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1. 发明授权

US09580333B2 Process for preparing chromium(III) oxide 有权
标题翻译：制备氧化铬（III）的方法
公开(公告)号：US09580333B2
公开(公告)日：2017-02-28
申请号：US13991516
申请日：2011-12-07
申请人： Holger Friedrich , Matthias Boll , Rainer Ortmann
发明人： Holger Friedrich , Matthias Boll , Rainer Ortmann
IPC分类号： C01G37/033 , C01G37/00 , C09C1/34
CPC分类号： C01G37/033 , C01G37/00 , C01P2006/80 , C09C1/346
摘要： Process for preparing chromium(III) oxide, which comprises the steps: a) reaction of sodium monochromate with gaseous ammonia, in particular at a temperature of from 200 to 800° C., b) hydrolysis of the reaction product obtained in step a) with the pH of the water for the hydrolysis being reduced before the hydrolysis or that of the alkaline mother liquor being reduced during or after the hydrolysis, to a value of from 4 to 11, preferably from 5 to 10, by means of an acid, c) isolation of the hydrolysis product which has precipitated in step b), preferably at a pH of from 4 to 11, in particular from 5 to 10, and optionally washing and optionally drying and d) calcination of the hydrolysis product obtained in step c) at a temperature of from 700 to 1400° C., in particular from 800 to 1300° C.
摘要翻译：制备氧化铬（III）的方法，其包括以下步骤：a）将单色钠与气态氨反应，特别是在200至800℃的温度下，b）水解步骤a）中获得的反应产物，在水解之前水解的水的pH降低，或在水解期间或之后碱性母液的pH降低至4至11，优选5至10的值，借助于酸， c）分离在步骤b）中沉淀的水解产物，优选在4至11，特别是5至10的pH下，并任选地洗涤和任选地干燥和d）煅烧步骤c中获得的水解产物），温度为700〜1400℃，特别是800〜1300℃。

2. 发明授权

US07824580B2 Silver-containing aqueous formulation and its use to produce electrically conductive or reflective coatings 有权
标题翻译：含银水性配方及其用于生产导电或反射涂层的用途
公开(公告)号：US07824580B2
公开(公告)日：2010-11-02
申请号：US11923887
申请日：2007-10-25
申请人： Matthias Boll , Stefanie Eiden , Johan Kijlstra
发明人： Matthias Boll , Stefanie Eiden , Johan Kijlstra
IPC分类号： H01B1/22 , B22F7/00 , C09D5/00
CPC分类号： H01B1/22 , B05D5/067 , C09D5/24 , C09D11/30 , H05K1/097 , H05K3/125 , H05K2203/013 , Y10T428/298
摘要： A silver-containing, disperse, water-containing formulation and its use to produce electrically conductive and/or optically reflective coatings is described. The formulation contains at least a) 0.5 to 30 parts by wt. of silver metal particles with an effective diameter of at most 150 nm, preferably at most 100 nm, particularly preferably 40 to 80 nm, with a bimodal size distribution, b) 50 to 99.5 parts by wt. of water and optionally up to 30 parts by wt. of solvent, c) 0.01 to 10 parts by wt. of at least one, in particular polymeric, dispersant, d) 0 to 5 parts by wt. of film-producer, e) 0 to 5 parts by wt. of additives, f) 0 to 5 parts by wt. of conductive polymers, and has a viscosity of at most 150 mPa.s.
摘要翻译：描述了含银，分散，含水的配方及其制备导电和/或光反射涂层的用途。制剂含有至少a）0.5-30重量份。银双金属颗粒，有效直径至多为150nm，优选为至多100nm，特别优选为40至80nm，具有双峰尺寸分布，b）50至99.5重量份。的水和任选地至多30重量份。的溶剂，c）0.01至10重量份的至少一种，特别是聚合物分散剂，d）0至5重量份。的电影制作人，e）0至5重量份。的添加剂，f）0-5重量份。的导电聚合物，并且具有至多150mPa.s的粘度。

3. 发明申请

US20100252784A1 PROCESS FOR PREPARING SILVER-CONTAINING AQUEOUS FORMULATION USEFUL FOR ELECTRICALLY CONDUCTIVE OR REFLECTIVE COATINGS 有权
标题翻译：制备用于导电或反射涂层的含银水性配方的方法
公开(公告)号：US20100252784A1
公开(公告)日：2010-10-07
申请号：US12814050
申请日：2010-06-11
申请人： Matthias BOLL , Stefanie Eiden , Johan Kijlstra
发明人： Matthias BOLL , Stefanie Eiden , Johan Kijlstra
IPC分类号： H01B1/22
CPC分类号： H01B1/22 , B05D5/067 , C09D5/24 , C09D11/30 , H05K1/097 , H05K3/125 , H05K2203/013 , Y10T428/298
摘要： Process for preparing A silver-containing, disperse, water-containing formulation useful for producing electrically conductive and/or optically reflective coatings, which comprises (i) reacting a silver salt solution with a solution containing hydroxide ions, wherein at least one of said solutions comprises a polymeric dispersant, to produce an Ag2O sol, (ii) reacting the Ag2O sol obtained from step i) with a reduction agent, and (iii) purifying the solution obtained from step ii).
摘要翻译：制备用于制备导电和/或光反射涂层的含银分散的含水制剂的方法，其包括（i）使银盐溶液与含有氢氧根离子的溶液反应，其中至少一种所述溶液包括聚合物分散剂，以产生Ag 2 O溶胶，（ii）使由步骤i）获得的Ag 2 O溶胶与还原剂反应，和（iii）纯化由步骤ii）获得的溶液。

4. 发明申请

US20060237123A1 Method of producing a sheet 审中-公开
标题翻译：生产片材的方法
公开(公告)号：US20060237123A1
公开(公告)日：2006-10-26
申请号：US11397879
申请日：2006-04-03
申请人： Martin Dobler , Roland Kunzel , Dirk Pophusen , Winfried Kohl , Matthias Boll
发明人： Martin Dobler , Roland Kunzel , Dirk Pophusen , Winfried Kohl , Matthias Boll
IPC分类号： B32B37/00 , B44C1/17 , B29C47/00
CPC分类号： B29C70/82 , B29C45/14811 , B29C65/64 , B29C66/21 , B29C66/69 , B29C66/71 , B29C66/742 , B29K2033/12 , B29K2069/00 , B29K2705/00 , B29K2995/0026 , B29K2995/0029 , B29L2031/30 , B29L2031/3055 , B29L2031/747 , B29L2031/779 , F21Y2105/00 , H05B2203/017 , B29K2075/00 , B29K2067/003 , B29K2033/08 , B29K2025/08 , B29K2025/06 , B29K2023/38 , B29K2023/12 , B29K2023/00
摘要： A method of producing a plastic sheet equipped with electrical conductors is disclosed. The method that enables automatic production includes (a) fixing in a frame an electrically conducting wire in a sinusoidal, square wave pattern and in a single plane, (b) bringing into contact the single plane and a surface of a plastic sheet under conditions calculated to bond the plastic to said conductor, and (c) removing the frame.
摘要翻译：公开了一种制造配备有电导体的塑料片的方法。实现自动生产的方法包括（a）以正弦，方波图案和单个平面在框架中固定导电线，（b）在计算的条件下使单个平面和塑料片的表面接触将塑料粘合到所述导体上，和（c）移除框架。

5. 发明授权

US09663383B2 Process for preparing chromium(III) oxide 有权
公开(公告)号：US09663383B2
公开(公告)日：2017-05-30
申请号：US13635963
申请日：2011-03-23
申请人： Rainer Ortmann , Matthias Stenger , Matthias Boll , Holger Friedrich
发明人： Rainer Ortmann , Matthias Stenger , Matthias Boll , Holger Friedrich
IPC分类号： C01G37/00 , C01G37/033 , C09C1/34
CPC分类号： C01G37/033 , C01G37/00 , C01P2006/80 , C09C1/346
摘要： The present invention relates to a process for preparing chromium(III) oxide by reaction of alkali metal chromate with gaseous ammonia, subsequent hydrolysis, isolation of the hydrolysis product and calcination.

6. 发明申请

US20130216471A1 PROCESS FOR PREPARING CHROMIUM(III) OXIDE 有权
标题翻译：制备氧化铬（III）的方法
公开(公告)号：US20130216471A1
公开(公告)日：2013-08-22
申请号：US13635963
申请日：2011-03-23
申请人： Rainer Ortmann , Matthias Stenger , Matthias Boll , Holger Friedrich
发明人： Rainer Ortmann , Matthias Stenger , Matthias Boll , Holger Friedrich
IPC分类号： C01G37/033
CPC分类号： C01G37/033 , C01G37/00 , C01P2006/80 , C09C1/346
摘要： The present invention relates to a process for preparing chromium(III) oxide by reaction of alkali metal chromate with gaseous ammonia, subsequent hydrolysis, isolation of the hydrolysis product and calcination.
摘要翻译：本发明涉及通过碱金属铬酸盐与气态氨反应制备氧化铬（III）的方法，随后的水解，水解产物的分离和煅烧。

7. 发明申请

US20130129604A1 METHOD FOR PRODUCING AMMONIUM DICHROMATE 审中-公开
标题翻译：生产二氧化铬的方法
公开(公告)号：US20130129604A1
公开(公告)日：2013-05-23
申请号：US13518107
申请日：2010-12-08
申请人： Holger Friedrich , Rainer Ortmann , Matthias Stenger , Matthias Boll , Daniel Van Rooyen , Naveen Kalideen
发明人： Holger Friedrich , Rainer Ortmann , Matthias Stenger , Matthias Boll , Daniel Van Rooyen , Naveen Kalideen
IPC分类号： C01G37/14
CPC分类号： C01G37/14
摘要： Process for preparing ammonium dichromate, comprising the steps of c) thermally decomposing an alkali metal ammonium chromate double salt, especially a sodium ammonium chromate double salt or hydrates thereof, at a temperature up to 200° C., especially of 75 to 190° C., to form ammonium dichromate and d) removing the ammonium dichromate from the decomposition product obtained after step c), by crystallization, characterized in that the alkali metal ammonium chromate double salt corresponds to the formula Mx(NH4)yCrO4 or hydrates thereof, in which M is Na or K, particular preference being given to Na, x is from 0.1 to 0.9, preferably from 0.4 to 0.7, y is from 1.1 to 1.9, preferably from 1.3 to 1.6, and the sum of x and y is 2.
摘要翻译：制备重铬酸铵的方法，包括以下步骤：c）在高达200℃，特别是75至190℃的温度下热分解碱金属铬酸铬复合盐，特别是铬酸铵钠盐或其水合物以形成重铬酸铵，和d）通过结晶从步骤c）中获得的分解产物中除去重铬酸铵，其特征在于碱金属铬酸铬复盐对应于式Mx（NH4）yCrO4或其水合物，其在其中M为Na或K，特别优选为Na，x为0.1至0.9，优选为0.4至0.7，y为1.1至1.9，优选为1.3至1.6，x和y之和为2。

8. 发明授权

US08252924B2 Process for preparing benzomorpholine derivatives by hydrogenating o-nitrophenoxy carbonyl compounds 失效
标题翻译：通过氢化邻硝基苯氧羰基化合物制备苯并吗啉衍生物的方法
公开(公告)号：US08252924B2
公开(公告)日：2012-08-28
申请号：US12641426
申请日：2009-12-18
申请人： Matthias Boll , Burkhard Koch
发明人： Matthias Boll , Burkhard Koch
IPC分类号： C07D265/30 , C07D295/00
CPC分类号： C07D265/36
摘要： A process for preparing benzomorpholine derivatives is described, in which an o-nitrophenoxy carbonyl compound is hydrogenated in the presence of extraneous metal-doped sponge metal catalysts based on nickel or cobalt with ring formation.
摘要翻译：描述了制备苯并吗啉衍生物的方法，其中邻硝基苯氧基羰基化合物在具有环形成的基于镍或钴的外来金属掺杂海绵金属催化剂存在下氢化。

9. 发明授权

US07976736B2 Process for preparing silver-containing aqueous formulation useful for electrically conductive or reflective coatings 有权
标题翻译：制备用于导电或反射涂层的含银水性配方的方法
公开(公告)号：US07976736B2
公开(公告)日：2011-07-12
申请号：US12814050
申请日：2010-06-11
申请人： Matthias Boll , Stefanie Eiden , Johan Kijlstra
发明人： Matthias Boll , Stefanie Eiden , Johan Kijlstra
IPC分类号： H01B1/02 , C01G3/00
CPC分类号： H01B1/22 , B05D5/067 , C09D5/24 , C09D11/30 , H05K1/097 , H05K3/125 , H05K2203/013 , Y10T428/298
摘要： Process for preparing A silver-containing, disperse, water-containing formulation useful for producing electrically conductive and/or optically reflective coatings, which comprises (i) reacting a silver salt solution with a solution containing hydroxide ions, wherein at least one of said solutions comprises a polymeric dispersant, to produce an Ag2O sol, (ii) reacting the Ag2O sol obtained from step i) with a reduction agent, and (iii) purifying the solution obtained from step ii).
摘要翻译：制备用于制备导电和/或光反射涂层的含银分散的含水制剂的方法，其包括（i）使银盐溶液与含有氢氧根离子的溶液反应，其中至少一种所述溶液包括聚合物分散剂，以产生Ag 2 O溶胶，（ii）使由步骤i）获得的Ag 2 O溶胶与还原剂反应，和（iii）纯化由步骤ii）获得的溶液。

10. 发明申请

US20090226684A1 Printable Composition Containing Carbon Nanotubes, Processes for Their Preparation and Electrically Conductive Coating Prepared Therefrom 审中-公开
标题翻译：含有碳纳米管的可印刷组合物，其制备方法和导电涂层
公开(公告)号：US20090226684A1
公开(公告)日：2009-09-10
申请号：US12370643
申请日：2009-02-13
申请人： Stefan Bahnmuller , Stefanie Eiden , Olaf Behrend , Diana Dimova Landen , Matthias Boll
发明人： Stefan Bahnmuller , Stefanie Eiden , Olaf Behrend , Diana Dimova Landen , Matthias Boll
IPC分类号： H01B1/24 , B05D5/12 , B32B3/00
CPC分类号： C09D11/52 , Y10T428/24893
摘要： Aqueous, printable compositions comprising carbon nanotubes and a polymeric dispersing agent, wherein at least one fifth of the carbon nanotubes have a molecular structure comprising a plurality of stacked and rolled graphene layers; processes for preparing such compositions, methods of use and electrically conductive coatings prepared therewith.
摘要翻译：包含碳纳米管和聚合物分散剂的水性可印刷组合物，其中至少五分之一的碳纳米管具有包括多个层叠和滚动的石墨烯层的分子结构; 制备这种组合物的方法，使用方法和用其制备的导电涂层。

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