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1. 发明申请

US20130168226A1 METHOD AND APPARATUS FOR EVAPORATING HYDROGEN HALIDE AND WATER FROM BIOMASS HYDROLYZATES CONTAINING HALOGEN ACID 有权
标题翻译：用于从包含卤酸的生物质水解产物中蒸发氢化物和水的方法和装置
公开(公告)号：US20130168226A1
公开(公告)日：2013-07-04
申请号：US13809904
申请日：2011-07-12
申请人： Frank Kose , Matthias Schmidt
发明人： Frank Kose , Matthias Schmidt
IPC分类号： B01D3/40
CPC分类号： B01D3/40 , B01D1/14 , B01D1/16 , Y02P30/20
摘要： The invention relates to a method and a device with the aid of which hydrogen halide and water are removed from biomass hydrolyzates containing halogen acid. The core of the invention is an evacuated container (B1), which is continuously supplied with a heat-transfer medium and which is completely filled with the heat-transfer medium in a part. In said evaporation chamber, the biomass hydrolyzate is likewise continuously introduced. In the container (B1), heat is transferred from the heat-transfer medium to the hydrolyzate, wherein hydrogen halide and water are continuously evaporated. The remaining hydrolyzate particles are continuously discharged with the cooled heat-transfer medium and continuously removed by means of the heat-transfer medium and continuously separated from said heat-transfer medium. The invention described can also be used to treat other mixtures or solutions for the purpose of evaporation. The following is fundamental in regard to the heat-transfer medium used: the heat-transfer medium is chemically inert with respect to the introduced substances.
摘要翻译：本发明涉及一种借助卤化氢和水从含有卤素酸的生物质水解产物中除去的方法和装置。本发明的核心是抽真空容器（B1），其连续地供给传热介质，并且部分地完全填充有传热介质。在所述蒸发室中，生物质水解产物同样被连续引入。在容器（B1）中，热量从传热介质转移到水解液中，其中卤化氢和水连续蒸发。剩余的水解物颗粒用冷却的传热介质连续排出，并通过传热介质连续除去，并与所述传热介质连续分离。所描述的本发明也可用于处理用于蒸发目的的其它混合物或溶液。以下是使用的传热介质的基础：传热介质相对于引入的物质是化学惰性的。

2. 发明申请

US20190055408A1 Method for the Fixation of Metals, Transition Metals and their Oxides on Siliceous Materials of Plant Origin and Use of these Modified Siliceous Materials as a Catalyst and a Loading Material for Pigments, Paints, Plastics, Elastomers and Sizing Materials 审中-公开
公开(公告)号：US20190055408A1
公开(公告)日：2019-02-21
申请号：US16079109
申请日：2017-02-17
申请人： Matthias Schmidt , Frank Kose , Green Sugar AG
发明人： Matthias Schmidt , Frank Kose
IPC分类号： C09C1/30 , B01J21/06 , B01J37/06 , B01J37/08 , B01J37/02
摘要： The invention relates to a method, in which siliceous biomass is modified in the spectrum of the existing non-silicon metals and these non-silicon metals are fixed onto the siliceous skeleton of the plant by burning. The ashes produced can be used as auxiliary agents for heterogeneous catalysis in the chemical industry and as loading materials for plastics, elastomers, pigments, paints and sizing materials.

3. 发明授权

US07483812B2 Method for determining a linear relationship from measured data that can be stored electronically 失效
标题翻译：从可以电子存储的测量数据确定线性关系的方法
公开(公告)号：US07483812B2
公开(公告)日：2009-01-27
申请号：US11182723
申请日：2005-07-15
申请人： Matthias Holschneider , Frank Kose
发明人： Matthias Holschneider , Frank Kose
IPC分类号： G06F17/18 , G06F19/00
CPC分类号： G06F17/18
摘要： A method for determining a linear relationship in a set of measured data is provided. A set of measured values for at least two measured variables from the set of measured data is selected, and a respective measurement uncertainty interval is assigned to each of the selected set of measured values. A set of hypothetical linear relationships is formed based at least in part on the selected set of measured values. Partial probabilities for the set of hypothetical linear relationships are determined and assigned to the set of hypothetical linear relationships. A total probability is determined for at least a portion of the hypothetical linear relationships by summing the partial probabilities associated with the portion of the hypothetical linear relationships, and a rank of the set of hypothetical linear relationships is determined as a function of the total probabilities determined for the portion of the set of hypothetical linear relationships.
摘要翻译：提供了一种用于确定一组测量数据中的线性关系的方法。选择来自该组测量数据的至少两个测量变量的一组测量值，并且将相应的测量不确定性间隔分配给所选择的一组测量值中的每一个。至少部分地基于所选择的一组测量值形成一组假设的线性关系。确定一组假设线性关系的部分概率并将其分配给一组假设的线性关系。通过对与假设线性关系的部分相关联的部分概率求和来确定假想线性关系的至少一部分的总概率，并且确定该组假设线性关系的等级作为所确定的总概率的函数对于该组假设线性关系的一部分。

4. 发明申请

US20060015307A1 Method for determining a linear relationship from measured data that can be stored electronically 失效
标题翻译：从可以电子存储的测量数据确定线性关系的方法
公开(公告)号：US20060015307A1
公开(公告)日：2006-01-19
申请号：US11182723
申请日：2005-07-15
申请人： Matthias Holschneider , Frank Kose
发明人： Matthias Holschneider , Frank Kose
IPC分类号： G06F17/10
CPC分类号： G06F17/18
摘要： The invention relates to a method for determining a linear relationship in a set of measured data that can be stored electronically, it being possible for the linear relationship to be represented graphically by means of a straight line and the measured data in each case comprising a measured value assigned to a measured variable, the method having the following steps: selecting a set of measured values for at least two measured variables from the set of measured data that can be stored electronically; assigning a respective measurement uncertainty interval to the selected measured values; forming a set of hypothetical linear relationships by means of the set of selected measured values; determining partial probabilities for the set of hypothetical linear relationships and assigning the partial probabilities determined to the hypothetical linear relationships, a partial probability being determined and assigned for one of the measured values for one of the hypothetical linear relationships if the measurement uncertainty interval of the one of the measured values is intersected by the one of the hypothetical linear relationships; determining a total probability for at least some of the hypothetical linear relationships by the associated partial probabilities for at least some of the hypothetical linear relationships being summed; and determining a rank of the hypothetical linear relationships as a function of the total probabilities determined for at least some of the hypothetical linear relationships.
摘要翻译：本发明涉及一种用于确定可以电子存储的一组测量数据中的线性关系的方法，可以通过直线以线性方式表示线性关系，并且每种情况下的测量数据包括测量的数据分配给测量变量的值，该方法具有以下步骤：从可以电子存储的一组测量数据中选择至少两个测量变量的一组测量值; 将相应的测量不确定性间隔分配给所选择的测量值; 通过所选择的测量值的集合形成一组假设的线性关系; 确定所述一组假设线性关系的部分概率并且将所确定的部分概率分配给所述假设线性关系，如果所述假设线性关系中的一个的测量不确定性间隔的测量值与假设的线性关系之一相交; 对所述假设线性关系中的至少一些相加的相关部分概率确定所述假设线性关系中的至少一些的总概率; 以及确定所述假设线性关系的等级作为针对所述假设线性关系中的至少一些所确定的总概率的函数。

5. 发明授权

US09254451B2 Method and apparatus for evaporating hydrogen halide and water from biomass hydrolyzates containing halogen acid 有权
标题翻译：用于从含有卤素酸的生物质水解产物中蒸发卤化氢和水的方法和装置
公开(公告)号：US09254451B2
公开(公告)日：2016-02-09
申请号：US13809904
申请日：2011-07-12
申请人： Frank Kose , Matthias Schmidt
发明人： Frank Kose , Matthias Schmidt
IPC分类号： B01D3/40 , B01D1/14 , B01D1/16
CPC分类号： B01D3/40 , B01D1/14 , B01D1/16 , Y02P30/20
摘要： The invention relates to a method and a device with the aid of which hydrogen halide and water are removed from biomass hydrolyzates containing halogen acid. The core of the invention is an evacuated container (B1), which is continuously supplied with a heat-transfer medium and which is completely filled with the heat-transfer medium in a part. In said evaporation chamber, the biomass hydrolyzate is likewise continuously introduced. In the container (B1), heat is transferred from the heat-transfer medium to the hydrolyzate, wherein hydrogen halide and water are continuously evaporated. The remaining hydrolyzate particles are continuously discharged with the cooled heat-transfer medium and continuously removed by means of the heat-transfer medium and continuously separated from said heat-transfer medium. The invention described can also be used to treat other mixtures or solutions for the purpose of evaporation. The following is fundamental in regard to the heat-transfer medium used: the heat-transfer medium is chemically inert with respect to the introduced substances.
摘要翻译：本发明涉及一种借助卤化氢和水从含有卤素酸的生物质水解产物中除去的方法和装置。本发明的核心是抽真空容器（B1），其连续地供给传热介质，并且部分地完全填充有传热介质。在所述蒸发室中，生物质水解产物同样被连续引入。在容器（B1）中，热量从传热介质转移到水解液中，其中卤化氢和水连续蒸发。剩余的水解物颗粒用冷却的传热介质连续排出，并通过传热介质连续除去，并与所述传热介质连续分离。所描述的本发明也可用于处理用于蒸发目的的其它混合物或溶液。以下是使用的传热介质的基础：传热介质相对于引入的物质是化学惰性的。

6. 发明授权

US08283178B2 Method and apparatus for removing halogen hydracids from biomass hydrolysates 有权
标题翻译：从生物质水解产物中除去卤素氢的方法和设备
公开(公告)号：US08283178B2
公开(公告)日：2012-10-09
申请号：US12991611
申请日：2009-05-02
申请人： Matthias Schmidt , Frank Kose
发明人： Matthias Schmidt , Frank Kose
IPC分类号： G01N25/22
CPC分类号： B01J19/26 , B01J19/0013 , B01J19/2405 , B01J2219/00123 , B01J2219/00128 , C13K1/02
摘要： A process for removing hydrogen halide and water from hydrolyzates obtained by way of halogen-acid hydrolysis from vegetable biomasses. Two containers are connected to each other via a tube. Two flows are fed in at the inlet of the first container, one representing the hydrolyzates and the other a heat transfer medium; both flows are sprayed together in the first container, producing a homogeneous mixing of the two flows, including heat transfer, which subsequently results in complete evaporation of water and the hydrogen halide dissolved in the hydrolyzates. The evaporation produces a mixture of granular solid bodies and heat transfer medium droplets that is pulled from the first container into the second container through the connecting tube via a pressure gradient. The second container is configured as a cyclone or centrifugal force precipitator, and there is a separation of liquid and solid constituents from the gas.
摘要翻译：从通过植物生物质的卤酸水解获得的水解产物中除去卤化氢和水的方法。两个容器通过管相互连接。在第一容器的入口处输入两个流量，一个代表水解产物，另一个代表传热介质; 两个流体在第一容器中一起喷雾，产生两个流动的均匀混合，包括热传递，其随后导致水和溶解在水解产物中的卤化氢的完全蒸发。蒸发产生颗粒状固体和传热介质液滴的混合物，其通过压力梯度通过连接管从第一容器进入第二容器。第二容器被构造为旋风分离器或离心力除尘器，并且液体和固体成分与气体分离。

7. 发明申请

US20110070131A1 APPARATUS FOR REMOVING HALOGEN HYDRACIDS FROM BIOMASS HYDROLYSATES 有权
公开(公告)号：US20110070131A1
公开(公告)日：2011-03-24
申请号：US12991611
申请日：2009-05-02
申请人： Matthias Schmidt , Frank Kose
发明人： Matthias Schmidt , Frank Kose
IPC分类号： B01D17/038
CPC分类号： B01J19/26 , B01J19/0013 , B01J19/2405 , B01J2219/00123 , B01J2219/00128 , C13K1/02
摘要： An apparatus for removing hydrogen halide and water from hydrolysates that were obtained by way of halogen-acid hydrolysis from vegetable biomasses, characterized in that: —said apparatus comprises two containers, which are connected to each other by a tube, —at the inlet of the first container two flows are fed, one representing the hydrolysates and the other a heat transfer medium, which dissolves in the hydrolysate only to an economically justifiable extent (no additional process steps due to potential contamination during mixing), or enriches matter therefrom, —both flows are sprayed together in the first container, thereby producing a homogeneous mixing of the two flows, including heat transfer, which subsequently results in complete evaporation of water and the hydrogen halide dissolved in the hydrolysates, —the evaporation produces a mixture of granular solid bodies and heat transfer medium droplets, which is pulled from the first container into the second container via the connecting tube by way of a pressure gradient, —the second container is configured as a cyclone or centrifugal force precipitator, and a separation of liquid (heat transfer medium droplets) and solid constituents (granular solid bodies) from the gas flow takes place. An apparatus, characterized in that the second container (here: cyclone) on the inside wall may be lined with polyvinylchloride [PVC] (hard), PVC (chlorinated), polyethylene (PE), polypropylene (PP), polybutylene (PB), polytetrafluoroethylene (PTFE), polyvinylidene fluoride (PVDF), polyvinyl fluoride (PVF), ethylene-propylene-diene rubber (EPDM), ethylene-propylene copolymer, ethylene-tetrafluoroethylene (ETFE), perfluoro-ethylene-propylene plastic (FEP), fluoropolymer plastics (FPM and FKM=group designation), perfluoro trifluoroethylene (PCTFE), perfluorinated rubber (FFPM and FFKM), butyl robber (HR), isoprene rubber (IR), chlorinated polyethylene (PE-C) and rubber (collective term for rubbers containing sulfur) and copolymers and mixtures thereof from said polymers, or comprises them.

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