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1. 发明授权

US08501897B2 Method for producing liquid-crystalline polyester 失效
标题翻译：液晶聚酯的制造方法
公开(公告)号：US08501897B2
公开(公告)日：2013-08-06
申请号：US13556871
申请日：2012-07-24
申请人： Tomoya Hosoda , Eiji Hosoda , Masanobu Matsubara
发明人： Tomoya Hosoda , Eiji Hosoda , Masanobu Matsubara
IPC分类号： C08G63/02 , C08G64/00
CPC分类号： C09K19/3809 , C08G63/605 , C08G63/87
摘要： The present invention provides a method for producing a liquid-crystalline polyester, which comprises melt-polymerizing monomers in a reactor having a draw outlet to obtain a polymer melt and drawing the polymer melt through the draw outlet, characterized in that the monomers comprise a compound selected from an aromatic hydroxycarboxylic acid and derivatives thereof, a compound selected from an aromatic dicarboxylic acid and derivatives thereof and a compound selected from an aromatic diol, an aromatic hydroxyamine, an aromatic diamine and derivatives thereof; the amount of units derived from a compound containing a 1,2-phenylene and/or a 1,3-phenylene skeleton(s) in the polyester is from 0 to 10 mol %; the melt polymerization is performed in the presence of a heterocyclic compound containing two or more nitrogen atoms; and the polymer melt has a flow initiation temperature of from 220 to 250° C.
摘要翻译：本发明提供一种液晶聚酯的制造方法，其包括在具有拉出口的反应器中使单体熔融聚合以获得聚合物熔体并通过拉出口拉伸聚合物熔体，其特征在于，所述单体包含化合物选自芳族羟基羧酸及其衍生物，选自芳族二羧酸及其衍生物的化合物和选自芳族二醇，芳族羟胺，芳族二胺及其衍生物的化合物; 衍生自聚酯中含有1,2-亚苯基和/或1,3-亚苯基骨架的化合物的单元的量为0至10mol％; 在含有两个或更多个氮原子的杂环化合物的存在下进行熔融聚合; 聚合物熔体的起始温度为220-250℃。

2. 发明申请

US20130030142A1 METHOD FOR PRODUCING LIQUID-CRYSTALLINE POLYESTER 失效
标题翻译：生产液晶聚酯的方法
公开(公告)号：US20130030142A1
公开(公告)日：2013-01-31
申请号：US13556963
申请日：2012-07-24
申请人： Tomoya HOSODA , Eiji Hosoda , Masanobu Matsubara
发明人： Tomoya HOSODA , Eiji Hosoda , Masanobu Matsubara
IPC分类号： C08G63/60
CPC分类号： C09K19/3809 , C08G63/605 , C08G63/80 , C08G63/87
摘要： The present invention provides a method for producing a liquid-crystalline polyester, the method comprising: a step of melt-polymerizing raw monomers in a melt polymerization vessel to obtain a polymer melt; a step of drawing the polymer melt from the melt polymerization vessel and granulating the polymer melt to obtain a granulate; a step of allowing the granulate to undergo solid phase polymerization in a solid phase polymerization vessel to obtain a solid phase polymer; and a step of making an impact on the solid phase polymerization vessel containing the solid phase polymer, and taking out the solid phase polymer from the solid phase polymerization vessel.
摘要翻译：本发明提供了一种液晶聚酯的制造方法，该方法包括：在熔融聚合容器中熔融聚合原料单体以获得聚合物熔体; 从熔融聚合容器中拉伸聚合物熔体并使聚合物熔体成粒以获得颗粒的步骤; 使该颗粒在固相聚合釜中进行固相聚合以获得固相聚合物的步骤; 以及对含有固相聚合物的固相聚合容器产生影响，从固相聚合容器中取出固相聚合物的步骤。

3. 发明申请

US20090205965A1 Method and apparatus for forming oxide coating 有权
标题翻译：用于形成氧化物涂层的方法和装置
公开(公告)号：US20090205965A1
公开(公告)日：2009-08-20
申请号：US10583775
申请日：2004-11-09
申请人： Wataru Kurokawa , Hiroshi Matsubayashi , Mitsuhide Aihara , Masanobu Matsubara , Masatoki Ishida , Norimasa Maida
发明人： Wataru Kurokawa , Hiroshi Matsubayashi , Mitsuhide Aihara , Masanobu Matsubara , Masatoki Ishida , Norimasa Maida
IPC分类号： C25D11/00
CPC分类号： C23C8/40 , C25D9/08
摘要： Disclosed are a method and an apparatus for forming an oxide coating film with excellent corrosion resistance and adhesiveness on a cathode made of a metal plate by a simple process at low cost. A direct current voltage is applied between an anode (12) and a cathode (13) in an electrolyte solution which cathode (13) is made of a metal plate to be coated with oxide and arranged opposite to the anode (12), while supplying oxygen or a gas containing oxygen into the electrolyte solution, so that the metal plate cathode (13) is coated with oxide, thereby being formed into a oxide-coated metal plate.
摘要翻译：公开了一种通过简单的方法以低成本形成由金属板制成的阴极，具有优异的耐腐蚀性和粘附性的氧化物涂膜的方法和装置。在电解质溶液中的阳极（12）和阴极（13）之间施加直流电压，阴极（13）由要镀有氧化物的金属板制成并与阳极（12）相对设置，同时供应氧气或含氧的气体进入电解质溶液中，使得金属板阴极（13）涂覆氧化物，从而形成氧化物涂覆的金属板。

4. 发明授权

US5525725A Process for producing a high purity caprolactam 失效
公开(公告)号：US5525725A
公开(公告)日：1996-06-11
申请号：US293180
申请日：1994-08-19
申请人： Yasuhiko Higashio , Hiroshi Kajikuri , Keisuke Sugita , Hideki Doi , Masanobu Matsubara
发明人： Yasuhiko Higashio , Hiroshi Kajikuri , Keisuke Sugita , Hideki Doi , Masanobu Matsubara
IPC分类号： C07D201/16 , C07D201/04 , C07D201/06
CPC分类号： C07D201/16
摘要： A process for producing a high purity caprolactam is disclosed in which a crude caprolactam obtained by a catalytic rearrangement of cyclohexanone oxime is subjected(1) to mixing, while stirring, with at least one hydrocarbon selected from the group consisting of aliphatic hydrocarbons and alicyclic hydrocarbons to form a liquid-liquid, two-layer liquid mixture, and then crystallizing caprolactam out of the liquid mixture;(2) to mixing with both at least one hydrocarbon selected from the group consisting of aliphatic hydrocarbons and alicyclic hydrocarbons, and water to form a liquid mixture, separating the liquid mixture into a hydrocarbon layer and a water layer, and then recovering caprolactam from the water layer; or(3) to distillation in the co-presence of at least one aliphatic saturated hydrocarbon of 10 to 18 carbon atoms.

5. 发明授权

US08492500B2 Method for producing liquid-crystalline polyester 失效
标题翻译：液晶聚酯的制造方法
公开(公告)号：US08492500B2
公开(公告)日：2013-07-23
申请号：US13556963
申请日：2012-07-24
申请人： Tomoya Hosoda , Eiji Hosoda , Masanobu Matsubara
发明人： Tomoya Hosoda , Eiji Hosoda , Masanobu Matsubara
IPC分类号： C08G63/02 , C08G64/00
CPC分类号： C09K19/3809 , C08G63/605 , C08G63/80 , C08G63/87
摘要： The present invention provides a method for producing a liquid-crystalline polyester, the method comprising: a step of melt-polymerizing raw monomers in a melt polymerization vessel to obtain a polymer melt; a step of drawing the polymer melt from the melt polymerization vessel and granulating the polymer melt to obtain a granulate; a step of allowing the granulate to undergo solid phase polymerization in a solid phase polymerization vessel to obtain a solid phase polymer; and a step of making an impact on the solid phase polymerization vessel containing the solid phase polymer, and taking out the solid phase polymer from the solid phase polymerization vessel.
摘要翻译：本发明提供了一种液晶聚酯的制造方法，该方法包括：在熔融聚合容器中熔融聚合原料单体以获得聚合物熔体; 从熔融聚合容器中拉伸聚合物熔体并使聚合物熔体成粒以获得颗粒的步骤; 使该颗粒在固相聚合釜中进行固相聚合以获得固相聚合物的步骤; 以及对含有固相聚合物的固相聚合容器产生影响，从固相聚合容器中取出固相聚合物的步骤。

6. 发明申请

US20130030141A1 METHOD FOR PRODUCING LIQUID-CRYSTALLINE POLYESTER 失效
标题翻译：生产液晶聚酯的方法
公开(公告)号：US20130030141A1
公开(公告)日：2013-01-31
申请号：US13556871
申请日：2012-07-24
申请人： Tomoya HOSODA , Eiji HOSODA , Masanobu MATSUBARA
发明人： Tomoya HOSODA , Eiji HOSODA , Masanobu MATSUBARA
IPC分类号： C08G63/60
CPC分类号： C09K19/3809 , C08G63/605 , C08G63/87
摘要： The present invention provides a method for producing a liquid-crystalline polyester, which comprises melt-polymerizing monomers in a reactor having a draw outlet to obtain a polymer melt and drawing the polymer melt through the draw outlet, characterized in that the monomers comprise a compound selected from an aromatic hydroxycarboxylic acid and derivatives thereof, a compound selected from an aromatic dicarboxylic acid and derivatives thereof and a compound selected from an aromatic diol, an aromatic hydroxyamine, an aromatic diamine and derivatives thereof; the amount of units derived from a compound containing a 1,2-phenylene and/or a 1,3-phenylene skeleton(s) in the polyester is from 0 to 10 mold; the melt polymerization is performed in the presence of a heterocyclic compound containing two or more nitrogen atoms; and the polymer melt has a flow initiation temperature of from 220 to 250° C.
摘要翻译：本发明提供一种液晶聚酯的制造方法，其包括在具有拉出口的反应器中使单体熔融聚合以获得聚合物熔体并通过拉出口拉伸聚合物熔体，其特征在于，所述单体包含化合物选自芳族羟基羧酸及其衍生物，选自芳族二羧酸及其衍生物的化合物和选自芳族二醇，芳族羟胺，芳族二胺及其衍生物的化合物; 衍生自在聚酯中含有1,2-亚苯基和/或1,3-亚苯基骨架的化合物的单元的量为0至10个模具; 在含有两个或更多个氮原子的杂环化合物的存在下进行熔融聚合; 聚合物熔体的起始温度为220-250℃。

7. 发明申请

US20100300527A1 SUBSTRATE FOR COMPOUND SEMICONDUCTOR SOLAR CELL 审中-公开
标题翻译：复合半导体太阳能电池基板
公开(公告)号：US20100300527A1
公开(公告)日：2010-12-02
申请号：US12790213
申请日：2010-05-28
申请人： Hiroshi Okamura , Hirofumi Yamano , Masanobu Matsubara , Shigeyoshi Nishiyama
发明人： Hiroshi Okamura , Hirofumi Yamano , Masanobu Matsubara , Shigeyoshi Nishiyama
IPC分类号： H01L31/0216
CPC分类号： H01L31/0392 , H01L31/03928 , Y02E10/541
摘要： [Problem] A substrate for a compound semiconductor solar cell which maintains excellent elasticity even after a high temperature process at the time of forming a thin film is provided.[Means for Resolution] The substrate for a compound semiconductor solar cell is formed of a steel plate, and a Cr layer having a coating film quantity of 300 to 8000 mg/m2 is formed on a surface of the substrate on a side to which a solar cell layer is laminated. The Cr layer having a coating film quantity of 500 to 3000 mg/m2 may be formed on the surface of the substrate on a side to which the solar cell layer is laminated, and a film forming temperature of the solar cell layer is less than 550° C. The Cr layer having a coating film quantity of 2000 to 8000 mg/m2 may be formed on the surface of the substrate on a side to which the solar cell layer is laminated, and a film forming temperature of the solar cell layer is more than 800° C. The Cr layer having a coating film quantity of 2000 to 5000 mg/m2 may be formed on the surface of the substrate on a side to which the solar cell layer is laminated, and a film forming temperature of the solar cell layer is not less than 550° C. and not more than 800° C. A quantity of Mn component in a steel strip is not more than 2 wt % . A quantity of Fe component in the steel strip is not more than 98 wt %.
摘要翻译： [问题]提供了一种化合物半导体太阳能电池的基板，其即使在形成薄膜时的高温处理之后也保持优异的弹性。 [解决方法]化合物半导体太阳能电池用基板由钢板形成，并且在基板的表面上形成具有300〜8000mg / m 2的涂膜量的Cr层，层叠太阳能电池层。可以在层叠有太阳能电池层的一侧的基板的表面上形成涂膜量为500〜3000mg / m 2的Cr层，并且太阳能电池层的成膜温度小于550 可以在层叠太阳能电池层的基板的表面上形成涂膜量为2000〜8000mg / m 2的Cr层，太阳能电池层的成膜温度为超过800℃。可以在层叠太阳能电池层的一侧的基板的表面上形成涂膜量为2000〜5000mg / m 2的Cr层，并且形成太阳能电池层的成膜温度电池层不低于550℃并且不超过800℃。钢带中的Mn组分的量不大于2重量％。钢带中的Fe成分量不大于98重量％。

8. 发明授权

US5459261A Process for producing a high purity caprolactam 失效
标题翻译：生产高纯度己内酰胺的方法
公开(公告)号：US5459261A
公开(公告)日：1995-10-17
申请号：US289577
申请日：1994-08-15
申请人： Yasuhiko Higashio , Hiroshi Kajikuri , Keisuke Sugita , Hideki Doi , Masanobu Matsubara
发明人： Yasuhiko Higashio , Hiroshi Kajikuri , Keisuke Sugita , Hideki Doi , Masanobu Matsubara
IPC分类号： C07D201/16 , C07D201/14
CPC分类号： C07D201/16
摘要： A process for producing a high purity caprolactam is disclosed in which a crude caprolactam obtained by a catalytic rearrangement of cyclohexanone oxime is subjected(1) to mixing, while stirring, with at least one hydrocarbon selected from the group consisting of aliphatic hydrocarbons and alicyclic hydrocarbons to form a liquid-liquid, two-layer liquid mixture, and then crystallizing caprolactam out of the liquid mixture;(2) to mixing with both at least one hydrocarbon selected from the group consisting of aliphatic hydrocarbons and alicyclic hydrocarbons, and water to form a liquid mixture, separating the liquid mixture into a hydrocarbon layer and a water layer, and then recovering caprolactam from the water layer; or(3) to distillation in the co-presence of at least one aliphatic saturated hydrocarbon of 10 to 18 carbon atoms.
摘要翻译：公开了一种制备高纯度己内酰胺的方法，其中通过环己酮肟的催化重排获得的粗己内酰胺在搅拌下与至少一种选自脂族烃和脂环族烃的烃进行混合形成液 - 液两层液体混合物，然后从该液体混合物中结晶己内酰胺; （2）与选自脂族烃和脂环烃的至少一种烃和水混合以形成液体混合物，将液体混合物分离成烃层和水层，然后从其中回收己内酰胺水层; 或（3）在至少一种10至18个碳原子的脂族饱和烃的共存下进行蒸馏。

9. 发明授权

US5362870A Process for producing a high purity caprolactam 失效
标题翻译：生产高纯度己内酰胺的方法
公开(公告)号：US5362870A
公开(公告)日：1994-11-08
申请号：US46146
申请日：1993-04-15
申请人： Yasuhiko Higashio , Hiroshi Kajikuri , Keisuke Sugita , Hideki Doi , Masanobu Matsubara
发明人： Yasuhiko Higashio , Hiroshi Kajikuri , Keisuke Sugita , Hideki Doi , Masanobu Matsubara
IPC分类号： C07D201/16
CPC分类号： C07D201/16
摘要： A process for producing a high purity caprolactam is disclosed in which a crude caprolactam obtained by a catalytic rearrangement of cyclohexanone oxime is subjected(1) to mixing, while stirring, with at least one hydrocarbon selected from the group consisting of aliphatic hydrocarbons and alicyclic hydrocarbons to form a liquid-liquid, two-layer liquid mixture, and then crystallizing caprolactam out of the liquid mixture;(2) to mixing with both at least one hydrocarbon selected from the group consisting of aliphatic hydrocarbons and alicyclic hydrocarbons, and water to form a liquid mixture, separating the liquid mixture into a hydrocarbon layer and a water layer, and then recovering caprolactam from the water layer; or(3) to distillation in the co-presence of at least one aliphatic saturated hydrocarbon of 10 to 18 carbon atoms.
摘要翻译：公开了一种制备高纯度己内酰胺的方法，其中通过环己酮肟的催化重排获得的粗己内酰胺在搅拌下与至少一种选自脂族烃和脂环族烃的烃进行混合形成液 - 液两层液体混合物，然后从该液体混合物中结晶己内酰胺; （2）与选自脂族烃和脂环烃的至少一种烃和水混合以形成液体混合物，将液体混合物分离成烃层和水层，然后从其中回收己内酰胺水层; 或（3）在至少一种10至18个碳原子的脂族饱和烃的共存下进行蒸馏。

10. 发明申请

US20120329975A1 METHOD FOR PRODUCING LIQUID CRYSTAL POLYESTER 审中-公开
标题翻译：生产液晶聚酯的方法
公开(公告)号：US20120329975A1
公开(公告)日：2012-12-27
申请号：US13488935
申请日：2012-06-05
申请人： Tomoya HOSODA , Eiji HOSODA , Masanobu MATSUBARA
发明人： Tomoya HOSODA , Eiji HOSODA , Masanobu MATSUBARA
IPC分类号： C08G63/87
CPC分类号： C09K19/3809 , C08G63/605 , C08G63/80
摘要： Disclosed is a method for producing a liquid crystal polyester, which includes the following steps of: (1) melt-polycondensing a compound as a monomer in a polymerization tank to produce a prepolymer; (2) discharging the prepolymer from the polymerization tank in a molten state, and solidifying the prepolymer through cooling to produce a sheet in which a portion having a thickness of 1.6 to 2 mm accounts for 80% by mass or more (of 100% by mass of the entire sheet); (3) crushing the sheet; and (4) subjecting the crushed product to solid-phase polymerization through heating.
摘要翻译：公开了一种液晶聚酯的制备方法，其包括以下步骤：（1）在聚合槽中熔融缩聚作为单体的化合物以制备预聚物; （2）以熔融状态从聚合槽中排出预聚物，并通过冷却使预聚物固化，得到厚度为1.6〜2mm的部分为80质量％以上（100％× 整个纸张的质量）; （3）破碎片材; 和（4）通过加热对粉碎产物进行固相聚合。

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