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1. 发明授权

US08801804B2 Non-metal tanning process 有权
标题翻译：非金属鞣制工艺
公开(公告)号：US08801804B2
公开(公告)日：2014-08-12
申请号：US13879230
申请日：2011-10-05
申请人： Claus Reineking , Roberta Gamarino , Licia Trimarco , Maurizio Quaglierini , Markus Gisler , Rainer Nusser
发明人： Claus Reineking , Roberta Gamarino , Licia Trimarco , Maurizio Quaglierini , Markus Gisler , Rainer Nusser
IPC分类号： C14C3/26 , C07D237/06 , C14C3/00 , C14C3/02 , C14C3/04 , C07D237/00 , C07D247/02 , C07D239/02
CPC分类号： C14C3/00 , C07D237/00 , C07D237/06 , C07D239/02 , C07D247/02 , C14C3/02 , C14C3/04 , C14C3/26
摘要： Tanned leather, skin or pelt is produced by non-metal tanning, comprising the step of tanning a bated hide, skin or belt with a tanning agent (A) of at least a mixture of compounds of formula (I) and formula (II), wherein Hal signifies fluorine or chlorine, R1 signifies hydrogen, C1-8-alkyl or an alkyleneoxy radical of formula (III), —(—C2-3 alkylene-O—)q—H (III); R2 signifies a) phenyl, mono- or di-substituted with SO3M or COOM and optionally substituted also with hydroxyl, C1-4-alkyl C1-4-alkoxy; b) naphthyl, mono- or di- or tri-substituted with SO3M and optionally substituted also with hydroxyl; c) C1-8-alkylene, substituted with (SO3M) or (COOM); d) aradical of formula (IV), —(—C2-3 alkylene-O—)p—Y (IV) or e) a radical of formula (IVa) —(C2-3 alkylene-O)p—C2-3 alkylene-SO2CH2CH2O—Y (IVa), M signifies 1 or 2, p signifies 0 or 1, Y signifies hydrogen or —SO3M, q signifies 1 to 10, M signifies hydrogen, an alkali metal cation or an ammonium cation being aprotonated tertiary amine or a quaternary ammonium cation, R3 signifies hydrogen or chlorine. In a tanning bath having a pH of from 6 to 10 at the beginning of tanning step.
摘要翻译：鞣制的皮革，皮肤或毛皮是通过非金属鞣制生产的，其包括用至少一种式（I）和式（II）的化合物的混合物的鞣剂（A）鞣制皮肤，皮肤或皮带的步骤，其中Hal表示氟或氯，R1表示氢，C1-8 - 烷基或式（III）的亚烷基氧基， - （ - C2-3亚烷基-O-）q-H（III）; R2表示a）苯基，被SO 3 M或COOM单取代或二取代，并任选也被羟基，C 1-4 - 烷基C 1-4 - 烷氧基取代; b）萘基，被SO 3 M单取代或二取代或三取代，并任选被羟基取代; c）被（SO 3 M）或（COOM）取代的C 1-8亚烷基; （IV）， - （ - C2-3亚烷基-O-）p-Y（IV）或e）式（Ⅳa） - （C2-3亚烷基-O）p-C2-3的基团亚烷基-SO 2 CH 2 CH 2 O-Y（IVa），M表示1或2，p表示0或1，Y表示氢或-SO 3 M，q表示1至10，M表示氢，碱金属阳离子或铵阳离子为非质子化叔胺或季铵阳离子，R3表示氢或氯。在鞣制步骤开始时pH为6〜10的鞣制浴。

2. 发明授权

US07091328B2 Fiber-reactive mono-azo dyes 有权
标题翻译：纤维反应性单偶氮染料
公开(公告)号：US07091328B2
公开(公告)日：2006-08-15
申请号：US10475624
申请日：2002-04-15
申请人： Roland Wald , Markus Gisler
发明人： Roland Wald , Markus Gisler
IPC分类号： C09B62/51 , C09B67/22 , C09D11/02 , D06P1/384
CPC分类号： C09B67/0051 , C09B62/4413
摘要： According to the invention there are provided fiber-reactive dyestuffs which are compounds of the formula (I) wherein the substituents are defined as in claim 1, a process making the same and their use in dyeing or printing hydroxy-group-containing organic substrates.
摘要翻译：根据本发明，提供了作为式（I）化合物的纤维反应性染料，其中取代基如权利要求1中所定义，其制备方法及其在染色或印刷含羟基的有机底物中的用途。

3. 发明授权

US5597903A Disazo dyes containing 1-amino-8-hydroxy-naphthalene-3,6-or 4,6-disulfonic acid biscoupling component radicals and 5-cyano-2, 4-or 4,6-dichloropyrimidyl fiber-reactive groups 失效
公开(公告)号：US5597903A
公开(公告)日：1997-01-28
申请号：US470669
申请日：1995-06-06
申请人： Markus Gisler
发明人： Markus Gisler
IPC分类号： C09B62/25 , C09B62/44 , C09B62/513 , C09B62/533 , D06P1/39 , D06P3/66 , C09B62/08
CPC分类号： C09B62/4424 , C09B62/25
摘要： Compounds of the formula ##STR1## salts thereof, and mixtures of such compounds and salts, wherein D.sub.1 is ##STR2## wherein R.sub.1 is hydrogen, halo, C.sub.1-4 alkyl, C.sub.1-4 alkoxy, --SO.sub.3 H or --COOH,R.sub.2 is --COOH, --CONR.sub.6 R.sub.7, --SO.sub.2 NR.sub.6 R.sub.7 or --SO.sub.2 --X, wherein each of R.sub.6 and R.sub.7 is independently hydrogen, C.sub.1-4 alkyl, C.sub.2-4 -hydroxyalkyl or C.sub.2-4 sulfatoalkyl, or--NR.sub.6 R.sub.7 is a saturated 5- or 6-membered heterocyclic ring containing no hetero atom in addition to the nitrogen atom to which R.sub.6 and R.sub.7 are attached or containing one hetero atom selected from nitrogen and oxygen in addition to said nitrogen atom, which ring is unsubstituted or substituted by 1 to 3 C.sub.1-4 alkyl groups, andm is 0, 1 or 2, andD.sub.2 is ##STR3## wherein R.sub.3 is hydrogen, --SO.sub.3 H or --COOH,R.sub.4 is hydrogen, C.sub.1-4 alkyl or C.sub.1-4 alkyl monosubstituted by hydroxy, halo, cyano, --SO.sub.3 H, --OSO.sub.3 H or --COOH,n is 0 or 1, andp is 1 or 2,whereinX is --CH.dbd.CH.sub.2 or --W--Y,whereinW is linear or branched C.sub.2-4 alkylene, andY is hydroxy or a group which can be split off under alkaline conditions,with the provisos that (i) R.sub.1 may be --COOH only when R.sub.2 is --SO.sub.2 --X, (ii) D.sub.2 must be a group of Formula (d) when D.sub.1 is a group of Formula (a) wherein R.sub.1 is hydrogen, halo, C.sub.1-4 alkyl, C.sub.1-4 alkoxy or --SO.sub.3 H, and R.sub.2 is --COOH, --CONR.sub.6 R.sub.7 or --SO.sub.2 NR.sub.6 R.sub.7 or a group of Formula (b), and (iii) D.sub.2 must be a group of Formula (e) when D.sub.1 is a group of Formula (a) wherein R.sub.1 is --COOH, and R.sub.2 is --SO.sub.2 --X, useful for dyeing or printing hydroxy group- or nitrogen-containing organic substrates, for example leather and fiber material comprising natural or synthetic polyamides or natural or regenerated cellulose, especially textile material comprising cotton. The obtained dyeings and printings show good general fastness properties such as good light fastness, wet fastnesses and resistance towards oxidative influences.

4. 发明授权

US5527886A Dyes containing 5-cyano-2,4 or 4,6-dichloropyrimidyl fiber-reactive groups 失效
标题翻译：染料含有5-氰基-2,4或4,6-二氯嘧啶基纤维反应性基团
公开(公告)号：US5527886A
公开(公告)日：1996-06-18
申请号：US899570
申请日：1992-06-16
申请人： Gunther Auerbach , Markus Dorr , Paul Doswald , Markus Gisler , Werner Koch , Helmut A. Moser , Roland Wald
发明人： Gunther Auerbach , Markus Dorr , Paul Doswald , Markus Gisler , Werner Koch , Helmut A. Moser , Roland Wald
IPC分类号： C09B62/44 , C09B62/08 , C07F3/10 , C07F9/02
CPC分类号： C09B62/4422
摘要： Fiber-reactive compounds of the formulaX-O.sub.2 S-W.sub.1 [F.sub.c ]W.sub.2 -NR-Z,and water-soluble salts thereof each cation of which is independently a non-chromophoric cation, and mixtures of such compounds or water-soluble salts,whereinFc is a chromophore-containing radical of a monoazo, disazo, polyazo, formazan, anthraquinone, dioxazine, phenazine or azomethine dye, which is in metal-free or metal complex form,each of W.sub.1 and W.sub.2 is independently a direct bond or a bridging group which is attached to a carbon atom of an aromatic carbocyclic ring or to a carbon or nitrogen atom of an aromatic heterocyclic ring present in F.sub.c,X is --CH.dbd.CH.sub.2 or --C.sub.2-4 alkylene--Y, wherein Y is hydroxy or a group which can be split off under alkaline conditions,R is hydrogen, C.sub.1-4 alkyl or C.sub.1-4 alkyl monosubstituted by hydroxy, halo, cyano, --SO.sub.3 H, --OSO.sub.3 H or --COOH, andZ is ##STR1## with the provisos as set forth herein.
摘要翻译：式X-O 2 S-W1 [Fc] W2-NR-Z的纤维反应性化合物及其各自阳离子独立地是非发色阳离子的水溶性盐，以及这些化合物或水溶性盐的混合物，其中Fc是含有金属或金属络合物形式的单偶氮，二偶氮，多偶氮，甲an，蒽醌，二恶嗪，吩嗪或偶氮甲碱染料的含发色团的基团，W1和W2各自独立地为直接键或连接于芳香族碳环的碳原子或存在于Fc中的芳香族杂环的碳原子或氮原子上的桥连基团，X为-CH = CH 2或-C 2-4亚烷基-Y，其中Y为羟基或基团可以在碱性条件下分离，R是氢，C 1-4烷基或被羟基，卤素，氰基，-SO 3 H，-OSO 3 H或-COOH单取代的C 1-4烷基，Z是，条件是如上所述这里。

5. 发明授权

US5491221A Fibre-reactive copper-complex formazan compounds which contain a difluoropyrimidinyl group 失效
标题翻译：含有二氟嘧啶基的纤维反应性铜络合物甲an化合物
公开(公告)号：US5491221A
公开(公告)日：1996-02-13
申请号：US247154
申请日：1994-05-20
申请人： Markus Gisler , Roland Wald
发明人： Markus Gisler , Roland Wald
IPC分类号： C09B62/20 , C09B62/44 , C09B62/465 , D06P1/38
CPC分类号： C09B62/205 , C09B62/4422
摘要： Fibre-reactive formazan compounds, salts thereof or free acid forms thereof according to formula (I) ##STR1## in which R.sub.1 is hydrogen or --COOH, each of R.sub.2 and R.sub.4 is independently hydrogen, --COOH, --SO.sub.3 H, --NHCOCH.sub.3, --NHCOCHY.sub.2 --CH.sub.2 Y.sub.1, --NHCOCY.sub.2 .dbd.CH.sub.2 or --NHCOCH.sub.2 Y.sub.1,R.sub.3 is hydrogen, halogen, C.sub.1-4 alkyl, C.sub.1-4 alkoxy, --COOH or --SO.sub.3 H,Y.sub.1 is chlorine, bromine, --OSO.sub.3 H or --SSO.sub.3 H,Y.sub.2 is hydrogen, chlorine or bromine, andZ is ##STR2## The compounds are particularly useful in dyeing or printing hydroxy-group containing or nitrogen-containing organic substrates, including leather, fiber materials, and textiles.
摘要翻译：根据式（I）的纤维反应性甲an化合物，其盐或游离酸形式，R 2和R 4各自独立地是氢，-COOH，-SO 3 H，-NHCOCH 3，-NHCOCHY 2 -CH 2 Y 1，-NHCOCY 2 = CH 2或-NHCOCH 2 Y 1 ，R3为氢，卤素，C1-4烷基，C1-4烷氧基，-COOH或-SO3H，Y1为氯，溴，-OSO3H或-SSO3H，Y2为氢，氯或溴，Z为化合物特别适用于染色或印刷包含皮革，纤维材料和纺织品的含羟基或含氮有机基材。

6. 发明授权

US5216136A Fiber-reactive disazo dyes containing piperazino linking radicals and processes of dyeing therewith 失效
标题翻译：含有哌嗪基连接基团的纤维反应性双偶氮染料及其染色方法
公开(公告)号：US5216136A
公开(公告)日：1993-06-01
申请号：US674440
申请日：1991-03-22
申请人： Markus Gisler
发明人： Markus Gisler
IPC分类号： C09B62/04
CPC分类号： C09B62/043
摘要： Compounds of the formula ##STR1## and salts thereof, and their use as as reactive dyes for the dyeing and printing of hydroxy group- and nitrogen- containing organic substrates, e.g., leather, natural and synthetic polyamides and natural and regenerated cellulose.
摘要翻译：式中的化合物及其盐，以及它们用于染料和印刷含羟基和含氮有机基质（如皮革，天然和合成聚酰胺）的活性染料的用途和天然和再生纤维素。

7. 发明授权

US08795389B2 Non metal tanning 有权
标题翻译：非金属鞣制
公开(公告)号：US08795389B2
公开(公告)日：2014-08-05
申请号：US13879172
申请日：2011-10-05
申请人： Claus Reineking , Roberta Gamarino , Licia Trimarco , Maurizio Quaglierini , Markus Gisler , Rainer Nusser
发明人： Claus Reineking , Roberta Gamarino , Licia Trimarco , Maurizio Quaglierini , Markus Gisler , Rainer Nusser
IPC分类号： C14C3/26 , C14C3/00 , C14C3/02 , C14C3/04 , C14C3/08 , C07D253/00 , C07D253/065 , C07D253/07 , C07D253/075
CPC分类号： C14C3/00 , C07D251/44 , C07D253/00 , C07D253/065 , C07D253/07 , C07D253/075 , C14C3/02 , C14C3/04 , C14C3/08 , C14C3/26 , C14C3/28
摘要： Tanned leather, skin or pelt is produced by non-metal tanning, comprising the step of tanning a bated hide, skin or pelt with a tanning agent (A), the tanning agent (A) being at least one compound of a formula (I), wherein X signifies fluorine or chlorine, and/or (+NR3)0-1, wherein R is a substituted or unsubstituted C1 to C6 alkyl group, a substituted or unsubstituted C6 to C10 aryl or a C5 to C6heteroaryl group, R1 signifies hydrogen, C1-8-alkyl or an alkyleneoxy radical of a formula (Ia), -(—C2-3 alkylene-O—)q—H (Ia), R2 signifies hydrogen or hydroxyl, m, signifies 1, 2 or 3, q is of from 1 to 10, M signifies hydrogen or an alkali metal cation or an ammonium cation, being a protonated tertiary amine or a quaternary ammonium cation, in a tanning bath having a pH of from 6 to 10 at the beginning of tanning step.
摘要翻译：鞣制的皮革，皮肤或毛皮是通过非金属鞣制制成的，包括用鞣剂（A）鞣制皮肤，皮肤或皮肤的步骤，鞣剂（A）是至少一种式（I ），其中X表示氟或氯，和/或（+ NR3）0-1，其中R是取代或未取代的C1至C6烷基，取代或未取代的C6至C10芳基或C5至C6杂芳基，R1表示氢，C1-8烷基或式（Ia）的亚烷基氧基， - （ - C2-3亚烷基-O-）q-H（Ia），R2表示氢或羟基，m表示1,2或3 q为1〜10，M表示在鞣制开始时pH为6〜10的鞣制浴中的氢或碱金属阳离子或铵阳离子，为质子化叔胺或季铵阳离子步。

8. 发明授权

US08790416B2 Non-metal tanning process 有权
标题翻译：非金属鞣制工艺
公开(公告)号：US08790416B2
公开(公告)日：2014-07-29
申请号：US13879207
申请日：2011-10-05
申请人： Claus Reineking , Roberta Gamarino , Licia Trimarco , Maurizio Quaglierini , Markus Gisler , Rainer Nusser
发明人： Claus Reineking , Roberta Gamarino , Licia Trimarco , Maurizio Quaglierini , Markus Gisler , Rainer Nusser
IPC分类号： C14C3/26 , C14C3/00 , C14C3/02 , C14C3/04 , C14C3/08 , C07D251/44 , C07D253/00 , C07D253/07 , C07D253/075
CPC分类号： C14C3/00 , C07D251/44 , C07D253/00 , C07D253/07 , C07D253/075 , C14C3/02 , C14C3/04 , C14C3/08 , C14C3/26 , C14C3/28
摘要： Tanned leather, skin or pelt is produced by non-metal tanning, comprising the step of tanning a bated hide, skin or pelt with a tanning agent (A), the tanning agent (A) being at least one compound of a formula (I), wherein X signifies fluorine or chlorine, and/or (+NR3)0-1, wherein R is a substituted or unsubstituted C1 to C6 alkyl group, a substituted or unsubstituted C6 to C10 aryl or a C5 to C6 heteroaryl group, R1 signifies hydrogen, C1-8-alkyl or an alkyleneoxy radical of a formula (Ia), —(—C2-3 alkylene-O—)q—H (Ia), R2 signifies hydrogen, hydroxyl, C1-4-alkyl or C1-4-alkoxy, m, signifies 1 or 2, n signifies 0 to 2, q is of from 1 to 10, M signifies hydrogen or an alkali metal cation or an ammonium cation, the ammonium cation being a protonated tertiary amine or a quaternary ammonium cation, in a tanning bath, the tanning bath having a pH of from 6 to 10 at the beginning of tanning step, wherein the bated hide or skin or pelt is subjected to tanning with (A) without previous pickling.
摘要翻译：鞣制的皮革，皮肤或毛皮是通过非金属鞣制制成的，包括用鞣剂（A）鞣制皮肤，皮肤或皮肤的步骤，鞣剂（A）是至少一种式（I ），其中X表示氟或氯，和/或（+ NR3）0-1，其中R是取代或未取代的C1至C6烷基，取代或未取代的C6至C10芳基或C5至C6杂芳基，R1 表示氢，C 1-8 - 烷基或式（Ia）的亚烷氧基， - （ - C 2-3亚烷基-O-）q -H（Ia），R 2表示氢，羟基，C 1-4 - 烷基或C 1 -4-烷氧基，m表示1或2，n表示0至2，q表示1至10，M表示氢或碱金属阳离子或铵阳离子，铵阳离子为质子化叔胺或季铵铵阳离子，在鞣制浴中，在鞣制步骤开始时，鞣制浴的pH为6至10，其中所述皮肤或皮肤或毛皮用（A）进行鞣制，不需要预先我们酸洗

9. 发明授权

US08790415B2 Non metal tanning 有权
标题翻译：非金属鞣制
公开(公告)号：US08790415B2
公开(公告)日：2014-07-29
申请号：US13879152
申请日：2011-10-05
申请人： Claus Reineking , Roberta Gamarino , Licia Trimarco , Maurizio Quaglierini , Markus Gisler , Rainer Nusser
发明人： Claus Reineking , Roberta Gamarino , Licia Trimarco , Maurizio Quaglierini , Markus Gisler , Rainer Nusser
IPC分类号： C14C3/26
CPC分类号： C14C3/26 , C07D251/44 , C14C3/28
摘要： Tanned leather, skin or pelt is produced by non-metal tanning, comprising the step of tanning a bated hide, skin or pelt with a tanning agent (A), the tanning agent (A) being at least one compound of a formula (I), wherein X signifies fluorine or chlorine, and/or (+NR3)0-1, wherein R is a substituted or unsubstituted C1 to C6 alkyl group, a substituted or unsubstituted C6 to C10 aryl group or a C5 to C6 heteroaryl group, R1 signifies hydrogen, C1-8-alkyl or an alkyleneoxy radical of a formula (Ia), —(—C2-3 alkylene-O—)q—H (Ia), R2 signifies substituted or unsubstituted C2 to C8 alkylenesulphonic acid, substituted or unsubstituted C2 to C8 alkylenecarboxylic acid or an alkyleneoxy radical of formula (Ib), —(—C2-3 alkylene-O—)m—Y (Ib) or an alkylene sulfonyl alkyleneoxy radical of formula (Ic), —(—C2-3 alkylene-O—)p—C2-3 alkylene- SO2CH2O—Y (Ic), m signifies 1 or 2, p signifies 0 or 1, q is of from 1 to 10, Y signifies hydrogen or —SO3M, M signifies hydrogen or an alkali metal cation or an ammonium cation, the ammonium cation being a protonated tertiary amine or a quaternary ammonium cation, in a tanning bath, the tanning bath having a pH of from 6 to 10 at the beginning of tanning step.
摘要翻译：鞣制的皮革，皮肤或毛皮是通过非金属鞣制制成的，包括用鞣剂（A）鞣制皮肤，皮肤或皮肤的步骤，鞣剂（A）是至少一种式（I ），其中X表示氟或氯，和/或（+ NR3）0-1，其中R是取代或未取代的C1至C6烷基，取代或未取代的C6至C10芳基或C5至C6杂芳基， R1表示氢，C1-8 - 烷基或式（Ia）的亚烷基氧基， - （ - C2-3亚烷基-O-）q-H（Ia），R2表示取代或未取代的C2至C8亚烷基磺酸，取代或（C 1 -C 6）的 - （ - C 2-3亚烷基-O-）m-Y（Ib）或亚烷基磺酰基亚烷基氧基， - （ - C2 -3亚烷基-O-）对-C2-3亚烷基-SO2CH2O-Y（Ic），m表示1或2，p表示0或1，q表示1至10，Y表示氢或-SO3M，M表示氢气碱金属阳离子或铵阳离子，铵阳离子是质子化叔胺或季铵阳离子，在鞣制浴中，鞣制浴在鞣制步骤开始时的pH为6至10。

10. 发明申请

US20080233289A1 Dyes Comprising [(4-[2-Amino-3,6-Disulpho-8-Hydroxynaphth-1-Ylazo]Anilino)- 1,3,5-Triazinyl] Moities 审中-公开
标题翻译：包含[（4- [2-氨基-3,6-二磺基-8-羟基萘-1-基]偶氮苯胺基）-1,3,5-三嗪基]摩尔的染料
公开(公告)号：US20080233289A1
公开(公告)日：2008-09-25
申请号：US10573015
申请日：2004-09-23
申请人： Markus Gisler
发明人： Markus Gisler
IPC分类号： B05D5/04 , C09B31/12 , C09D11/02 , C09B43/40
CPC分类号： C09D11/328 , C09B62/043 , C09B62/09
摘要： A dyestuff according to formula (1) or a salt thereof wherein the substituents have the definitions as defined in claim 1. The dyestuffs are useful for dyeing or printing nitrogen-containing or hydroxy-group-containing organic substrates and for the production of (ink-jet) printing inks.
摘要翻译：根据式（1）的染料或其盐，其中取代基具有如权利要求1中所定义的定义。染料可用于染色或印刷含氮或含羟基的有机基材和用于（油墨喷墨）印刷油墨。

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