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1. 发明授权

US08188299B2 Acrylate derivatives, alcohol derivatives, and method for producing them 有权
标题翻译：丙烯酸酯衍生物，醇衍生物及其制备方法
公开(公告)号：US08188299B2
公开(公告)日：2012-05-29
申请号：US12884677
申请日：2010-09-17
申请人： Kazuya Shimizu , Masayoshi Yamanaka , Tatsuhiko Hayashibara , Hideharu Iwasaki
发明人： Kazuya Shimizu , Masayoshi Yamanaka , Tatsuhiko Hayashibara , Hideharu Iwasaki
IPC分类号： C07D209/56
CPC分类号： C07D209/02 , C07D491/18
摘要： Provided are an acrylate derivative useful as a raw material of a polymer compound for resist compositions capable of giving resist patterns which are excellent in lithographic performance and have a good shape, an intermediate thereof (alcohol derivative) and production processes for them. To be specific, it is an acrylate derivative represented by a formula shown below: (wherein R1 represents a hydrogen atom, methyl or trifluoromethyl; R2, R3, R5, R7, R8, R9 and R10 each represent independently a hydrogen atom, an alkyl group having 1 to 6 carbon atoms, a cycloalkyl group having 3 to 6 carbon atoms or an alkoxy group having 1 to 6 carbon atoms; R4 and R6 each represent independently a hydrogen atom, an alkyl group having 1 to 6 carbon atoms, a cycloalkyl group having 3 to 6 carbon atoms or an alkoxy group having 1 to 6 carbon atoms, or both of R4 and R6 are combined to represent an alkylene group having 1 to 3 carbon atoms, —O— or —S—; and R11 represents a hydrogen atom, an alkyl group having 1 to 6 carbon atoms or a cyclic hydrocarbon group having 3 to 10 carbon atoms).
摘要翻译：提供可用作抗蚀剂组合物的聚合物化合物的原料的丙烯酸酯衍生物，其能够提供平版印刷性能优异且形状良好的抗蚀剂图案，其中间体（醇衍生物）及其制备方法。具体来说，它是由下式表示的丙烯酸酯衍生物：其中R1表示氢原子，甲基或三氟甲基; R2，R3，R5，R7，R8，R9和R10各自独立地表示氢原子，烷基具有1至6个碳原子的基团，具有3至6个碳原子的环烷基或具有1至6个碳原子的烷氧基; R 4和R 6各自独立地表示氢原子，具有1至6个碳原子的烷基，环烷基具有3至6个碳原子的烷基或具有1至6个碳原子的烷氧基，或者R 4和R 6都被结合以表示具有1至3个碳原子的亚烷基，-O-或-S-; R 11表示氢原子，碳原子数1〜6的烷基或碳原子数3〜10的环状烃基）。

2. 发明授权

US08110124B2 Method of preparing fluorescent body precursor 有权
标题翻译：制备荧光体前体的方法
公开(公告)号：US08110124B2
公开(公告)日：2012-02-07
申请号：US12373989
申请日：2007-07-26
申请人： Yoshihisa Tsuji , Hideharu Iwasaki
发明人： Yoshihisa Tsuji , Hideharu Iwasaki
IPC分类号： C09K11/56
CPC分类号： C09K11/7702 , C01G9/00 , C01G9/006 , C01G9/08 , C01G45/006 , C01G45/02 , C01P2002/52 , C01P2002/72 , C01P2006/80 , C09K11/574 , C09K11/876
摘要： To produce fluorescent bodies providing high brightness and high energy efficiency, a method of preparing a fluorescent body precursor is provided to enable an activator having a large ionic radius to be doped arbitrarily. The problems described above are solved by a method of preparing a fluorescent body precursor, which method is characterized by comprising applying a shock pressure of 0.1 GPa or higher to a mixture consisting essentially of a fluorescent body base, an activator and a co-activating particle-growth promoter to dope the activator into the fluorescent body base in the presence of the co-activating particle-growth promoter.
摘要翻译：为了产生提供高亮度和高能量效率的荧光体，提供了制备荧光体前体的方法，以使得具有大离子半径的活化剂能够被任意掺杂。上述问题是通过制备荧光体前体的方法来解决的，该方法的特征在于包括对基本上由荧光体碱，活化剂和共活化颗粒组成的混合物施加0.1GPa或更高的冲击压力生长促进剂，在共活化的颗粒生长促进剂存在下将活化剂掺入荧光体碱中。

3. 发明申请

US20110147663A1 METHOD FOR PRODUCING ZINC SULFIDE BASED PHOSPHOR 失效
标题翻译：生产基于硫化锌的磷光体的方法
公开(公告)号：US20110147663A1
公开(公告)日：2011-06-23
申请号：US13057168
申请日：2009-07-30
申请人： Yoshihisa Tsuji , Kazuma Inoue , Jun Takai , Hideharu Iwasaki
发明人： Yoshihisa Tsuji , Kazuma Inoue , Jun Takai , Hideharu Iwasaki
IPC分类号： C09K11/56
CPC分类号： C09K11/625 , C09K11/876 , H05B33/14
摘要： The present invention provides a method for producing a zinc sulfide based phosphor by firing a zinc sulfide based phosphor precursor, comprising at least: a first firing step of firing a mixture containing a zinc sulfide based phosphor precursor, sulfur, and a chlorine-containing flux; and a second firing step of further firing the fired product obtained from the first firing step, wherein the first firing step comprises: heating the mixture in an atmosphere wherein an air stream is introduced so that a temperature of the mixture is increased from normal temperature to a transformation temperature at which a crystal system of the phosphor precursor is transformed; when a temperature of the mixture is increased above the transformation temperature, switching the atmosphere to a nitrogen atmosphere and continuing the heating of the mixture; and when the temperature of the mixture reaches a temperature in a range of 1000° C. to 1200° C., inclusive, maintaining the temperature of the mixture at a constant level and thereafter rapidly quenching the mixture and washing the mixture to obtain a fired product; and wherein the second firing step comprises heating in the nitrogen atmosphere the fired product obtained from the first firing step so that the temperature of the fired product is increased from normal temperature to a temperature in a range of 650° C. to 1000° C., inclusive; and when a temperature of the fired product reaches the temperature in the range of 650° C. to 1000° C., inclusive, introducing oxygen while maintaining the temperature of the fired product and thereafter rapidly quenching the fired product and washing the fired product to obtain a zinc sulfide based phosphor. Use of the method of the present invention makes it possible to provide a zinc sulfide based phosphor material suitable for use in the production of an EL device that shows high brightness.
摘要翻译：本发明提供了一种通过焙烧硫化锌系荧光体前体来制造硫化锌系荧光体的方法，该方法至少包括：将含有硫化锌系荧光体前体，硫和含氯助熔剂的混合物进行烧成的第一烧成工序 ; 以及第二烧成工序，对从所述第一烧成工序得到的烧成品进一步进行烧成，其中，所述第一烧成工序包括：在导入空气流的气氛中加热所述混合物，使得所述混合物的温度从常温升高到改变荧光体前体的晶体体系的相变温度; 当混合物的温度升高到转化温度以上时，将气氛切换至氮气氛并继续加热混合物; 并且当混合物的温度达到1000℃至1200℃的范围内的温度时，将混合物的温度保持在恒定水平，然后快速骤冷混合物并洗涤该混合物以获得烧制产品; 并且其中所述第二烧制步骤包括在所述氮气气氛中加热从所述第一烧制步骤获得的烧制产品，使得所述烧制产品的温度从常温升高至650℃至1000℃的温度。，包括的; 并且当烧制品的温度达到650℃至1000℃的温度时，在保持烧制产品的温度的同时引入氧气，然后迅速骤冷烧制产品并将烧制产品洗涤至得到硫化锌系荧光体。通过使用本发明的方法，可以提供一种适用于制造高亮度的EL器件的硫化锌系荧光体材料。

4. 发明授权

US07709415B2 Method for manufacturing activated carbon, polarizable electrode, and electric double-layered capacitor 失效
标题翻译：活性炭，极化电极和双电层电容器的制造方法
公开(公告)号：US07709415B2
公开(公告)日：2010-05-04
申请号：US10509087
申请日：2003-04-22
申请人： Nozomu Sugo , Hideharu Iwasaki , Takanori Kitamura , Tatsuo Morotomi , Tsuyoshi Kowaka , Teruhiro Okada , Shushi Nishimura , Takeshi Fujino , Shigeki Oyama , Yuji Kawabuchi
发明人： Nozomu Sugo , Hideharu Iwasaki , Takanori Kitamura , Tatsuo Morotomi , Tsuyoshi Kowaka , Teruhiro Okada , Shushi Nishimura , Takeshi Fujino , Shigeki Oyama , Yuji Kawabuchi
IPC分类号： C01B31/08
CPC分类号： H01G9/155 , C01B32/342 , H01M4/0471 , H01M4/583 , Y02E60/13
摘要： Activated carbon useful as polarizable electrode material for an electric double-layer capacitor can be obtained by mixing a carbonaceous material and an alkali metal hydroxide while maintaining a solid state, granulating the obtained mixture while maintaining its solid state, dehydrating the obtained granulated substance while maintaining its solid state, and subjecting the granulated dehydration product obtained in the dehydration step to an activation treatment. The preferred pressure of the granulation treatment in the granulation step is 0.01 to 300 Torr, and the preferred temperature of the granulation treatment is 90 to 140° C. The preferred pressure of the dehydration treatment in the dehydration step is 0.01 to 10 Torr, and the preferred temperature of the dehydration treatment is 200 to 400° C.
摘要翻译：用作双电层电容器的可极化电极材料的活性炭可以通过在保持固体状态下混合碳质材料和碱金属氢氧化物同时保持固体状态使所得到的混合物成粒，同时保持所得粒状物质，同时保持其固体状态，并将脱水步骤中获得的造粒脱水产物进行活化处理。制粒工序中的造粒处理的优选压力为0.01〜300乇，造粒处理温度优选为90〜140℃。脱水工序中脱水处理的优选压力为0.01〜10乇，脱水处理的优选温度为200〜400℃。

5. 发明授权

US07700698B2 Process for producing ring-opening metathesis polymer 有权
标题翻译：开环易位聚合物的制备方法
公开(公告)号：US07700698B2
公开(公告)日：2010-04-20
申请号：US11815803
申请日：2006-02-07
申请人： Hideharu Iwasaki , Yasutaka Inubushi
发明人： Hideharu Iwasaki , Yasutaka Inubushi
IPC分类号： C08F4/80 , C08G61/08 , C08F2/44
CPC分类号： C08G61/08 , C08K5/13 , C08K5/50 , C08K5/526
摘要： A process of producing a ring-opening metathesis polymer characterized in that a treatment to decrease the amount of oxygen and/or peroxide in at least one kind of polymerization starting material is performed prior to the ring-opening metathesis polymerization reaction of a cyclic olefin performed in the presence of a ruthenium carbene complex (catalyst). Treatments to decrease the amount of oxygen and/or peroxide include applying an adsorbent to a polymerization starting material to remove oxygen and/or peroxide by adsorption, applying an antioxidant to a polymerization starting material to decompose oxygen or peroxide, and the like.
摘要翻译：一种制备开环易位聚合物的方法，其特征在于在至少一种聚合原料中减少氧和/或过氧化物的量的处理在环烯烃的开环易位聚合反应之前进行在钌卡宾络合物（催化剂）的存在下。减少氧和/或过氧化物的量的处理包括将吸附剂施加到聚合起始材料上以通过吸附除去氧和/或过氧化物，将抗氧化剂施加到聚合起始材料上以分解氧气或过氧化物等。

6. 发明申请

US20090166587A1 METHOD OF PREPARING FLUORESCENT BODY PRECURSOR 有权
标题翻译：制备荧光体前体的方法
公开(公告)号：US20090166587A1
公开(公告)日：2009-07-02
申请号：US12373989
申请日：2007-07-26
申请人： Yoshihisa Tsuji , Hideharu Iwasaki
发明人： Yoshihisa Tsuji , Hideharu Iwasaki
IPC分类号： C09K11/77 , C09K11/54
CPC分类号： C09K11/7702 , C01G9/00 , C01G9/006 , C01G9/08 , C01G45/006 , C01G45/02 , C01P2002/52 , C01P2002/72 , C01P2006/80 , C09K11/574 , C09K11/876
摘要： To produce fluorescent bodies providing high brightness and high energy efficiency, a method of preparing a fluorescent body precursor is provided to enable an activator having a large ionic radius to be doped arbitrarily.The problems described above are solved by a method of preparing a fluorescent body precursor, which method is characterized by comprising applying a shock pressure of 0.1 GPa or higher to a mixture consisting essentially of a fluorescent body base, an activator, and a co-activating particle-growth promoter to dope the activator into the fluorescent body base in the presence of the co-activating particle-growth promoter.
摘要翻译：为了产生提供高亮度和高能量效率的荧光体，提供了制备荧光体前体的方法，以使得具有大离子半径的活化剂能够被任意掺杂。上述问题通过制备荧光体前体的方法来解决，该方法的特征在于包括将基本上由荧光体碱，活化剂和共活化剂组成的混合物施加0.1GPa或更高的冲击压颗粒生长促进剂，以在共活化颗粒生长促进剂存在下将活化剂掺杂到荧光体碱中。

7. 发明申请

US20090023874A1 PROCESS FOR PRODUCING RING-OPENING METATHESIS POLYMER 有权
标题翻译：生产开环元素聚合物的方法
公开(公告)号：US20090023874A1
公开(公告)日：2009-01-22
申请号：US11815803
申请日：2006-02-07
申请人： Hideharu Iwasaki , Yasutaka Inubushi
发明人： Hideharu Iwasaki , Yasutaka Inubushi
IPC分类号： C08F4/60 , C08F4/80
CPC分类号： C08G61/08 , C08K5/13 , C08K5/50 , C08K5/526
摘要： The process of producing a ring-opening metathesis polymer of the present invention is mainly characterized in that a treatment to decrease the amount of oxygen and/or peroxide in at least one kind of polymerization starting material is performed prior to the ring-opening metathesis polymerization reaction of a cyclic olefin performed in the presence of a ruthenium carbene complex (catalyst). As used herein, the “polymerization starting material” refers to various materials used for a ring-opening metathesis polymerization reaction and present in the reaction system, such as ruthenium carbene complex (catalyst) and cyclic olefin (monomer), as well as solvents, chain transfer agents and the like. In addition, the method for a treatment to decrease the amount of oxygen and/or peroxide include a method comprising applying an adsorbent to a polymerization starting material to remove oxygen and/or peroxide by adsorption, a method comprising applying an antioxidant to a polymerization starting material to decompose oxygen or peroxide and the like.According to the present invention, a ring-opening metathesis polymer can be produced at a higher reaction rate without degrading the high activity inherently possessed by a ruthenium carbene complex (catalyst). Because of being free of a decrease in the concentration of the catalyst maintaining the high activity during reaction, the thus-obtained polymer shows a small difference between polymerization lots and becomes homogeneous, and a polymer having a comparatively sharp molecular weight distribution can be produced.
摘要翻译：本发明的开环易位聚合物的制造方法的主要特征在于，在开环易位聚合之前进行至少一种聚合原料中的氧和/或过氧化物的量的减少处理在钌卡宾络合物（催化剂）的存在下进行的环状烯烃的反应。如本文所用，“聚合原料”是指用于开环易位聚合反应并存在于反应体系中的各种材料，例如钌卡宾络合物（催化剂）和环烯烃（单体），以及溶剂，链转移剂等。此外，减少氧和/或过氧化物的量的处理方法包括将吸附剂施加到聚合起始材料以通过吸附除去氧和/或过氧化物的方法，包括将抗氧化剂施加到聚合开始的方法用于分解氧气或过氧化物等的物质。根据本发明，可以以更高的反应速率制备开环易位聚合物，而不会降低钌卡宾配合物（催化剂）固有的高活性。由于在反应过程中催化剂的浓度降低而保持高的活性，所以由此获得的聚合物在聚合批间之间显示出很小的差异并且变得均匀，并且可以生产具有相当尖锐的分子量分布的聚合物。

8. 发明申请

US20070197834A1 Bisphosphite and process for producing aldehyde compound with the bisphosphite 有权
标题翻译：二亚磷酸酯和与二亚磷酸酯生产醛化合物的方法
公开(公告)号：US20070197834A1
公开(公告)日：2007-08-23
申请号：US10594131
申请日：2005-03-22
申请人： Tomoaki Tsuji , Hideharu Iwasaki
发明人： Tomoaki Tsuji , Hideharu Iwasaki
IPC分类号： C07F15/00 , C07F9/06 , C07C45/49
CPC分类号： B01J31/185 , B01J2231/321 , B01J2531/822 , C07C45/50 , C07F9/145 , C07C47/02 , C07C47/19
摘要： Bisphosphite(s) represented by the following general formula (I): wherein Ar1 and Ar2 are each independently a substituted or unsubstituted arylene group; R1, R2, R7 and R8 are each independently a substituted or an unsubstituted alkyl group, a substituted or an unsubstituted aryl group or a substituted or an unsubstituted heterocyclic group, or R1and R2 or R7 and R8 may together form a ring with their associated oxygen atoms and phosphor atom; and R3, R4, R5 and R6 are each independently a hydrogen atom or an alkyl group, with the proviso that the carbon atom bearing R3 and R4 and the carbon atom bearing R5 and R6 are bound to the respective arylene groups at the ortho position to the Ar1—Ar2 bond. Also provided is a process for producing aldehyde(s) using the bisphosphite and a Group 8 to 10 metal compound. A composition comprising the bisphosphite and a Group 8 to 10 metal compound is further provided.
摘要翻译：由以下通式（I）表示的二亚磷酸酯：其中Ar 1和Ar 2各自独立地为取代或未取代的亚芳基; R 1，R 2，R 7和R 8各自独立地为取代或未取代的烷基，取代或未取代的芳基或取代或未取代的杂环基，或R 1和R 2或R 7和R 0 > 8可以一起形成具有其相关氧原子和磷原子的环; R 3，R 4，R 5和R 6各自独立地为氢原子或烷基条件是带有R 3和R 4的碳原子和带有R 5和R 6的碳原子， SUP>在与Ar 1 -Ar 2 O 2键的邻位上的各个亚芳基结合。还提供了使用二亚磷酸酯和第8至10族金属化合物生产醛的方法。还提供包含二亚磷酸酯和第8至10族金属化合物的组合物。

9. 发明授权

US06239295B1 Process for producing 3-methyltetrahydrofuran, and process for producing an intermediate thereof 有权
标题翻译：制备3-甲基四氢呋喃的方法及其中间体的制备方法
公开(公告)号：US06239295B1
公开(公告)日：2001-05-29
申请号：US09577318
申请日：2000-05-24
申请人： Hideharu Iwasaki
发明人： Hideharu Iwasaki
IPC分类号： C07D30702
CPC分类号： C07D307/06
摘要： A process for producing 3-methyltetrahydrofuran, and processes for producing 3-hydroxy-3-methyltetrahydrofuran and 3-methyldihydrofuran, which are intermediates thereof, are provided.
摘要翻译：提供了制备3-甲基四氢呋喃的方法，以及作为其中间体的3-羟基-3-甲基四氢呋喃和3-甲基二氢呋喃的制备方法。

10. 发明授权

US5955636A Process for producing 6-methyl-3-hepten-2-one and 6-methyl-2-heptanone analogues, and process for producing phyton or isophytol 失效
标题翻译：生产6-甲基-3-庚烯-2-酮和6-甲基-2-庚酮类似物的方法，以及生产植物油或异植醇的方法
公开(公告)号：US5955636A
公开(公告)日：1999-09-21
申请号：US887260
申请日：1997-07-02
申请人： Yoichi Kido , Noriaki Kumagai , Hideharu Iwasaki , Takashi Onishi , Fuyuo Ueyama
发明人： Yoichi Kido , Noriaki Kumagai , Hideharu Iwasaki , Takashi Onishi , Fuyuo Ueyama
IPC分类号： C07C29/17 , C07C29/40 , C07C29/42 , C07C45/51 , C07C45/62 , C07C45/67 , C07C45/73 , C07C45/74 , C07C49/04 , C07C49/203 , C07C45/61
CPC分类号： C07C29/172 , C07C29/40 , C07C29/42 , C07C45/513 , C07C45/62 , C07C45/676 , C07C45/73 , C07C45/74 , C07C49/04 , C07C49/203
摘要： Provided are a process for producing 6-methyl-3-hepten-2-one by cross aldol condensation carried out while each continuously adding to acetone, isovaleraldehyde and an aqueous alkali containing an alkaline substance; a process for producing a 6-methyl-2-heptanone analogue represented by Formula (1): ##STR1## wherein n is an integer of 0 or 1 or more; which comprises allowing hydrogen, acetone and an aldehyde represented by Formula (2): ##STR2## wherein n is as defined above; X and Y each represents a hydrogen atom or they are coupled together to form a carbon-carbon bond; and Z and W each represents a hydrogen atom or they are coupled together to form a carbon-carbon bond;to react in the presence of an aqueous alkali containing an alkaline substance, and a hydrogenation catalyst; and a process for producing phyton or isophytol using the 6-methyl -3-hepten-2-one or the 6-methyl-2-heptanone analogue.
摘要翻译：本发明提供通过交叉醛醇缩合制备6-甲基-3-庚烯-2-酮的方法，同时连续加入丙酮，异戊醛和含碱性物质的碱水溶液; 一种由式（1）表示的6-甲基-2-庚酮类似物的制备方法：其中n为0或1以上的整数; 其包括使氢，丙酮和由式（2）表示的醛：其中n如上所定义; X和Y各自表示氢原子或它们连接在一起形成碳 - 碳键; Z和W各自表示氢原子或它们连接在一起形成碳 - 碳键; 在含有碱性物质的碱性水溶液和氢化催化剂的存在下反应; 以及使用6-甲基-3-庚烯-2-酮或6-甲基-2-庚酮类似物生产植物油或异植醇的方法。

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