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1. 发明授权

US09321037B2 Hydroprocessing co-catalyst compositions and methods of introduction thereof into hydroprocessing units 有权
标题翻译：加氢处理助催化剂组合物及其引入加氢处理装置的方法
公开(公告)号：US09321037B2
公开(公告)日：2016-04-26
申请号：US13715918
申请日：2012-12-14
申请人： Julie Chabot , Bo Kou , Alexander Kuperman
发明人： Julie Chabot , Bo Kou , Alexander Kuperman
IPC分类号： B01J8/20 , B01J23/78 , B01J23/28 , B01J23/30 , B01J23/75 , B01J23/755 , B01J35/00 , B01J23/85 , B01J31/02 , B01J35/02 , B01J37/00 , B01J31/04 , B01J31/06 , C10G45/08 , C10G45/16 , B01J37/04 , B01J21/02 , B01J21/06 , B01J21/10 , B01J21/12
CPC分类号： B01J23/78 , B01J21/02 , B01J21/06 , B01J21/10 , B01J21/12 , B01J23/28 , B01J23/30 , B01J23/75 , B01J23/755 , B01J23/85 , B01J31/0247 , B01J31/04 , B01J31/06 , B01J35/0006 , B01J35/023 , B01J37/0036 , B01J37/04 , C10G45/08 , C10G45/16 , C10G2300/1033 , C10G2300/202
摘要： A hydroprocessing co-catalyst composition may comprise in an embodiment a first component comprising co-catalyst particles and a liquid carrier, and a second component comprising a dispersant and a dispersant diluent. The co-catalyst particles may be in the micron size range, and the dispersant may promote dispersion of the co-catalyst particles in materials such as the liquid carrier, the dispersant diluent, and combinations thereof. Methods of introducing a hydroprocessing co-catalyst composition into a hydroprocessing system are also disclosed.
摘要翻译：加氢处理助催化剂组合物可以在一个实施方案中包括包含助催化剂颗粒和液体载体的第一组分，和包含分散剂和分散剂稀释剂的第二组分。助催化剂颗粒可以在微米尺寸范围内，并且分散剂可以促进助催化剂颗粒在诸如液体载体，分散剂稀释剂及其组合的材料中的分散。还公开了将加氢助催化剂组合物引入加氢处理系统的方法。

2. 发明授权

US08846560B2 Hydroprocessing catalysts and methods for making thereof 有权
标题翻译：加氢处理催化剂及其制备方法
公开(公告)号：US08846560B2
公开(公告)日：2014-09-30
申请号：US13331274
申请日：2011-12-20
申请人： Shuwu Yang , Bruce Edward Reynolds , Julie Chabot , Bo Kou
发明人： Shuwu Yang , Bruce Edward Reynolds , Julie Chabot , Bo Kou
IPC分类号： B01J23/00 , B01J23/40 , B01J23/42 , B01J23/44 , B01J23/70 , B01J23/74 , B01J27/02 , B01J27/043 , B01J27/045 , B01J27/24 , B01J31/00 , B01J23/883 , B01J27/051 , B01J23/85 , B01J37/20 , B01J23/887 , C10G49/04 , B01J23/24 , B01J35/00 , B01J35/10
CPC分类号： B01J23/883 , B01J23/24 , B01J23/85 , B01J23/8872 , B01J23/8873 , B01J27/051 , B01J27/0515 , B01J35/0073 , B01J35/1019 , B01J35/1023 , B01J35/1042 , B01J35/1047 , B01J35/1095 , B01J37/20 , C10G49/04 , C10G49/06 , C10G49/12 , C10G2300/107 , C10G2300/1077 , C10G2300/205 , C10G2300/301 , C10G2300/701 , C10G2300/703 , C10G2300/802
摘要： A process for preparing a slurry catalyst is provided. The slurry catalyst is prepared from at least a Group VIB metal precursor and optionally at least a Promoter metal precursor selected from Group VIII, Group IIB, Group IIA, Group IVA metals and combinations thereof. The slurry catalyst comprises a plurality of dispersed particles in a hydrocarbon medium having an average particle size ranging from 1 to 300 μm. The slurry catalyst is then mixed with a hydrogen feed at a pressure from 1435 psig (10 MPa) to 3610 psig (25 MPa) and a temperature from 200-800° F. at 500 to 15,000 scf hydrogen per bbl of slurry catalyst for a minute to 20 hours, for the slurry catalyst to be saturated with hydrogen providing an increase of k-values in terms of HDS, HDN, and HDMCR of at least 15% compared to a slurry catalyst that is not saturated with hydrogen.
摘要翻译：提供了一种制备浆料催化剂的方法。浆料催化剂由至少VIB族金属前体和任选的至少一种选自VIII族，IIB族，IIA族，IVA族金属及其组合的促进剂金属前体制备。浆料催化剂在平均粒度为1〜300μm的烃介质中含有多个分散粒子。然后将浆料催化剂与氢气进料混合，压力为1435psig（10MPa）至3610psig（25MPa），温度为200-800°F，每桶浆料催化剂为500至15,000scf氢气分钟至20小时，浆液催化剂用氢饱和，与不饱和氢气的浆料催化剂相比，HDS，HDN和HDMCR的k值提高至少15％。

3. 发明授权

US08809223B2 Hydroprocessing catalysts and methods for making thereof 有权
标题翻译：加氢处理催化剂及其制备方法
公开(公告)号：US08809223B2
公开(公告)日：2014-08-19
申请号：US13331660
申请日：2011-12-20
申请人： Joseph V. Nguyen , Julie Chabot , Oleg Mironov
发明人： Joseph V. Nguyen , Julie Chabot , Oleg Mironov
IPC分类号： B01J27/02 , B01J27/043 , B01J27/045 , B01J23/00 , B01J23/40 , B01J23/42 , B01J23/58 , B01J23/70 , B01J23/74 , B01J23/44 , B01J23/02 , B01J23/06 , B01J23/883 , B01J23/85 , B01J27/051 , C10G49/04 , B01J35/00 , B01J37/20 , B01J23/24 , B01J23/887 , B01J35/10
CPC分类号： B01J23/883 , B01J23/24 , B01J23/85 , B01J23/8872 , B01J23/8873 , B01J27/051 , B01J27/0515 , B01J35/0073 , B01J35/1019 , B01J35/1023 , B01J35/1042 , B01J35/1047 , B01J35/1095 , B01J37/20 , C10G49/04 , C10G49/06 , C10G49/12 , C10G2300/107 , C10G2300/1077 , C10G2300/205 , C10G2300/301 , C10G2300/701 , C10G2300/703 , C10G2300/802
摘要： A process for preparing an improved slurry catalyst for the upgrade of heavy oil feedstock is provided. The process comprises providing at least a metal precursor in solution comprising at least two different metal cations in its molecular structure, with at least one of the metal cations is a Group VIB metal cation; sulfiding the metal precursor with a sulfiding agent in solution forming a catalyst precursor; and mixing the catalyst precursor with a hydrocarbon diluent to form the slurry catalyst. In one embodiment, the at least a metal precursor comprising at least two different metal cations is prepared by combining and reacting at least one Group VIB metal compound with at least a Promoter metal compound selected from Group VIII, Group IIB, Group IIA, Group IVA metals and combinations thereof.
摘要翻译：提供了一种制备用于提高重油原料的改进的浆料催化剂的方法。该方法包括在其分子结构中提供包含至少两种不同金属阳离子的溶液中的至少一种金属前体，至少一种金属阳离子是VIB族金属阳离子; 在形成催化剂前体的溶液中用硫化剂硫化金属前体; 并将催化剂前体与烃稀释剂混合以形成浆料催化剂。在一个实施方案中，至少包含至少两种不同金属阳离子的金属前体通过将至少一种VIB族金属化合物与至少一种选自第VIII族，IIB族，IIA族，IVA族的促进剂金属化合物金属及其组合。

4. 发明申请

US20140171299A1 HYDROPROCESSING CO-CATALYST COMPOSITIONS AND METHODS OF INTRODUCTION THEREOF INTO HYDROPROCESSING UNITS 有权
标题翻译：氢化催化剂组合物及其引入方法进入水解单位
公开(公告)号：US20140171299A1
公开(公告)日：2014-06-19
申请号：US13715943
申请日：2012-12-14
申请人： Julie Chabot , Bo Kou , Alexander Kuperman
发明人： Julie Chabot , Bo Kou , Alexander Kuperman
IPC分类号： B01J23/78 , B01J23/75 , B01J23/755 , B01J23/28 , B01J23/30
CPC分类号： B01J23/78 , B01J21/02 , B01J21/06 , B01J21/10 , B01J21/12 , B01J23/28 , B01J23/30 , B01J23/75 , B01J23/755 , B01J23/85 , B01J31/0205 , B01J31/0247 , B01J35/0006 , B01J35/023 , B01J37/0036 , B01J37/04 , C10G47/26 , C10G49/02 , C10G49/12
摘要： A hydroprocessing co-catalyst composition may comprise in an embodiment a first component comprising co-catalyst particles and a liquid carrier, and a second component comprising a dispersant and a dispersant diluent. The co-catalyst particles may be in the micron size range, and the dispersant may promote dispersion of the co-catalyst particles in materials such as the liquid carrier, the dispersant diluent, and combinations thereof. Methods of introducing a hydroprocessing co-catalyst composition into a hydroprocessing system are also disclosed.
摘要翻译：加氢处理助催化剂组合物可以在一个实施方案中包括包含助催化剂颗粒和液体载体的第一组分，和包含分散剂和分散剂稀释剂的第二组分。助催化剂颗粒可以在微米尺寸范围内，并且分散剂可以促进助催化剂颗粒在诸如液体载体，分散剂稀释剂及其组合的材料中的分散。还公开了将加氢助催化剂组合物引入加氢处理系统的方法。

5. 发明申请

US20140166541A1 HYDROPROCESSING CO-CATALYST COMPOSITIONS AND METHODS OF INTRODUCTION THEREOF INTO HYDROPROCESSING UNITS 审中-公开
公开(公告)号：US20140166541A1
公开(公告)日：2014-06-19
申请号：US13715959
申请日：2012-12-14
申请人： Julie Chabot , Bo Kou , Alexander Kuperman
发明人： Julie Chabot , Bo Kou , Alexander Kuperman
IPC分类号： C10G45/04
CPC分类号： C10G45/04 , C10G45/16
摘要： A hydroprocessing co-catalyst composition may comprise in an embodiment a first component comprising co-catalyst particles and a liquid carrier, and a second component comprising a dispersant and a dispersant diluent. The co-catalyst particles may be in the micron size range, and the dispersant may promote dispersion of the co-catalyst particles in materials such as the liquid carrier, the dispersant diluent, and combinations thereof. Methods of introducing a hydroprocessing co-catalyst composition into a hydroprocessing system are also disclosed.

6. 发明授权

US07897035B2 Systems and methods for producing a crude product 有权
标题翻译：用于生产粗产品的系统和方法
公开(公告)号：US07897035B2
公开(公告)日：2011-03-01
申请号：US12212796
申请日：2008-09-18
申请人： Julie Chabot
发明人： Julie Chabot
IPC分类号： C10G45/00
CPC分类号： C10G65/10 , C10G47/26 , C10G65/12
摘要： Systems and methods for hydroprocessing a heavy oil feedstock, the system employs a plurality of contacting zones and separation zones with at least some of the heavy oil feedstock being supplied to at least a contacting zone other than the first contacting zone. The contacting zones operate under hydrocracking conditions, employing a slurry catalyst for upgrading the heavy oil feedstock, forming upgraded products of lower boiling boiling hydrocarbons. In the separation zones, upgraded products are removed overhead and optionally, further treated in an in-line hydrotreater. At least a portion of the non-volatile fractions recovered from at least one of the separation zones is recycled back to the first contacting zone in the system.
摘要翻译：用于加氢处理重油原料的系统和方法，所述系统采用多个接触区域和分离区域，其中至少一些重油原料供应至少于除第一接触区域之外的接触区域。接触区在加氢裂化条件下运行，使用用于升级重油原料的浆料催化剂，形成较低沸点沸点烃的升级产物。在分离区中，升级产物在顶部除去，任选地，在直列加氢处理机中进一步处理。从至少一个分离区回收的至少一部分非挥发性馏分被循环回系统中的第一接触区。

7. 发明授权

US06387334B1 Balanced flow resistance OCR distributor cone 失效
标题翻译：平衡流阻OCR分配锥
公开(公告)号：US06387334B1
公开(公告)日：2002-05-14
申请号：US09216268
申请日：1998-12-18
申请人： William B. Krantz , David E. Earls , Harold J. Trimble , Julie Chabot , Krishniah Parimi
发明人： William B. Krantz , David E. Earls , Harold J. Trimble , Julie Chabot , Krishniah Parimi
IPC分类号： B01J808
CPC分类号： B01J8/003 , B01J8/008 , B01J8/0085 , B01J8/06 , B01J8/44 , B01J2208/00752 , B01J2208/00884 , B01J2208/024
摘要： The invention comprises an OCR catalyst reactor which includes passive spheres and catalyst particles having substantially the same size and separated on opposite sides of a distributor cone by a screen. The use of passive spheres of substantially the same size to the catalyst particles provides for a more uniform distribution of the gas liquid reactants charged into the reactor vessel. The screen is configured such that it provides a separation of the catalyst and the passive spheres while being sized to prevent plugging.
摘要翻译：本发明包括一种OCR催化剂反应器，其包括无源球体和具有基本相同尺寸的催化剂颗粒，并通过筛网在分配器锥体的相对侧上分离。使用与催化剂颗粒基本上相同尺寸的被动球提供了装入反应器容器中的气体液体反应物更均匀的分布。屏幕被配置为使得其提供催化剂和被动球的分离，同时确定尺寸以防止堵塞。

8. 发明授权

US09206361B2 Hydroprocessing catalysts and methods for making thereof 有权
标题翻译：加氢处理催化剂及其制备方法
公开(公告)号：US09206361B2
公开(公告)日：2015-12-08
申请号：US13330910
申请日：2011-12-20
申请人： Julie Chabot , Bruce E. Reynolds , Erin Maris , Shuwu Yang
发明人： Julie Chabot , Bruce E. Reynolds , Erin Maris , Shuwu Yang
IPC分类号： C10G47/26 , C10G49/02 , B01J37/20 , B01J35/00 , B01J23/883 , B01J35/02 , B01J35/10 , B01J37/00 , B01J37/02 , C10G49/12
CPC分类号： C10G49/02 , B01J23/883 , B01J35/0006 , B01J35/023 , B01J35/1019 , B01J35/1023 , B01J35/1042 , B01J35/1047 , B01J35/1052 , B01J35/1066 , B01J35/1076 , B01J37/0036 , B01J37/0201 , B01J37/20 , C10G49/12 , C10G2300/208 , C10G2300/4056 , C10G2300/70 , C10G2300/708 , C10G2300/802
摘要： A method to upgrade heavy oil feedstock using an ebullated bed reactor and a novel catalyst system is provided. The ebullated bed reactor system includes two different catalyst with different characteristics: an expanded catalyst zone containing particulate catalyst having a particle size of greater than 0.65 mm; and a slurry catalyst having an average particle size ranging from 1 to 300 μm. The slurry catalyst is provided to the ebullated bed system containing the heavy oil feedstock, and entrained in the upflowing hydrocarbon liquid passing through the ebullated bed reaction zone. The slurry catalyst reduces the formation of sediment and coke precursors in the ebullating bed reactor system. The slurry catalyst is prepared from rework materials, which form a slurry catalyst in-situ upon mixing with the heavy oil feedstock.
摘要翻译：提供了一种使用沸腾床反应器和新型催化剂体系升级重油原料的方法。沸腾床反应器系统包括具有不同特性的两种不同的催化剂：包含粒度大于0.65mm的颗粒催化剂的膨胀催化剂区; 和平均粒度为1〜300μm的浆料催化剂。将浆料催化剂提供给含有重油原料的沸腾床系统，并夹带在通过沸腾床反应区的向上流动的烃液中。浆料催化剂减少沸腾床反应器系统中沉淀物和焦炭前体的形成。浆料催化剂由返工材料制备，其在与重油原料混合时原位形成浆料催化剂。

9. 发明授权

US09068132B2 Hydroprocessing catalysts and methods for making thereof 有权
标题翻译：加氢处理催化剂及其制备方法
公开(公告)号：US09068132B2
公开(公告)日：2015-06-30
申请号：US13233477
申请日：2011-09-15
申请人： Shuwu Yang , Julie Chabot , Bruce Edward Reynolds , Bo Kou
发明人： Shuwu Yang , Julie Chabot , Bruce Edward Reynolds , Bo Kou
IPC分类号： C10G47/26 , C10G47/32 , C10G47/36 , C10G65/00 , C10G65/10 , C10G65/18 , C10G47/00 , C10G47/02
CPC分类号： C10G47/02 , C10G47/26 , C10G47/32 , C10G47/36 , C10G65/00 , C10G65/10 , C10G65/18 , C10G2300/205 , C10G2300/4075 , C10G2300/701 , C10G2300/802
摘要： A method to reduce metal deposit in the hydroprocessing or upgrade of heavy oil feedstock is provided. The method comprises feeding an improved catalyst feed to the system, with the improved catalyst feed comprising a fresh slurry catalyst and a deoiled spent catalyst, with the deoiled spent catalyst being present in an amount of at least 10% the catalyst feed for the heavy oil upgrade system to have at least a 5% reduction in metal contaminant build-up compared to heavy oil upgrade system without the deoiled spent catalyst in the feed.
摘要翻译：提供了一种在重油原料的加氢处理或升级中减少金属沉积的方法。该方法包括将改进的催化剂进料进料给系统，改进的催化剂进料包含新鲜的浆料催化剂和脱油的废催化剂，脱油的废催化剂的存在量为重油的催化剂进料的至少10％升级系统与重油升级系统相比，金属污染物累积量减少至少5％，而在进料中没有脱油废催化剂。

10. 发明授权

US08927448B2 Hydroprocessing catalysts and methods for making thereof 有权
标题翻译：加氢处理催化剂及其制备方法
公开(公告)号：US08927448B2
公开(公告)日：2015-01-06
申请号：US13233491
申请日：2011-09-15
申请人： Bo Kou , Julie Chabot
发明人： Bo Kou , Julie Chabot
IPC分类号： B01J38/48 , C10G47/02 , C10G47/26 , C10G65/00 , C10G65/10 , C10G65/18
CPC分类号： C10G47/02 , C10G47/26 , C10G47/32 , C10G65/00 , C10G65/10 , C10G65/18 , C10G2300/205 , C10G2300/206 , C10G2300/701 , C10G2300/802
摘要： A method to prepare an improved catalyst feed to a system to upgrade heavy oil. The method comprises: providing a spent catalyst that has been used in a hydroprocessing operation has with a solid content ranging from 5 to 50 wt. % in soluble hydrocarbons and having less than 80% but more than 10% of original catalytic activity; removing at least 50% of the soluble hydrocarbons removed in a deoiling step; treating the deoiled spent catalyst with a treating solution containing at least one of plain water, a mineral acid, an oxidizing agent, and combinations thereof to reduce the concentration of at least one metal contaminant in the deoiled spent catalyst by at least 40%. After treatment, the treated deoiled spent catalyst is slurried in a hydrocarbon medium, and fed to the heavy oil upgrade system as part of the catalyst feed system with a fresh slurry catalyst.
摘要翻译：一种制备改进的催化剂进料到系统以升级重油的方法。该方法包括：提供已经在加氢操作中使用的废催化剂的固体含量范围为5-50wt。％的可溶性碳氢化合物，并且具有小于80％但大于10％的原始催化活性; 去除在脱油步骤中去除的至少50％的可溶性烃; 用含有浅水，无机酸，氧化剂及其组合中的至少一种的处理溶液处理脱油的废催化剂，以将去除的废催化剂中的至少一种金属污染物的浓度降低至少40％。处理后，经处理的脱油废催化剂在烃介质中浆化，并作为催化剂进料系统的一部分用新鲜的浆料催化剂进料至重油升级系统。

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