51/48 , C07C53/02
摘要： A process for preparing formic acid by reaction of carbon dioxide (1) with hydrogen (2) in a hydrogenation reactor (I) in the presence of a catalyst comprising an element of group 8, 9 or 10 of the Periodic Table, a tertiary amine comprising at least 12 carbon atoms per molecule and a polar solvent comprising one or more monoalcohols selected from among methanol, ethanol, propanols and butanols, to form formic acid/amine adducts as intermediates which are subsequently thermally dissociated, where the work-up of the output (3) from the hydrogenation reactor (I) is carried out by addition of water so as to increase the distribution coefficient of the catalyst between the upper phase (4) and the lower phase.
摘要翻译：在含有元素周期表第8,9,10族元素的催化剂存在下，在氢化反应器（I）中，通过二氧化碳（1）与氢气（2）的反应制备甲酸的方法，每分子含有至少12个碳原子的极性溶剂和包含一种或多种选自甲醇，乙醇，丙醇和丁醇的一元醇的极性溶剂，以形成甲酸/胺加合物作为随后热解离的中间体，其中后处理通过加入水进行加氢反应器（I）的输出（3），以增加催化剂在上相（4）和下相之间的分配系数。

8. 发明授权

US08791297B2 Process for preparing formic acid by reaction of carbon dioxide with hydrogen 有权
标题翻译：通过二氧化碳与氢气反应制备甲酸的方法
公开(公告)号：US08791297B2
公开(公告)日：2014-07-29
申请号：US13172123
申请日：2011-06-29
申请人： Thomas Schaub , Donata Maria Fries , Rocco Paciello , Klaus-Dieter Mohl , Martin Schäfer , Stefan Rittinger , Daniel Schneider
发明人： Thomas Schaub , Donata Maria Fries , Rocco Paciello , Klaus-Dieter Mohl , Martin Schäfer , Stefan Rittinger , Daniel Schneider
IPC分类号： C07C51/44 , C07C53/02 , C07C51/15 , C07C51/48 , C07C51/487
CPC分类号： C07C53/02 , C07C51/15 , C07C51/48 , C07C51/487
摘要： A process for preparing formic acid by reaction of carbon dioxide (1) with hydrogen (2) in a hydrogenation reactor (I) in the presence of a catalyst comprising an element of group 8, 9 or 10 of the Periodic Table, a tertiary amine comprising at least 12 carbon atoms per molecule and a polar solvent comprising one or more monoalcohols selected from among methanol, ethanol, propanols and butanols and also water, to form formic acid/amine adducts as intermediates which are subsequently thermally dissociated, with work-up of the output (3) from the hydrogenation reactor (I) in a plurality of process steps, where a tertiary amine-comprising stream (13) from the work-up is used as selective solvent for the catalyst, is proposed.
摘要翻译：在含有元素周期表第8,9,10族元素的催化剂存在下，在氢化反应器（I）中，通过二氧化碳（1）与氢气（2）的反应制备甲酸的方法，每分子含有至少12个碳原子，以及包含一种或多种选自甲醇，乙醇，丙醇和丁醇的一元醇和极性溶剂的极性溶剂，以形成甲酸/胺加合物作为随后热解离的中间体，具有后处理提出了在多个工艺步骤中，来自加氢反应器（I）的输出物（3）的来自后处理的含叔胺的物流（13）用作催化剂的选择性溶剂。

9. 发明授权

US08785693B2 Process for the preparation of primary amines by homogeneously catalyzed alcohol amination 有权
标题翻译：通过均匀催化醇胺化制备伯胺的方法
公开(公告)号：US08785693B2
公开(公告)日：2014-07-22
申请号：US13415412
申请日：2012-03-08
申请人： Thomas Schaub , Boris Buschhaus , Marion Kristina Brinks , Mathias Schelwies , Rocco Paciello , Johann-Peter Melder , Martin Merger
发明人： Thomas Schaub , Boris Buschhaus , Marion Kristina Brinks , Mathias Schelwies , Rocco Paciello , Johann-Peter Melder , Martin Merger
IPC分类号： C07C209/16 , C07C209/18 , C07D265/30 , C07D241/04 , C07D295/00 , C07D207/18 , C07D207/06 , C07D295/02 , C07D317/00
CPC分类号： C07C209/16 , C07C213/02 , C07D207/04 , C07D207/20 , C07D295/023 , C07D307/52 , C07C211/07 , C07C211/09 , C07C215/08 , C07C217/08
摘要： Process for the preparation of primary amines which have at least one functional group of the formula (—CH2—NH2) by alcohol amination of starting materials which have at least one functional group of the formula (—CH2—OH), with ammonia, with the elimination of water, where the alcohol amination is carried out under homogeneous catalysis in the presence of at least one complex catalyst which comprises at least one element selected from groups 8 and 9 of the Periodic Table of the Elements, and also at least one phosphorus donor ligand of the general formula (I).
摘要翻译：具有至少一个式（-CH 2 -NH 2）官能团的伯胺的方法，其通过具有至少一个式（-CH 2 -OH）官能团的起始原料与氨进行醇胺化反应，与消除水，其中在均相催化下，在至少一种包含至少一种选自元素周期表第8和9族的元素的复合催化剂存在下进行醇胺化，以及至少一种磷通式（I）的供体配体。

10. 发明申请

US20130137901A1 SYNTHESIS OF POLYALKYLENEPOLYAMINES HAVING A LOW COLOR INDEX BY HOMOGENEOUSLY CATALYZED ALCOHOL AMINATION IN THE PRESENCE OF HYDROGEN 有权
标题翻译：在氢存在下通过均相催化醇醇胺化合成具有低颜色指数的聚亚烷基酰胺的合成
公开(公告)号：US20130137901A1
公开(公告)日：2013-05-30
申请号：US13680625
申请日：2012-11-19
申请人： Julia STRAUTMANN , Thomas Schaub , Stephan Hueffer , Steffen Maas , Rocco Paciello
发明人： Julia STRAUTMANN , Thomas Schaub , Stephan Hueffer , Steffen Maas , Rocco Paciello
IPC分类号： C07C209/68 , C08G73/02
CPC分类号： C07C209/68 , C08G73/0213 , C07C211/11
摘要： Process for the preparation of polyalkylenepolyamines by homogeneously catalyzed alcohol amination, in which aliphatic amino alcohols are reacted with one another or aliphatic diamines or polyamines are reacted with aliphatic diols or polyols with the elimination of water in the presence of a homogeneous catalyst and in the presence of hydrogen gas. Polyalkylenepolyamines obtainable by such processes and polyalkylenepolyamines comprising hydroxy groups, secondary amines or tertiary amines. Uses of such polyalkylenepolyamines as adhesion promoters for printing inks, adhesion promoters in composite films, cohesion promoters for adhesives, crosslinkers/curing agents for resins, primers for paints, wet-adhesion promoters for emulsion paints, complexing agents and flocculating agents, penetration assistants in wood preservation, corrosion inhibitors, immobilizing agents for proteins and enzymes.
摘要翻译：通过均相催化的醇胺化制备聚亚烷基多胺的方法，其中脂肪族氨基醇彼此反应或脂族二胺或多胺与脂肪族二醇或多元醇在均相催化剂存在下与水反应，的氢气。可通过这些方法获得的聚亚烷基多胺和包含羟基，仲胺或叔胺的聚亚烷基多胺。使用这种聚亚烷基多胺作为印刷油墨的粘合促进剂，复合膜中的粘合促进剂，粘合剂的内聚力促进剂，树脂的交联剂/固化剂，油漆的底漆，乳液漆的湿粘合促进剂，络合剂和絮凝剂，渗透助剂木材保存，腐蚀抑制剂，蛋白质和酶的固定剂。

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