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1. 发明授权

US08568886B2 Fluorine-containing copolymer, paper processing agent, and coating film-forming agent for cosmetic preparation 有权
标题翻译：含氟共聚物，纸张加工剂和化妆品制备用涂膜成膜剂
公开(公告)号：US08568886B2
公开(公告)日：2013-10-29
申请号：US12935554
申请日：2009-03-27
申请人： Michio Matsuda , Tetsuya Uehara , Mitsuhiro Usugaya , Ikuo Yamamoto , Takashi Enomoto , Kayo Kusumi
发明人： Michio Matsuda , Tetsuya Uehara , Mitsuhiro Usugaya , Ikuo Yamamoto , Takashi Enomoto , Kayo Kusumi
IPC分类号： B32B27/10
CPC分类号： D21H17/20 , A61K8/8152 , A61Q3/02 , A61Q5/06 , A61Q19/00 , B29C33/62 , C08F220/24 , C08F222/1006 , C09D133/16 , D21H19/20 , Y10T428/3154 , C08F220/26
摘要： Disclosed is a fluorine-containing copolymer having sufficient stability in water, which is capable of providing paper with sufficient oil resistance. The fluorine-containing polymer contains, as essential components, (a) a fluorine-containing monomer represented by general formula (I) CH2═C(—X)—C(═O)—Y—[—(CH2)m—Z—]p—(CH2)n—Rf (wherein X represents a hydrogen atom; Y represents —O— or —NH—; Z represents a direct bond, —S— or —SO2—; Rf represents a fluoroalkyl group having 1-6 carbon atoms; m is a number of 1-10; n is a number of 0-10; and p is 0 or 1) and (b) an alkoxy group-containing monomer represented by general formula (II) CH2═C(X′)—C(═O)—O—(RO)q—H (wherein X′ represents a hydrogen atom or a methyl group; R represents an alkylene group having 2-4 carbon atoms wherein a part or all of hydrogen atoms may be substituted by a hydroxyl group; and q represent an integer of 1-50). The fluorine-containing polymer does not contain a monomer having an amino group.
摘要翻译：公开了一种在水中具有足够稳定性的含氟共聚物，其能够为纸提供足够的耐油性。含氟聚合物含有（a）由通式（I）表示的含氟单体CH 2 = C（-X）-C（= O）-Y - [ - （CH 2）m Z-）对 - （CH 2）n -R f（其中X表示氢原子; Y表示-O-或-NH-; Z表示直接键，-S-或-SO 2 - ; Rf表示具有1-6个碳原子的氟代烷基原子; m是1-10的数; n是0-10的数; p是0或1）和（b）由通式（II）表示的含烷氧基的单体CH 2 = C（X' ）-C（= O）-O-（RO）qH（其中X'表示氢原子或甲基; R表示具有2-4个碳原子的亚烷基，其中部分或全部氢原子可以被羟基; q表示1-50的整数）。含氟聚合物不含有具有氨基的单体。

2. 发明申请

US20120171495A1 WATER AND OIL RESISTANT AGENT FOR PAPER, TREATMENT PROCESS AND PAPER 有权
标题翻译：用于纸张，处理过程和纸张的耐水和耐油剂
公开(公告)号：US20120171495A1
公开(公告)日：2012-07-05
申请号：US13393431
申请日：2010-08-31
申请人： Eiji Masuda , Michio Matsuda , Kayo Kusumi , Tetsuya Uehara
发明人： Eiji Masuda , Michio Matsuda , Kayo Kusumi , Tetsuya Uehara
IPC分类号： C08F220/22 , B32B27/10 , D21H17/37
CPC分类号： D21H21/16 , C08F214/18 , C08F220/06 , C08F220/24 , C08F2220/281 , C08F2220/286 , C09D133/16 , Y10T428/3154
摘要： Disclosed is a water and oil resistant agent comprising a fluorine-containing copolymer obtained by copolymerizing a (meth)acrylate monomer having a polyfluoroalkyl group having 1-6 carbon atoms, hydrophilic monomer, and monomer having an anion-donating group, which agent affords a superior water and oil resistance to a paper. The invention also discloses a process for treating a paper by the water and oil resistant agent and a treated paper thereby.
摘要翻译：公开了一种耐油和耐油剂，其包含通过使具有1-6个碳原子的具有多氟烷基的（甲基）丙烯酸酯单体，亲水性单体和具有阴离子供体基团的单体共聚而得到的含氟共聚物，优异的耐水和耐油性的纸张。本发明还公开了一种由防水防油剂和经处理的纸处理纸的方法。

3. 发明授权

US07758656B2 Water-and-oil repellent treatment of textile 有权
标题翻译：防水和拒油处理纺织品
公开(公告)号：US07758656B2
公开(公告)日：2010-07-20
申请号：US10258067
申请日：2001-04-16
申请人： Takashi Enomoto , Ikuo Yamamoto , Norihito Otsuki , Teruyuki Fukuda , Kayo Kusumi
发明人： Takashi Enomoto , Ikuo Yamamoto , Norihito Otsuki , Teruyuki Fukuda , Kayo Kusumi
IPC分类号： D06M15/00 , B05D7/00
CPC分类号： D06M13/184 , D06M15/277 , D06M2200/11 , D06M2200/12 , Y10T442/2164 , Y10T442/2189 , Y10T442/2197
摘要： A textile having excellent water- and oil-repellency can be obtained by a method of preparing a treated textile, having steps of: (1) preparing a treatment liquid comprising a water- and oil-repellent agent, (2) adjusting pH of the treatment liquid to at most 7, preferably at most 3, (3) applying the treatment liquid to a textile, (4) treating the textile with steam, and (5) washing the textile with water and dehydrating the textile, wherein the water- and oil-repellent agent is at least one fluorine-containing compound selected from the group consisting of a fluorine-containing polymer and a fluorine-containing low molecular weight compound, and the water- and oil-repellent agent or the treatment liquid contains an organic salt.
摘要翻译：通过制备处理过的纺织品的方法可以获得具有优异的拒水拒油性的织物，其具有以下步骤：（1）制备包含拒水拒油剂的处理液，（2）调节（3）将处理液施加到纺织品上，（4）用蒸汽处理织物，和（5）用水洗涤织物并使织物脱水，其中，防油剂为选自含氟聚合物和含氟低分子化合物中的至少一种含氟化合物，防水防油剂或处理液含有有机物盐。

4. 发明申请

US20060091351A1 Fluorinated urethane compounds and compositions containing the same 有权
标题翻译：氟化氨基甲酸酯化合物和含有它们的组合物
公开(公告)号：US20060091351A1
公开(公告)日：2006-05-04
申请号：US10523518
申请日：2003-08-05
申请人： Ikuo Yamamoto , Kayo Kusumi , Takuya Yoshioka , Fumihiko Yamaguchi
发明人： Ikuo Yamamoto , Kayo Kusumi , Takuya Yoshioka , Fumihiko Yamaguchi
IPC分类号： D06M15/263 , C07C271/20
CPC分类号： C07D251/34 , C07C275/14 , C07D251/12 , D06M13/428 , D06M15/576 , D06M2200/11 , D06M2200/12
摘要： A fluorine-containing urethane compound of the general formula: [Rf-A1-(X1(OH))—(Y1)a—OC(═O)NH—]m I [—NHC(═O)O—Y2]n[—NHC(═O)O—((ClCH2—)X2O)b—R1]k (1) wherein I is a group remaining after an isocyanate group is removed from a polyisocyanate compound, Rf is a perfluoroalkyl group having 2 to 21 carbon atoms, A1 is a direct bond or a divalent organic group having 1 to 21 carbon atoms, X1 and X2 are trivalent linear or branched aliphatic group having 2 to 5 carbon atoms, Y1 is a divalent organic group having 0 to 5 carbon atoms and 0 to 2 nitrogen atoms (provided that at least one carbon atom or nitrogen atom is present) and at least one hydrogen atom, Y2 is a monovalent organic group optionally having a hydroxyl group, and R1 is a hydrogen atom or an alkyl group having 1 to 10 carbon atoms, can impart high water- and oil-repellency.
摘要翻译：具有以下通式的含氟氨基甲酸酯化合物：<？in-line-formula description =“In-line formula”end =“lead”？> [Rf-A 1 - （X ^{“end =”tail“？>其中I是在从异氰酸酯化合物除去异氰酸酯基后残留的基团，Rf是具有2至21个碳原子的全氟烷基，A 1是直接键或具有1至21个碳原子的二价有机基团，X 1和X 2是具有2至5个碳原子的三价直链或支链脂族基团，Y 1 是具有0至5个碳原子和0至2个氮原子的二价有机基团（条件是存在至少一个碳原子或氮原子）和至少一个氢原子，Y 2 O >是一价有机g 任选具有羟基的醇，R 1是氢原子或具有1-10个碳原子的烷基，可以赋予高斥水斥油性。}

5. 发明授权

US06740357B2 Water-and oil-repellent treatment of textile 有权
标题翻译：防水和防油处理纺织品
公开(公告)号：US06740357B2
公开(公告)日：2004-05-25
申请号：US10327190
申请日：2002-12-24
申请人： Fumihiko Yamaguchi , Ikuo Yamamoto , Kayo Kusumi
发明人： Fumihiko Yamaguchi , Ikuo Yamamoto , Kayo Kusumi
IPC分类号： B05D310
CPC分类号： D06N3/047 , D06M15/277 , D06M15/564 , D06M15/576 , D06M15/6433 , D06M15/6436 , D06M15/65 , D06M2200/11 , D06M2200/12 , D06N3/007 , D06N3/128 , D06N3/14
摘要： A method of preparing a treated textile, having steps of: (1) preparing a treatment liquid comprising a water- and oil-repellent agent, (2) adjusting pH of the treatment liquid to at most 7, (3) applying the treatment liquid to a textile, (4) treating the textile with steam, and (5) washing the textile with water and dehydrating the textile, wherein the water- and oil-repellent agent contains (A) a fluorine-containing compound which is a fluorine-containing polymer, and (B) a urethane compound and/or (C) a silicon-containing compound, can give a textile which is excellent in water repellency, oil repellency and soil releasability, when the textile is treated with the treatment liquid by an Exhaust process.
摘要翻译：一种制备经处理的织物的方法，具有以下步骤：（1）制备包含拒水拒油剂的处理液，（2）将处理液的pH调节至至多7，（3）施加处理液纺织品，（4）用蒸汽处理织物，（5）用水洗涤织物并使织物脱水，其中防水防油剂含有（A）含氟化合物，（B）氨基甲酸酯化合物和/或（C）含硅化合物可以得到当织物用处理液处理时具有优异的防水性，拒油性和污垢释放性的织物排气过程。

6. 发明授权

US09249540B2 Water and oil resistant agent for paper, treatment process and paper 有权
标题翻译：纸和纸的防水和防油剂
公开(公告)号：US09249540B2
公开(公告)日：2016-02-02
申请号：US13393431
申请日：2010-08-31
申请人： Eiji Masuda , Michio Matsuda , Kayo Kusumi , Tetsuya Uehara
发明人： Eiji Masuda , Michio Matsuda , Kayo Kusumi , Tetsuya Uehara
IPC分类号： D21H21/16 , C09D133/16 , C08F220/24 , C08F214/18 , C08F220/06 , C08F220/28
CPC分类号： D21H21/16 , C08F214/18 , C08F220/06 , C08F220/24 , C08F2220/281 , C08F2220/286 , C09D133/16 , Y10T428/3154
摘要： Disclosed is a water and oil resistant agent comprising a fluorine-containing copolymer obtained by copolymerizing a (meth)acrylate monomer having a polyfluoroalkyl group having 1-6 carbon atoms, hydrophilic monomer, and monomer having an anion-donating group, which agent affords a superior water and oil resistance to a paper. The invention also discloses a process for treating a paper by the water and oil resistant agent and a treated paper thereby.
摘要翻译：公开了一种耐油和耐油剂，其包含通过使具有1-6个碳原子的具有多氟烷基的（甲基）丙烯酸酯单体，亲水性单体和具有阴离子供体基团的单体共聚而得到的含氟共聚物，优异的耐水和耐油性的纸张。本发明还公开了一种由防水防油剂和经处理的纸处理纸的方法。

7. 发明申请

US20120285645A1 WATER- AND OIL-RESISTANT AGENT HAVING A DECREASED CONTENT OF VINYL PYRROLIDONE MONOMER 审中-公开
标题翻译：具有乙烯基吡咯烷酮单体的减少含量的耐油和耐油剂
公开(公告)号：US20120285645A1
公开(公告)日：2012-11-15
申请号：US13432801
申请日：2012-03-28
申请人： Kayo KUSUMI , Eiji MASUDA
发明人： Kayo KUSUMI , Eiji MASUDA
IPC分类号： C08F220/22 , C08K3/30 , C09D133/14 , D21H21/00 , C08L33/14 , C08K3/16 , C08K5/07
CPC分类号： D21H17/11 , C08F218/18 , C08F220/22 , D21H19/10 , D21H19/36 , D21H21/16
摘要： A water- and oil-resistant agent obtained by mixing a fluorine-containing copolymer obtained by copolymerizing (a) a (meth)acrylate monomer (a) having a polyfluoroalkyl group having 1 to 6 carbon atoms, (b) a vinylpyrrolidone monomer, (c) a monomer having an anion-donating group, and (d) a fluorine-free (meth)acrylate monomer with a liquid medium and an acid under heating, can have a decreased residual amount of unreacted vinylpyrrolidone monomer of at most 10 ppm and can afford a superior water- and oil-resistance to a paper. The invention also discloses a method of producing the water- and oil-resistant agent, a paper treatment composition comprising the water- and oil-resistant agent, a method for treating a paper with the treatment composition, and a paper treated with the water- and oil-resistant agent.
摘要翻译：通过将（a）具有碳原子数1〜6的多氟烷基的（甲基）丙烯酸酯单体（a），（b）乙烯基吡咯烷酮单体，（甲基）丙烯酸酯单体 c）具有阴离子供体基团的单体和（d）具有液体介质和加热酸的无氟（甲基）丙烯酸酯单体可以具有至少10ppm的残留量的未反应的乙烯基吡咯烷酮单体的残留量，以及可以为纸张提供卓越的耐水和耐油性。本发明还公开了一种生产防水和防油剂的方法，一种包含防水和防油剂的纸张处理组合物，用该处理组合物处理纸张的方法，以及用水 - 和耐油剂。

8. 发明授权

US07678155B2 Water- and oil-repellent treatment of textile 有权
标题翻译：防水和拒油处理纺织品
公开(公告)号：US07678155B2
公开(公告)日：2010-03-16
申请号：US10408777
申请日：2003-04-08
申请人： Ikuo Yamamoto , Kayo Kusumi , Mitsuhiro Usugaya , Ryosuke Hara , Takahito Kanbara
发明人： Ikuo Yamamoto , Kayo Kusumi , Mitsuhiro Usugaya , Ryosuke Hara , Takahito Kanbara
IPC分类号： D06M11/07 , D06M11/58 , D06M13/53
CPC分类号： D06M15/277 , D06M11/05 , D06M13/46 , D06M15/41 , D06M2200/11 , D06M2200/12 , Y10T428/23986 , Y10T428/2933 , Y10T442/2172 , Y10T442/2189 , Y10T442/227
摘要： Excellent water- and oil-repellency and soil releasability can be obtained by a method of preparing a treated textile, having steps of: (1) preparing a treatment liquid containing a water- and oil-repellent agent and a stain blocking agent, (2) adjusting pH of the treatment liquid to at most 7, (3) applying the treatment liquid to a textile, (4) treating the textile with steam, and (5) washing the textile with water and dehydrating the textile, wherein the water- and oil-repellent agent contains at least one fluorine-containing compound selected from the group consisting of a fluorine-containing polymer and a fluorine-containing low molecular weight compound, and the water- and oil-repellent agent or the treatment liquid contains a cationic emulsifying agent.
摘要翻译：通过制备经处理的织物的方法可以获得优异的拒水拒油性和污垢释放性，其具有以下步骤：（1）制备含有拒水拒油剂和防污剂的处理液（2 ）将处理液的pH调节至最多7，（3）将处理液施加到纺织品上，（4）用蒸汽处理织物，（5）用水洗涤织物并使织物脱水，防油剂含有选自含氟聚合物和含氟低分子化合物中的至少一种含氟化合物，防水防油剂或处理液含有阳离子性乳化剂。

9. 发明授权

US07388104B2 Fluorinated urethane compounds and compositions containing the same 有权
标题翻译：氟化氨基甲酸酯化合物和含有它们的组合物
公开(公告)号：US07388104B2
公开(公告)日：2008-06-17
申请号：US10523518
申请日：2003-08-05
申请人： Ikuo Yamamoto , Kayo Kusumi , Takuya Yoshioka , Fumihiko Yamaguchi
发明人： Ikuo Yamamoto , Kayo Kusumi , Takuya Yoshioka , Fumihiko Yamaguchi
IPC分类号： C07C271/00 , D06M15/19
CPC分类号： C07D251/34 , C07C275/14 , C07D251/12 , D06M13/428 , D06M15/576 , D06M2200/11 , D06M2200/12
摘要： A fluorine-containing urethane compound of the general formula: [Rf-A1-(X1(OH))—(Y1)a—OC(═O)NH—]mI[—NHC(═O)O—Y2]n[—NHC(═O)O—((ClCH2—)X2O)b—R1]k (1) wherein I is a group remaining after an isocyanate group is removed from a polyisocyanate compound, Rf is a perfluoroalkyl group having 2 to 21 carbon atoms, A1 is a direct bond or a divalent organic group having 1 to 21 carbon atoms, X1 and X2 are trivalent linear or branched aliphatic group having 2 to 5 carbon atoms, Y1 is a divalent organic group having 0 to 5 carbon atoms and 0 to 2 nitrogen atoms (provided that at least one carbon atom or nitrogen atom is present) and at least one hydrogen atom, Y2 is a monovalent organic group optionally having a hydroxyl group, and R1 is a hydrogen atom or an alkyl group having 1 to 10 carbon atoms, can impart high water- and oil-repellency.
摘要翻译：具有以下通式的含氟氨基甲酸酯化合物：<？in-line-formula description =“In-line formula”end =“lead”？> [Rf-A 1 - （X ^{“end =”tail“？>其中I是在从异氰酸酯化合物除去异氰酸酯基后残留的基团，Rf是具有2至21个碳原子的全氟烷基，A 1是直接键或具有1至21个碳原子的二价有机基团，X 1和X 2是具有2至5个碳原子的三价直链或支链脂族基团，Y 1 是具有0至5个碳原子和0至2个氮原子的二价有机基团（条件是存在至少一个碳原子或氮原子）和至少一个氢原子，Y 2 O >是一种单价有机基团o 具有羟基，R 1是氢原子或具有1-10个碳原子的烷基，可以赋予高斥水斥油性。}

10. 发明授权

US09540470B2 Copolymer, treatment agent for paper, and treated paper 有权
标题翻译：共聚物，纸张处理剂和处理纸
公开(公告)号：US09540470B2
公开(公告)日：2017-01-10
申请号：US13390758
申请日：2010-08-17
申请人： Michio Matsuda , Tetsuya Uehara , Norimasa Uesugi , Ikuo Yamamoto , Kayo Kusumi
发明人： Michio Matsuda , Tetsuya Uehara , Norimasa Uesugi , Ikuo Yamamoto , Kayo Kusumi
IPC分类号： C08F220/34 , C08F226/10 , D21H17/42 , D21H17/37 , D21H17/54 , C08F220/24 , C08K5/55 , D21H21/16 , C08F220/06 , C08F226/06
CPC分类号： C08F220/34 , C08F220/06 , C08F220/24 , C08F226/06 , C08F226/10 , C08K5/55 , D21H17/37 , D21H17/375 , D21H17/42 , D21H17/54 , D21H21/16 , C08L33/16
摘要： Disclosed is a treatment agent for paper comprising a fluorine-containing copolymer having a repeat unit (a) derived from a fluorine-containing monomer represented by general formula (I): CH2═C(—X)—C(═O)—Y—[—CH2)m—Z—]p—(CH2)n—Rf; a repeat unit (b) derived from at least one amino monomer represented by general formula (II-1): or a derivative thereof; and a repeat unit (c) derived from a pyrrolidone monomer represented by general formula (III): The treatment agent for paper provides paper having high oil resistance and high water resistance.
摘要翻译：公开了一种包含含有由通式（1）表示的含氟单体衍生的重复单元（a）的含氟共聚物的纸的处理剂：CH 2 = C（-X）-C（= O） - Y - [ - （CH 2）m -Z-] p - （CH 2）n -Rf; 衍生自由通式（11-1）表示的至少一个氨基单体的重复单元（b）：其衍生物; 和由通式（111）表示的吡咯烷酮单体衍生的重复单元（c）。纸的处理剂提供具有高耐油性和高耐水性的纸。

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