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1. 发明授权

US06211299B1 In situ solvent free method for making anhydride based graft copolymers 有权
标题翻译：用于制备基于酸酐的接枝共聚物的原位无溶剂方法
公开(公告)号：US06211299B1
公开(公告)日：2001-04-03
申请号：US09368512
申请日：1999-08-05
申请人： Thomas H. Moss, III , Klein A. Rodrigues
发明人： Thomas H. Moss, III , Klein A. Rodrigues
IPC分类号： C08F26704
CPC分类号： C11D3/3788 , C08F257/02 , C08F267/02 , C08F267/04 , C08F291/00 , C08L71/02 , C08L2666/04 , C08L2666/24
摘要： In situ solvent free methods for making anhydride based graft copolymers which involve mixing an ethylenically unsaturated monomer, an anhydride monomer, either a monofunctional polyglycol having a hydroxyl or amine terminal group or a polyfunctional polyglycol having a weight average molecular weight of greater than 5,000 and at least one terminal hydroxyl group, and a free radical initiator to form a mixture. The mixture is heated to form a copolymer having repeat units derived from the ethylenically unsaturated monomer and anhydride monomer, and a copolymer grafted polyglycol comprising a main polyglycol backbone having copolymer side chains which are heated to form an anhydride based graft copolymer. The anhydride based graft copolymers are especially useful as soil release agents in detergent formulations.
摘要翻译：用于制备基于酸酐的接枝共聚物的原位无溶剂方法，其包括将烯键式不饱和单体，酸酐单体，具有羟基或胺末端基团的单官能聚乙二醇或重均分子量大于5,000的多官能聚二醇混合，至少一个末端羟基和自由基引发剂形成混合物。将混合物加热以形成具有衍生自烯键式不饱和单体和酸酐单体的重复单元的共聚物，以及包含主要聚乙二醇主链的共聚物接枝聚乙二醇，其具有加热形成基于酸酐的接枝共聚物的共聚物侧链。基于酸酐的接枝共聚物特别用作洗涤剂配方中的去污剂。

2. 发明授权

US5629376A Polyacrylic acid compositions for textile processing 失效
标题翻译：用于纺织加工的聚丙烯酸组合物
公开(公告)号：US5629376A
公开(公告)日：1997-05-13
申请号：US63211
申请日：1993-05-17
申请人： R. Richard Sargent , Michael S. Williams , Thomas H. Moss, III , Jeffrey R. Alender
发明人： R. Richard Sargent , Michael S. Williams , Thomas H. Moss, III , Jeffrey R. Alender
IPC分类号： B01F17/52 , B01F17/00 , C07F9/09 , C08F2/00 , C08F2/44 , C08F12/24 , C08F16/34 , C08F16/36 , C08F16/38 , C08F20/00 , C08F20/04 , C08F20/06 , C08F20/10 , C08F20/52 , C08F28/00 , C08F28/02 , C08F30/02 , C08F220/04 , C08F220/06 , C08F220/10 , C08L33/00 , C08L33/04 , C09K3/00 , C09K3/16 , C09K15/10 , C09K21/06 , C09K21/14 , C10M107/46 , C10N40/00 , C11D1/22 , C11D3/37 , C14C3/22 , D06L1/12 , D06M13/02 , D06M13/244 , D06M13/248 , D06M13/256 , D06M13/282 , D06M13/292 , D06M15/263 , D06P1/52 , C08K5/42 , C08F120/54 , C08F122/18 , C08F128/02 , C08F130/02
CPC分类号： B01F17/0057 , C08F2/44 , C08F20/00 , C09K15/10 , C09K21/06 , C11D3/3757 , C11D3/378 , C14C3/22 , D06M15/263 , D06M7/00 , D06P1/5257 , D06M2200/40
摘要： Novel polyacrylic acid resins are prepared by polymerizing a monomer selected from the group consisting of H.sub.2 C.dbd.CHCO.sub.2 X, H.sub.2 C.dbd.CR.sup.1 CO.sub.2 X, HR.sup.2 C.dbd.CHCO.sub.2 X, HR.sup.2 C.dbd.CR.sup.1 CO.sub.2 X, HR.sup.2 C.dbd.CHCOX, H.sub.2 C.dbd.CHCOX, H.sub.2 C.dbd.CR.sup.1 COX, HR.sup.2 C.dbd.CR.sup.1 COX, H.sub.2 C.dbd.CHCSO.sub.v X, HR.sup.2 C.dbd.CHCSO.sub.v X, HR.sup.2 C.dbd.CR.sup.1 CSO.sub.v X, H.sub.2 C.dbd.CR.sup.1 CSO.sub.v X, H.sub.2 C.dbd.CHCON(R.sup.3).sub.2, HR.sup.2 C.dbd.CHCON(R.sup.3).sub.2, H.sub.2 C.dbd.CR.sup.1 CON(R.sup.3).sub.2, OR HR.sup.2 C.dbd.CR.sup.1 CON(R.sup.3).sub.2, or a combination thereof, in the presence of at least 10% by weight of reaction components of an aromatic sulfonic acid or its salt, wherein:R.sup.1 and R.sup.2 are independently a substituted or unsubstituted alkyl, alkenyl, aromatic, aralkyl or alkaryl moiety of C.sub.1 to C.sub.20 ;R.sup.3 is independently hydrogen or a substituted or unsubstituted alkyl, alkenyl, aromatic, aralkyl or alkaryl moiety of C.sub.1 to C.sub.20 ; andX is hydrogen, substituted or unsubstituted alkyl, alkenyl, aromatic, aralkyl, or alkaryl moiety of C.sub.1 to C.sub.20 ; --CH.sub.2 CH.sub.2 (CF.sub.2 CF.sub.2).sub.n CF.sub.2 CF.sub.3, wherein n is 1-7; polyoxyalkylene; --C(R.sup.2).sub.2 R.sup.3 Y, wherein R.sup.3 is alkylene or polyoxyalkylene (or a combination thereof), and Y is --OSO.sub.3 H, --SO.sub.3 H, --CO.sub.2 H, --PO.sub.3 H, --OPO.sub.3 H, or a salt thereof; CF.sub.3 (CF.sub.2).sub.q -, wherein q is 1-11, hexafluorobutyl, tetrafluoropropyl, sodium, potassium, lithium, ammonium, or quaternary amine; and v is 0, 1, or 2.
摘要翻译：通过聚合选自H 2 C = CHCO 2 X，H 2 C = CR 1 CO 2 X，HR 2 C = CHCO 2 X，HR 2 C = CR 1 CO 2 X，HR 2 C = CHCOX，H 2 C = CHCOX，H 2 C = CR 1 COX，HR 2 C = CR 1 COX，H 2 C = CHCSOvX，HR2C = CHCSOvX，HR2C = CR1CSOvX，H2C = CR1CSOvX，H2C = CHCON（R3）2，HR2C = CHCON（R3）2，H2C = CR1CON（R3）2，或HR2C = CR1CON（R3）在至少10重量％的芳族磺酸或其盐的反应组分的存在下，其中：R 1和R 2独立地是C 1 -C 20的取代或未取代的烷基，烯基，芳基，芳烷基或烷芳基部分; R 3独立地为氢或C1至C20的取代或未取代的烷基，烯基，芳族，芳烷基或烷芳基部分; 且X为氢，C1至C20的取代或未取代的烷基，烯基，芳族，芳烷基或烷芳基部分; -CH 2 CH 2（CF 2 CF 2）n CF 2 CF 3，其中n为1-7; 聚氧化烯 -C（R 2）2 R 3 Y，其中R 3是亚烷基或聚氧化烯（或其组合），Y是-OSO 3 H，-SO 3 H，-CO 2 H，-PO 3 H，-OPO 3 H或其盐; CF 3（CF 2）q - ，其中q为1-11，六氟丁基，四氟丙基，钠，钾，锂，铵或季胺; v为0,1或2。

3. 发明授权

US5223340A Stain resistant polyamide fibers 失效
标题翻译：抗污染聚酰胺纤维
公开(公告)号：US5223340A
公开(公告)日：1993-06-29
申请号：US730696
申请日：1991-07-16
申请人： Thomas H. Moss, III , Ralph R. Sargent , Michael S. Williams
发明人： Thomas H. Moss, III , Ralph R. Sargent , Michael S. Williams
IPC分类号： D06M15/263 , D06M15/41
CPC分类号： D06M15/412 , D06M15/263 , Y10T428/2969 , Y10T442/2279 , Y10T442/2287 , Y10T442/2762 , Y10T442/2893 , Y10T442/696
摘要： A stain resistant composition for fibers having polyamide linkages prepared by polymerizing an .alpha.-substituted acrylic acid or ester in the presence of a sulfonated aromatic formaldehyde condensation polymer, or by polymerization of a sulfonated hydroxyaromatic ester of an .alpha.-substituted acrylic acid or acrylic acid, and methods for making and applying the composition.
摘要翻译：通过在磺化芳族甲醛缩聚物的存在下聚合α取代的丙烯酸或酯或通过α-取代的丙烯酸或丙烯酸的磺化羟基芳族化合物的聚合制备聚酰胺键的纤维的耐污染组合物，以及制备和施用组合物的方法。

4. 发明授权

US5015259A Stain resistant polymeric composition 失效
标题翻译：耐污染聚合物组合物
公开(公告)号：US5015259A
公开(公告)日：1991-05-14
申请号：US521752
申请日：1990-05-10
申请人： Thomas H. Moss, III , Ralph R. Sargent , Michael S. Williams
发明人： Thomas H. Moss, III , Ralph R. Sargent , Michael S. Williams
IPC分类号： D06M15/263 , D06M15/41
CPC分类号： D06M15/412 , D06M15/263
摘要： A stain resistant composition for fibers having polyamide linkages prepared by polymerizing an .alpha.-substituted acrylic acid or ester in the presence of a sulfonated aromatic formaldehyde condensation polymer, and methods for making and applying the composition.
摘要翻译：在具有磺化芳族甲醛缩聚物存在下通过聚合α-取代的丙烯酸或酯制备聚酰胺键的纤维的耐污染组合物，以及制备和施用该组合物的方法。

5. 发明授权

US4940757A Stain resistant polymeric composition 失效
标题翻译：耐污染聚合物组合物
公开(公告)号：US4940757A
公开(公告)日：1990-07-10
申请号：US341774
申请日：1989-04-20
申请人： Thomas H. Moss, III , Ralph R. Sargent , Michael S. Williams
发明人： Thomas H. Moss, III , Ralph R. Sargent , Michael S. Williams
IPC分类号： D06M15/263 , D06M15/41
CPC分类号： D06M15/412 , D06M15/263
摘要： A stain resistant composition for fibers having polyamide linkages prepared by polymerizing an .alpha.-substituted acrylic acid or ester in the presence of a sulfonated aromatic formaldehyde condensation polymer, and methods for making and applying the composition.
摘要翻译：在具有磺化芳族甲醛缩聚物存在下通过聚合α-取代的丙烯酸或酯制备聚酰胺键的纤维的耐污染组合物，以及制备和施用该组合物的方法。

6. 发明授权

US5061763A Stain resistant treatment for polyamide fibers 失效
标题翻译：聚酰胺纤维的耐污染处理
公开(公告)号：US5061763A
公开(公告)日：1991-10-29
申请号：US457348
申请日：1989-12-27
申请人： Thomas H. Moss, III , Ralph R. Sargent , Michael S. Williams
发明人： Thomas H. Moss, III , Ralph R. Sargent , Michael S. Williams
IPC分类号： D06N3/00 , C08F20060101 , C08F220/00 , C08F290/14 , C08F299/00 , C08G8/00 , C08G8/18 , C08G8/38 , C08L33/02 , C08L33/04 , C08L33/14 , C14C11/00 , D06M13/02 , D06M13/248 , D06M13/256 , D06M15/263 , D06M15/41 , D06M15/564 , D06M23/04 , D06M101/00 , D06M101/02 , D06M101/10 , D06M101/16 , D06M101/30 , D06M101/34 , D06M101/36
CPC分类号： C08F290/14 , C08F299/00 , D06M15/263 , D06M15/412 , D06M15/564 , D06M2101/34
摘要： A stain resistant composition for fibers having polyamide linkages prepared by polymerizing an .alpha.-substituted acrylic acid or ester in the presence of a sulfonated aromatic formaldehyde condensation plymer, or by polymerization of a sulfonated hydroxyaromatic ester of an .alpha.-substituted acrylic acid or acrylic acid, and methods for making and applying the composition.
摘要翻译：通过在磺化芳族甲醛缩聚物的存在下聚合α取代的丙烯酸或酯或通过α-取代的丙烯酸或丙烯酸的磺化羟基芳族化合物的聚合制备聚酰胺键的纤维的耐污染组合物，以及制备和施用组合物的方法。

7. 发明授权

US5464911A Superior stain resistant compositions 失效
标题翻译：优异的抗污染组合物
公开(公告)号：US5464911A
公开(公告)日：1995-11-07
申请号：US231020
申请日：1994-04-21
申请人： Michael S. Williams , Thomas H. Moss, III
发明人： Michael S. Williams , Thomas H. Moss, III
IPC分类号： D06N3/00 , C08F20060101 , C08F220/00 , C08F290/00 , C08F290/14 , C08F299/00 , C08F299/02 , C08G8/00 , C08G8/18 , C08G8/28 , C08G8/38 , C08G10/00 , C08G10/02 , C08G16/00 , C08G16/02 , C08G18/54 , C08L33/02 , C08L33/04 , C08L33/14 , C14C11/00 , D06M13/02 , D06M13/184 , D06M13/203 , D06M13/248 , D06M13/256 , D06M15/263 , D06M15/41 , D06M15/564 , D06M23/04 , D06M101/00 , D06M101/02 , D06M101/10 , D06M101/16 , D06M101/30 , D06M101/34 , D06M101/36 , C08L61/14
CPC分类号： D06M15/263 , C08F290/14 , C08F299/00 , D06M15/412 , D06M15/564 , D06M2101/34 , Y10T428/31942 , Y10T442/2279 , Y10T442/2902
摘要： Novel polymeric compositions are provided for polyamide fibers or fibers having terminal amino groups that impart stain resistance and are resistant to discoloration.
摘要翻译：为聚酰胺纤维或具有赋予耐污染性并具有抗变色性能的末端氨基的纤维提供了新颖的聚合物组合物。

8. 发明授权

US5310828A Superior stain resistant compositions 失效
标题翻译：优异的抗污染组合物
公开(公告)号：US5310828A
公开(公告)日：1994-05-10
申请号：US783580
申请日：1991-10-28
申请人： Michael S. Williams , Thomas H. Moss, III
发明人： Michael S. Williams , Thomas H. Moss, III
IPC分类号： D06N3/00 , C08F20060101 , C08F220/00 , C08F290/00 , C08F290/14 , C08F299/00 , C08F299/02 , C08G8/00 , C08G8/18 , C08G8/28 , C08G8/38 , C08G10/00 , C08G10/02 , C08G16/00 , C08G16/02 , C08G18/54 , C08L33/02 , C08L33/04 , C08L33/14 , C14C11/00 , D06M13/02 , D06M13/184 , D06M13/203 , D06M13/248 , D06M13/256 , D06M15/263 , D06M15/41 , D06M15/564 , D06M23/04 , D06M101/00 , D06M101/02 , D06M101/10 , D06M101/16 , D06M101/30 , D06M101/34 , D06M101/36 , C08G8/30 , C08G63/48
CPC分类号： D06M15/263 , C08F290/14 , C08F299/00 , D06M15/412 , D06M15/564 , D06M2101/34 , Y10T428/31942 , Y10T442/2279 , Y10T442/2902
摘要： Novel polymeric compositions are provided for polyamide fibers or fibers having terminal amino groups that impart stain resistance and are resistant to discoloration.
摘要翻译：为聚酰胺纤维或具有赋予耐污染性并具有抗变色性能的末端氨基的纤维提供了新颖的聚合物组合物。

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