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1. 发明授权

US08895190B2 Preparation method of lithium-metal composite oxides 有权
标题翻译：锂金属复合氧化物的制备方法
公开(公告)号：US08895190B2
公开(公告)日：2014-11-25
申请号：US12223941
申请日：2007-02-16
申请人： Sung-Kyun Chang , Eui-Yong Bang , Min-Chul Jang , Sang-Hoon Choy , Ki-Young Lee , Wan-Jae Myeong , Kyu-Ho Song , Joo-Hyeong Lee , Young-Sik Hahn , Myung-Ho Cho , Yong-Tae Lee
发明人： Sung-Kyun Chang , Eui-Yong Bang , Min-Chul Jang , Sang-Hoon Choy , Ki-Young Lee , Wan-Jae Myeong , Kyu-Ho Song , Joo-Hyeong Lee , Young-Sik Hahn , Myung-Ho Cho , Yong-Tae Lee
IPC分类号： H01M4/485 , H01M4/88
CPC分类号： H01M4/505 , C01G45/1228 , C01G51/50 , C01G53/50 , C01P2002/72 , C01P2002/74 , C01P2002/86 , C01P2004/03 , C01P2004/32 , C01P2004/61 , C01P2006/11 , C01P2006/12 , C01P2006/13 , C01P2006/40 , H01M4/485 , H01M4/525 , H01M10/052 , H01M2004/021 , Y02P20/544 , Y10T29/49108
摘要： Disclosed is a method for preparing a lithium-metal composite oxide, the method comprising the steps of: (a) mixing an aqueous solution of one or more transition metal-containing precursor compounds with an alkalifying agent and a lithium precursor compound to precipitate hydroxides of the transition metals; (b) mixing the mixture of step (a) with water under supercritical or subcritical conditions to synthesize a lithium-metal composite oxide, and drying the lithium-metal composite oxide; and (c) subjecting the dried lithium-metal composite oxide either to calcination or to granulation and then calcination. Also disclosed are an electrode comprising the lithium-metal composite oxide, and an electrochemical device comprising the electrode. In the disclosed invention, a lithium-metal composite oxide synthesized based on the prior supercritical hydrothermal synthesis method is subjected either to calcination or to granulation and then calcination. Thus, unlike the prior dry calcination method or wet precipitation method, a uniform solid solution can be formed and the ordering of metals in the composite oxide can be improved. Accordingly, the lithium-metal composite oxide can show crystal stability and excellent electrochemical properties.
摘要翻译：公开了一种制备锂金属复合氧化物的方法，该方法包括以下步骤：（a）将一种或多种含过渡金属的前体化合物的水溶液与碱化剂和锂前体化合物混合，以沉淀氢氧化物过渡金属; （b）在超临界或亚临界条件下将步骤（a）的混合物与水混合以合成锂金属复合氧化物，并干燥该锂金属复合氧化物; 和（c）将干燥的锂金属复合氧化物进行煅烧或造粒，然后煅烧。还公开了包含锂金属复合氧化物的电极和包含电极的电化学装置。在所公开的发明中，将基于现有的超临界水热合成方法合成的锂金属复合氧化物进行煅烧或造粒，然后进行煅烧。因此，与现有的干式煅烧法或湿式沉淀法不同，可以形成均匀的固溶体，并且可以提高复合氧化物中的金属的有序性。因此，锂 - 金属复合氧化物可以显示出晶体稳定性和优异的电化学性能。

2. 发明申请

US20140004473A1 METHOD FOR CALCINING ELECTRODE MATERIALS USING A ROTARY KILN 审中-公开
标题翻译：使用旋转窑计算电极材料的方法
公开(公告)号：US20140004473A1
公开(公告)日：2014-01-02
申请号：US14004382
申请日：2012-03-15
申请人： Kyu Ho Song , Kee Do Han , Young Ho Shin
发明人： Kyu Ho Song , Kee Do Han , Young Ho Shin
IPC分类号： H01M4/04 , F27D7/06 , C04B35/64
CPC分类号： H01M4/0471 , C04B35/64 , F27B7/08 , F27B7/3205 , F27B7/33 , F27D7/06 , H01M4/587
摘要： A method of calcining an electrode material using a rotary kiln comprising a heat treatment section which has a cylindrical kiln shell, a supply section for introducing a process material into the kiln shell, and a discharge section for discharging the process material from the kiln shell, wherein the method comprises: introducing particles of the electrode material into the upper part of the kiln shell; flowing a positive pressure gas through the inside of the kiln shell and calcining the electrode material particles while moving them from the upper part to the lower part of the kiln shell; and discharging the electrode material particles from the lower part of the kiln shell.
摘要翻译：一种使用回转窑煅烧电极材料的方法，所述回转窑包括具有圆筒形窑壳的热处理部，用于将处理材料引入窑壳的供给部和用于从窑壳排出处理材料的排出部，其中所述方法包括：将所述电极材料的颗粒引入所述窑壳的上部; 使正压气体流过窑壳的内部，并在从窑壳的上部向下部移动的同时煅烧电极材料颗粒; 并从窑壳的下部排出电极材料颗粒。

3. 发明申请

US20120183980A1 KIT FOR AMPLIFYING DETECTED SIGNAL IN IMMUNOSENSOR AND METHOD FOR DETECTING TARGET ANTIGEN USING THE SAME 审中-公开
标题翻译：用于在免疫传感器中放大检测信号的试剂盒和使用其检测目标抗原的方法
公开(公告)号：US20120183980A1
公开(公告)日：2012-07-19
申请号：US13351816
申请日：2012-01-17
申请人： Tae Young KIM , Sun Kil KANG , Da Yeon KANG , Seung Mok HAN , Kyu Ho SONG , Guei Sam LIM , Ji Su KIM
发明人： Tae Young KIM , Sun Kil KANG , Da Yeon KANG , Seung Mok HAN , Kyu Ho SONG , Guei Sam LIM , Ji Su KIM
IPC分类号： G01N33/53 , G01N33/566 , B82Y5/00
CPC分类号： B82Y5/00 , B82Y15/00 , G01N33/54306 , G01N33/54346 , G01N33/54393
摘要： Disclosed is a kit for amplifying detected signal in immunosensor and a method for detecting target antigen using the same according to the present invention, whereby a target antigen can be effectively detected even by a small amount of target antibody to thereby reduce nonspecific detection signal and to detect an amplified signal.
摘要翻译：公开了用于扩增免疫传感器中的检测信号的试剂盒以及根据本发明的用于检测靶抗原的方法，由此即使通过少量的靶抗体也可以有效地检测靶抗原，从而减少非特异性检测信号，并且检测放大信号。

4. 发明授权

US08206852B2 Lithium-metal composite oxides and electrochemical device using the same 有权
标题翻译：锂金属复合氧化物和电化学装置使用相同
公开(公告)号：US08206852B2
公开(公告)日：2012-06-26
申请号：US12224031
申请日：2007-02-16
申请人： Sung-Kyun Chang , Eui-Yong Bang , Min-Chul Jang , Sang-Hoon Choy , Ki-Young Lee , Saebomi Park , Wan-Jae Myeong , Kyu-Ho Song , Joo-Hyeong Lee , Young-Sik Hahn , Myung-Ho Cho
发明人： Sung-Kyun Chang , Eui-Yong Bang , Min-Chul Jang , Sang-Hoon Choy , Ki-Young Lee , Saebomi Park , Wan-Jae Myeong , Kyu-Ho Song , Joo-Hyeong Lee , Young-Sik Hahn , Myung-Ho Cho
IPC分类号： H01M4/485 , H01M4/505 , H01M4/525 , C01D15/02 , C01G51/04 , C01G45/02
CPC分类号： C01D15/00 , C01G51/42 , C01G51/50 , C01G53/42 , C01G53/50 , C01P2002/74 , C01P2002/86 , C01P2004/03 , C01P2004/32 , C01P2004/61 , C01P2006/11 , C01P2006/12 , C01P2006/40 , C01P2006/42 , H01M4/131 , H01M4/485 , H01M4/505 , H01M4/525 , H01M10/052 , Y02T10/7011 , Y10T428/2982
摘要： The present invention relates to a lithium-containing metal composite oxide comprising paramagnetic and diamagnetic metals, which satisfies any one of the following conditions: (a) the ratio of intensity between a main peak of 0±10 ppm (I0ppm) and a main peak of 240±140 ppm (I240ppm), (I0ppm/I240ppm), is less than 0.117·Z wherein z is the ratio of moles of the diamagnetic metal to moles of lithium; (b) the ratio of line width between the main peak of 0±10 ppm (I0ppm) and the main peak of 240±140 ppm (I240ppm), (W240ppm/W0ppm), is less than 21.45; and (c) both the conditions (a) and (b). The peaks of the lithium-containing metal composite oxide are obtained according to the 7Li—NMR measurement conditions and means disclosed herein.
摘要翻译：本发明涉及包含顺磁性和抗磁性金属的含锂金属复合氧化物，其满足以下条件之一：（a）0±10ppm（I0ppm）的主峰与主峰之间的强度比的240±140ppm（I240ppm）（I0ppm / I240ppm）小于0.117·Z其中z是反磁性金属与摩尔数的摩尔比; （b）0±10ppm（I0ppm）主峰与240±140ppm（I240ppm）主峰之间的线宽比（W240ppm / W0ppm）小于21.45; 和（c）条件（a）和（b）。根据本文公开的7Li-NMR测量条件和手段，获得含锂金属复合氧化物的峰。

5. 发明授权

US07858233B2 Electrode-active anion-deficient non-stoichiometric lithium iron-phosphate, method for preparing the same, and electrochemical device using the same 有权
标题翻译：电极活性阴离子缺乏型非化学计量铁酸锂，其制备方法及使用其的电化学装置
公开(公告)号：US07858233B2
公开(公告)日：2010-12-28
申请号：US12685749
申请日：2010-01-12
申请人： Kyu Ho Song , Wan Jae Myeong , Soo Yeong Han , Kyoo Seung Han
发明人： Kyu Ho Song , Wan Jae Myeong , Soo Yeong Han , Kyoo Seung Han
IPC分类号： H01M4/00
CPC分类号： H01M4/5825 , C01B25/45 , C04B35/447 , C04B35/62695 , C04B2235/3203 , C04B2235/3272 , C04B2235/79 , H01M4/136 , H01M10/052
摘要： The invention provides an anion-deficient non-stoichiometric lithium iron phosphate as an electrode-active material, which is represented by the formula Li1−xFe(PO4)1−y, wherein 0
摘要翻译：本发明提供了一种阴离子不足的非化学计量的磷酸铁锂作为电极活性材料，其由式Li1-xFe（PO4）1-y表示，其中0

6. 发明申请

US20100159600A1 METHOD OF CONTROLLING FLUID FLOW IN MICROFLUIDIC DEVICE AND MICROFLUIDIC ANALYSIS APPARATUS 审中-公开
标题翻译：微流控器件流体流量控制方法及微流控分析仪
公开(公告)号：US20100159600A1
公开(公告)日：2010-06-24
申请号：US12581106
申请日：2009-10-16
申请人： Dong-Ho SHIN , Minsuk JEONG , Kyu Ho SONG , HyeYoon KIM , JuHyun JEON , Moon Youn JUNG , Seon Hee PARK
发明人： Dong-Ho SHIN , Minsuk JEONG , Kyu Ho SONG , HyeYoon KIM , JuHyun JEON , Moon Youn JUNG , Seon Hee PARK
IPC分类号： G01N35/10 , G01N33/00
CPC分类号： B01L3/50273 , B01L9/527 , B01L2400/0457 , G01N35/08 , Y10T436/11
摘要： Provided are methods of controlling a fluid flow in a microfluidic device and a microfluidic analysis apparatus. According to the method, an inclination of the microfluidic device with respect to a horizontal direction can be adjusted to simply and accurately control a fluid flow in the microfluidic device. Thus, a fluid conveyance can be completely controlled, and an inspection can be performed using only a small amount of sample. In addition, the method of controlling the fluid flow in the microfluidic device can be manually performed by a user. Thus, since a power is not required, the method of controlling the fluid flow in the microfluidic device can be economical and simple. The microfluidic analysis apparatus includes an inclination operation unit for causing an inclination change of a receiving part of the microfluidic device with respect to a horizontal plane and an inclination control part for controlling an operation of the inclination operation unit to simply and accurately control the fluid flow, thereby to accurately analyze the fluid.
摘要翻译：提供了控制微流体装置和微流体分析装置中的流体流动的方法。根据该方法，可以调节微流体装置相对于水平方向的倾斜度以简单且精确地控制微流体装置中的流体流动。因此，可以完全控制流体输送，并且可以仅使用少量的样品进行检查。此外，控制微流体装置中的流体流动的方法可以由用户手动执行。因此，由于不需要动力，所以控制微流体装置中的流体流动的方法可以是经济和简单的。微流体分析装置包括倾斜操作单元，用于使微流体装置的接收部相对于水平面倾斜变化，以及用于控制倾斜操作单元的操作的倾斜控制部，以简单且精确地控制流体流动，从而准确地分析流体。

7. 发明申请

US20060182677A1 Process for preparing fine metal oxide particles 有权
标题翻译：金属氧化物微粒的制备方法
公开(公告)号：US20060182677A1
公开(公告)日：2006-08-17
申请号：US10521642
申请日：2003-07-08
申请人： Wan-Jae Myeong , Jin-Soo Baik , Se-Woong Park , Chnag-Mo Chung , Kyu-Ho Song
发明人： Wan-Jae Myeong , Jin-Soo Baik , Se-Woong Park , Chnag-Mo Chung , Kyu-Ho Song
IPC分类号： C01F17/00
CPC分类号： C01G49/0036 , B82Y30/00 , C01B13/366 , C01F17/0043 , C01G1/02 , C01G9/02 , C01G51/42 , C01P2004/20 , C01P2004/41 , C01P2004/62 , C01P2004/64 , Y02P20/544 , Y10S977/773 , Y10S977/775 , Y10S977/811
摘要： Disclosed is a process for preparing fine metal oxide particles, comprising the following steps of reacting a reactant mixture comprising i) water, ii) at least one water-soluble metal nitrate and iii) ammonia or ammonium salt at 250-700° C. under 180-550 bar for 0.01 sec to 10 min in a reaction zone to synthesize the metal oxide particles, the metal nitrate being contained at an amount of 0.01-20 wt % in the reactant mixture; and separating and recovering the metal oxide particles from the resulting reaction products. According to the present invention, nano-sized metal oxide particles are synthesized, while the harmful by-products generated concurrently therewith are effectively decomposed in the same reactor.
摘要翻译：公开了一种制备金属氧化物微粒的方法，包括以下步骤：使反应物混合物反应，所述反应物混合物包含i）水，ii）至少一种水溶性金属硝酸盐和iii）氨或铵盐，在250-700℃下 180-550巴在反应区中0.01秒至10分钟以合成金属氧化物颗粒，在反应混合物中含有0.01-20重量％的金属硝酸盐; 并从所得反应产物中分离和回收金属氧化物颗粒。根据本发明，合成纳米尺寸金属氧化物颗粒，同时产生的有害副产物在同一反应器中有效分解。

8. 发明授权

US09121850B2 Cartridge for detecting target antigen and method for detecting target antigen using the same 有权
标题翻译：用于检测靶抗原的盒和使用该抗原检测靶抗原的方法
公开(公告)号：US09121850B2
公开(公告)日：2015-09-01
申请号：US13350132
申请日：2012-01-13
申请人： Da Yeon Kang , Sun Kil Kang , Tae Young Kim , Seung Mok Han , Kyu Ho Song , Guei Sam Lim , Ji Su Kim
发明人： Da Yeon Kang , Sun Kil Kang , Tae Young Kim , Seung Mok Han , Kyu Ho Song , Guei Sam Lim , Ji Su Kim
IPC分类号： G01N33/566 , G01N33/543 , G01N21/64 , G01N21/65
CPC分类号： G01N33/54366 , G01N21/6428 , G01N21/65 , G01N2458/10 , Y02A50/59
摘要： There are provided a cartridge for detecting a target antigen and a method for detecting a target antigen existing in a biological sample using the cartridge. In the cartridge, multiple detections of various antigens can be rapidly and conveniently performed, and a plurality of target antigens can be quantitatively analyzed using one cartridge, thereby reducing time and cost.
摘要翻译：提供了一种用于检测靶抗原的盒，以及使用该盒检测存在于生物样品中的靶抗原的方法。在盒中，可以快速方便地进行各种抗原的多次检测，并且可以使用一个盒定量分析多个靶抗原，从而减少时间和成本。

9. 发明申请

US20140131617A1 Single-Phase Lithium-Deficient Lithium Multicomponent Transition Metal Oxide Having a Layered Crystal Structure and a Method for Producing the Same 审中-公开
标题翻译：具有层状晶体结构的单相锂缺乏锂多组分转变金属氧化物及其制造方法
公开(公告)号：US20140131617A1
公开(公告)日：2014-05-15
申请号：US14130573
申请日：2012-07-09
申请人： Sei Ung Park , Ju Suk Ryu , Kyu Ho Song , Si Jin Oh , Dong Suek Lee , Seong Jae Lim , Ki Taeg Jung , Kyoo Seung Han
发明人： Sei Ung Park , Ju Suk Ryu , Kyu Ho Song , Si Jin Oh , Dong Suek Lee , Seong Jae Lim , Ki Taeg Jung , Kyoo Seung Han
IPC分类号： H01M4/505 , H01G11/50 , H01M4/525
CPC分类号： H01G11/50 , C01G53/42 , C01G53/50 , C01P2002/72 , H01M4/505 , H01M4/525 , H01M10/052 , Y02P20/544
摘要： The present invention relates to a single-phase lithium-deficient lithium multicomponent transition metal oxide having a layered crystal structure represented by the formula Li1-aM11-x-y-zM2xM3yM4zO2, wherein M1 is one or more transition metals having an oxidation number of +3; M2 is one or more transition metals having an oxidation number of +4; M3 is one or more transition metals having an oxidation number of +5; M4 is one or more elements having an oxidation number of +2; x+2y−z>0; x+y+z
摘要翻译：本发明涉及具有由式Li1-aM11-x-y-zM2xM3yM4zO2表示的层状结晶结构的单相锂缺乏型锂多组分过渡金属氧化物，其中M1是氧化数为+3的一种或多种过渡金属; M2是氧化数为+4的一种或多种过渡金属; M3是氧化数为+5的一种或多种过渡金属; M4是氧化数为+2的一种或多种元素; x + 2y-z> 0; x + y + z <1; 0

10. 发明申请

US20100227222A1 Lithium-Metal Composite Oxides and Electrochemical Device Using the Same 有权
标题翻译：锂金属复合氧化物及其使用的电化学装置
公开(公告)号：US20100227222A1
公开(公告)日：2010-09-09
申请号：US12224031
申请日：2007-02-16
申请人： Sung-Kyun Chang , Eui-Yong Bang , Min-Chul Jang , Sang-Hoon Choy , Ki-Young Lee , Saebomi Park , Wan-Jae Myeong , Kyu-Ho Song , Joo-Hyeong Lee , Young-Sik Hahn , Myung-Ho Cho
发明人： Sung-Kyun Chang , Eui-Yong Bang , Min-Chul Jang , Sang-Hoon Choy , Ki-Young Lee , Saebomi Park , Wan-Jae Myeong , Kyu-Ho Song , Joo-Hyeong Lee , Young-Sik Hahn , Myung-Ho Cho
IPC分类号： H01M4/485 , H01F1/00 , B32B5/00
CPC分类号： C01D15/00 , C01G51/42 , C01G51/50 , C01G53/42 , C01G53/50 , C01P2002/74 , C01P2002/86 , C01P2004/03 , C01P2004/32 , C01P2004/61 , C01P2006/11 , C01P2006/12 , C01P2006/40 , C01P2006/42 , H01M4/131 , H01M4/485 , H01M4/505 , H01M4/525 , H01M10/052 , Y02T10/7011 , Y10T428/2982
摘要： Disclosed is a lithium-containing metal composite oxide comprising paramagnetic and diamagnetic metals, which satisfies any one of the following conditions: (a) the ratio of intensity between a main peak of 0±10 ppm (Io PPm) and a main peak of 240±140 ppm (I240 pPm), Uoppm/124o PPm), is less than 0.117·Z wherein Z is the ratio of moles of the diamagnetic metal to moles of lithium; (b) the ratio of line width between the main peak of 0±10 ppm (Io PPm) and the main peak of 240+140 ppm (I24o PPm), (W24o PPm/WO ppm), is less than 21.45; and (c) both the conditions (a) and (b), the peaks being obtained according to the 7Li—NMR measurement conditions and means disclosed herein. Also, an electrode comprising the lithium-containing metal composite oxide, and an electrochemical device comprising the electrode are disclosed. The lithium-containing multicomponent metal composite oxide shows crystal stability and excellent physical properties as a result of an improved ordering structure of metals, in which the components of the composite oxide are uniformly distributed. Thus, it can provide a battery having high capacity characteristics, long cycle life characteristics and improved rate characteristics.
摘要翻译：公开了包含顺磁性和抗磁性金属的含锂金属复合氧化物，其满足以下条件中的任一个：（a）主峰为0±10ppm（Io PPm）与主峰为240的强度之比 ±140ppm（I240pPm），Uoppm / 124o PPm）小于0.117·Z其中Z是反磁性金属与摩尔数的摩尔比; （b）0±10ppm（Io PPm）的主峰与240 + 140ppm的主峰（I24o PPm）之间的线宽比（W24o PPm / WOppm）小于21.45; 和（c）条件（a）和（b），根据本文公开的7Li-NMR测量条件和手段获得峰。另外，公开了包含该含锂金属复合氧化物的电极和包含电极的电化学装置。含锂多组分金属复合氧化物由于复合氧化物的组分均匀分布的金属的排序结构改善而显示出晶体稳定性和优异的物理性能。因此，可以提供具有高容量特性，长循环寿命特性和改善的速率特性的电池。

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