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1. 发明申请

US20110186515A1 PROCESS FOR TREATMENT OF WATER/OIL EMULSIONS 失效
标题翻译：用于处理水/油乳液的方法
公开(公告)号：US20110186515A1
公开(公告)日：2011-08-04
申请号：US12980179
申请日：2010-12-28
申请人： Regina Celia Lourenco GUIMARÂES , Bianca Machado da Silva FERREIRA , Maria de Fatima Pereira DOS SANTOS , Ricardo Andre GUARNIERI , Montserrat Fortuny HEREDIA , Cláudio DARIVA , Alexandre Ferreira SANTOS , Rita de Cássia Bomfim LEMOS , Lisiane dos Santos FREITAS
发明人： Regina Celia Lourenco GUIMARÂES , Bianca Machado da Silva FERREIRA , Maria de Fatima Pereira DOS SANTOS , Ricardo Andre GUARNIERI , Montserrat Fortuny HEREDIA , Cláudio DARIVA , Alexandre Ferreira SANTOS , Rita de Cássia Bomfim LEMOS , Lisiane dos Santos FREITAS
IPC分类号： B01D11/04 , B01D17/04
CPC分类号： B01D11/04 , B01D17/04
摘要： A process for the treatment of water/oil (W/O) emulsions is described which includes the addition of an ionic liquid, under heating, to a water/oil emulsion containing between 0.5% and 85% of water per volume as a dispersion phase, until the concentration of the ionic liquid in the emulsion remains within the range of 0.01 μL/g to 100 μL/g. The ionic liquid used is a salt of a general C+ A− formula in a liquid state at temperatures below 150° C., where A− is an anion and C+ is a cation, which has at least a hydrophobic alkyl chain connected to a cation group. The heating method includes conventional heating and heating via microwaves. In the heating via microwaves, the salts of the general C+ A− formula present synergic behavior in separation efficiency in relation to conventional heating.
摘要翻译：描述了一种用于处理水/油（W / O）乳液的方法，其包括在加热下将离子液体加入含有0.5至85％水/体积的水/油乳液作为分散相直到乳液中离子液体的浓度保持在0.01μL/ g至100μL/ g的范围内。使用的离子液体是在低于150℃的温度下处于液态的一般C + 4-式的盐，其中A-是阴离子，C +是阳离子，其至少具有连接到阳离子的疏水性烷基链组。加热方法包括通过微波的常规加热和加热。在通过微波的加热中，一般C + A-配方的盐在与传统加热相关的分离效率中具有协同作用。

2. 发明授权

US07705058B2 Method for the microwave treatment of water-in-oil emulsions 有权
标题翻译：微波处理油包水乳液的方法
公开(公告)号：US07705058B2
公开(公告)日：2010-04-27
申请号：US12007082
申请日：2008-01-07
申请人： Raquel Campos Coutinho , Montserrat Fortuny Heredia , Márcio Nele De Souza , Alexandre Ferreira Santos
发明人： Raquel Campos Coutinho , Montserrat Fortuny Heredia , Márcio Nele De Souza , Alexandre Ferreira Santos
IPC分类号： B01D17/05
CPC分类号： C10G32/02 , B01D17/04 , B01D17/042 , B01D17/044 , C10G33/02
摘要： Method for the microwave emulsion treatment of water-in-oil (W/O) emulsions, including a) determining, for an W/O emulsion the optimum conditions of the variables: water content, salt content, pH value of the aqueous phase, initial temperature, microwave application power, final temperature and drop size distribution to be adjusted in the industrial plant, as a function of the features of the tested crude oil such as viscosity, density, asphaltene content, total acidity, such conditions being those required for obtaining at least 90% separation efficiency of the emulsion in the presence of microwave radiation: b) utilizing such information for the initial adjustment of application conditions of the method to phase separation units in refineries and production units; c) perform on line tests of the variables of step a) of the process response in the streams effluent from separation units, being the response the water content and salt content tests, so as to feedback the information to the best adjustment of the process conditions for microwave application; and d) utilizing the on line or laboratory tests of the effect of the method as a tool for monitoring the efficiency of the breaking of the W/O emulsion.
摘要翻译：油包水（W / O）乳液的微波乳液处理方法，包括a）确定W / O乳液的最佳条件：水含量，盐含量，水相pH值，初始温度，微波施加功率，最终温度和液滴尺寸分布在工业厂房中调整，作为测试原油的特征的函数，如粘度，密度，沥青质含量，总酸度，这些条件是所需的在微波辐射的存在下获得至少90％的乳液分离效率：b）利用这些信息来初步调整炼油厂和生产单元中相分离装置的方法的应用条件; c）对来自分离单元的流出物中的过程响应的步骤a）的变量进行在线测试，作为对含水量和盐含量测试的响应，以便反馈信息以最佳地调节过程条件用于微波应用; 以及d）利用该方法的在线或实验室测试作为监测W / O乳液破裂效率的工具。

3. 发明授权

US08747674B2 Process for treatment of water/oil emulsions 失效
标题翻译：水/油乳液的处理方法
公开(公告)号：US08747674B2
公开(公告)日：2014-06-10
申请号：US12980179
申请日：2010-12-28
申请人： Regina Celia Lourenco Guimarães , Bianca Machado da Silva Ferreira , Maria de Fatima Pereira dos Santos , Ricardo Andre Guarnieri , Montserrat Fortuny Heredia , Cláudio Dariva , Alexandre Ferreira Santos , Rita de Cássia Bomfim Lemos , Lisiane dos Santos Freitas
发明人： Regina Celia Lourenco Guimarães , Bianca Machado da Silva Ferreira , Maria de Fatima Pereira dos Santos , Ricardo Andre Guarnieri , Montserrat Fortuny Heredia , Cláudio Dariva , Alexandre Ferreira Santos , Rita de Cássia Bomfim Lemos , Lisiane dos Santos Freitas
IPC分类号： B01D11/04 , B01D17/04 , B01D17/05
CPC分类号： B01D11/04 , B01D17/04
摘要： A process for the treatment of water/oil (W/O) emulsions is described which includes the addition of an ionic liquid, under heating, to a water/oil emulsion containing between 0.5% and 85% of water per volume as a dispersion phase, until the concentration of the ionic liquid in the emulsion remains within the range of 0.01 μL/g to 100 μL/g. The ionic liquid used is a salt of a general C+ A− formula in a liquid state at temperatures below 150° C., where A− is an anion and C+ is a cation, which has at least a hydrophobic alkyl chain connected to a cation group. The heating method includes conventional heating and heating via microwaves. In the heating via microwaves, the salts of the general C+ A− formula present synergic behavior in separation efficiency in relation to conventional heating.
摘要翻译：描述了一种用于处理水/油（W / O）乳液的方法，其包括在加热下将离子液体加入含有0.5至85％水/体积的水/油乳液作为分散相直到乳液中离子液体的浓度保持在0.01μL/ g至100μL/ g的范围内。使用的离子液体是在低于150℃的温度下处于液态的一般C + 4-式的盐，其中A-是阴离子，C +是阳离子，其至少具有连接到阳离子的疏水性烷基链组。加热方法包括通过微波的常规加热和加热。在通过微波的加热中，一般C + A-配方的盐在与传统加热相关的分离效率中具有协同作用。

4. 发明申请

US20080221226A1 Method for the microwave treatment of water-in-oil emulsions 有权
标题翻译：微波处理油包水乳液的方法
公开(公告)号：US20080221226A1
公开(公告)日：2008-09-11
申请号：US12007082
申请日：2008-01-07
申请人： Raquel Campos Coutinho , Montserrat Fortuny Heredia , Marcio Nele de Souza , Alexandre Ferreira Santos
发明人： Raquel Campos Coutinho , Montserrat Fortuny Heredia , Marcio Nele de Souza , Alexandre Ferreira Santos
IPC分类号： B01D17/05
CPC分类号： C10G32/02 , B01D17/04 , B01D17/042 , B01D17/044 , C10G33/02
摘要： Method for the microwave emulsion treatment of water-in-oil (W/O) emulsions, including a) determining, for an W/O emulsion the optimum conditions of the variables: water content, salt content, pH value of the aqueous phase, initial temperature, microwave application power, final temperature and drop size distribution to be adjusted in the industrial plant, as a function of the features of the tested crude oil such as viscosity, density, asphaltene content, total acidity, such conditions being those required for obtaining at least 90% separation efficiency of the emulsion in the presence of microwave radiation: b) utilizing such information for the initial adjustment of application conditions of the method to phase separation units in refineries and production units; c) perform on line tests of the variables of step a) of the process response in the streams effluent from separation units, being the response the water content and salt content tests, so as to feedback the information to the best adjustment of the process conditions for microwave application; and d) utilizing the on line or laboratory tests of the effect of the method as a tool for monitoring the efficiency of the breaking of the W/O emulsion.
摘要翻译：油包水（W / O）乳液的微波乳液处理方法，包括a）确定W / O乳液的最佳条件：水含量，盐含量，水相pH值，初始温度，微波施加功率，最终温度和液滴尺寸分布在工业厂房中调整，作为测试原油的特征的函数，如粘度，密度，沥青质含量，总酸度，这些条件是所需的在微波辐射的存在下获得至少90％的乳液分离效率：b）利用这些信息来初步调整炼油厂和生产单元中相分离装置的方法的应用条件; c）对来自分离单元的流出物中的过程响应的步骤a）的变量进行在线测试，作为对含水量和盐含量测试的响应，以便反馈信息以最佳地调节过程条件用于微波应用; 以及d）利用该方法的在线或实验室测试作为监测W / O乳液破裂效率的工具。

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