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1. 发明授权

US11939669B2 Coating method for continuous preparation of diamond thin film with HFCVD device 有权
公开(公告)号：US11939669B2
公开(公告)日：2024-03-26
申请号：US17627754
申请日：2019-11-26
申请人： Institute of Metal Research Chinese Academy of Sciences
发明人： Lusheng Liu , Xin Jiang , Nan Huang
IPC分类号： C23C16/27 , C23C16/458 , C23C16/52 , C23C16/54
CPC分类号： C23C16/271 , C23C16/4587 , C23C16/52 , C23C16/54
摘要： A coating method for preparing diamond thin film continuously by HFCVD device includes the steps of: (a) carbonizing left and right chamber hot filaments; (b) disposing a substrate on a platform along with a trolley in a sample access chamber under vacuum condition; opening a left chamber gate valve and moving the substrate to left thin film growth chamber; closing the left chamber gate valve to grow diamond thin film on the substrate; (c) repeating step (b) by using a right chamber gate valve and right thin film growth chamber to grow diamond thin film; (d) opening the left chamber gate valve and moving the substrate to the sample access chamber; closing the left chamber gate valve and dropping to room temperature while under vacuum condition; releasing the vacuum condition and taking out the substrate with diamond thin film; (e) repeating step (d) for the right chamber gate valve.

2. 发明申请

US20220259707A1 ULTRA-CLEAN RARE EARTH STEEL AND OCCLUDED FOREIGN SUBSTANCE MODIFICATION CONTROL METHOD 有权
公开(公告)号：US20220259707A1
公开(公告)日：2022-08-18
申请号：US17611061
申请日：2019-09-29
申请人： INSTITUTE OF METAL RESEARCH CHINESE ACADEMY OF SCIENCES
发明人： Dianzhong LI , Yikun LUAN , Hongwei LIU , Paixian FU , Xiaoqiang HU , Pei WANG , Lijun XIA , Chaoyun YANG , Hanghang LIU , Yang LIU , Peng LIU , Yiyi LI
IPC分类号： C22C38/00 , C22C33/04 , C21C7/06 , C21C7/04 , C21C7/00
摘要： Provided are an ultra-clean rare earth steel and an occluded foreign substance modification control method, the steel includes 10-200 ppm of rare earth elements, 50% or more occluded foreign substances in the steel are dispersed into RE-oxygen-sulfide with the average equivalent diameter Dmean ranging from 1-5 μm in a spherical shape or a substantially spherical shape or a granular shape; according to the method, at least 80%, preferably at least 90%, of Al2O3 occluded foreign substances in the steel are modified into RE-oxygen-sulfide, compared with steel with the same components without rare earth, the total amount of the occluded foreign substances in the steel is reduced by 18% or higher, the cracking probability caused by occluded foreign substances such as Al2O3 in traditional pure steel is reduced, the mechanical performance such as the fatigue life of the steel is remarkably improved.

3. 发明授权

US11149095B2 Cellulose II nanocrystal particles and preparation method and use thereof 有权
公开(公告)号：US11149095B2
公开(公告)日：2021-10-19
申请号：US16475921
申请日：2017-12-27
申请人： Institute of Metal Research Chinese Academy of Sciences
发明人： Jinsong Zhang , Yukun Yan , Yangtao Zhou , Zhiyu Liu
IPC分类号： C08B1/00 , C08L1/04 , C08L1/00 , C08L1/06 , C08L1/02 , C08B15/02 , B01J31/06 , B01J35/02
摘要： Cellulose II nanocrystal particles have a crystallinity ≥80%, a number-average molecular weight ranging from 1200 to 2500, and a molecular weight distribution coefficient Mw/Mn≤1.30. The cellulose II nanocrystal particles can be prepared by: subjecting a cellulose raw material to an amorphization reconstitution and then to a crystallization acidolysis. The crystallization acidolysis may be carried out under a low concentration acidic condition. The method enables high efficient and clean production and quality control of cellulose nanocrystal materials.

4. 发明申请

US20210102280A1 ZR-BASED AMORPHOUS ALLOY AND MANUFACTURING METHOD THEREOF 有权
公开(公告)号：US20210102280A1
公开(公告)日：2021-04-08
申请号：US16500083
申请日：2018-04-20
申请人： INSTITUTE OF METAL RESEARCH, CHINESE ACADEMY OF SCIENCES , JIANGSU HAIJIN METALLIC GLASS TECHNOLOGY CO., LTD
发明人： Yi LI , Yinxiao WANG , Hongchuan CAI , Jinjiu QIU
IPC分类号： C22C45/10 , C22C1/00
摘要： A Zr-based amorphous alloy and a manufacturing method thereof, wherein the Zr-based amorphous alloy includes a composition of (ZraHfbCucNidAle)100-XOx, wherein a, b, c, d, e, x are atomic percentages, and 49≤a≤55, 0.05≤b≤1, 31≤c≤38, 3≤d≤5, 7≤e≤10.5, and 0.05≤x≤0.5, wherein based on the volume of the alloy, the Zr-based amorphous alloy is cast into a rod-shaped sample having a diameter of 12-16 mm and a length of 60 mm, an amorphous content of 40%-95%, a strength of above 1800 MPa, and a fracture toughness of higher than 90 KPam1/2.

5. 发明申请

US20140130972A1 Method for Transferring Graphene Nondestructively with Low Cost 有权
标题翻译：以低成本非破坏性地转移石墨烯的方法
公开(公告)号：US20140130972A1
公开(公告)日：2014-05-15
申请号：US14124072
申请日：2012-06-08
申请人： Wencai Ren , Libo Gao , Laipeng Ma , Huiming Cheng
发明人： Wencai Ren , Libo Gao , Laipeng Ma , Huiming Cheng
IPC分类号： B32B37/00
CPC分类号： B32B37/025 , B82Y30/00 , B82Y40/00 , C01B32/184 , C01B32/194 , C01B2204/02 , C25B1/00 , C25F5/00
摘要： A method for transferring graphene nondestructively and at a low cost. In the method, a graphene is used whose surface is coated with transferring media and whose original substrate is an electrode, the electrode is placed into an electrolyte, and the graphene is separated from the original substrate by means of the driving force of bubbles and the gas intercalation produced on the graphene electrode surface during electrolysis. Then, the graphene coated with transferring media is nondestructively combined with a target substrate. The transferring media is removed so as to transfer the graphene to the target substrate nondestructively. The transferring method results in no damage or loss with respect to the graphene and the original substrate, and the original substrate can be re-used. Furthermore, the method is easy to perform, works quickly, is easy to control, and is pollution-free.
摘要翻译：非破坏性地以低成本转移石墨烯的方法。在该方法中，使用其表面涂覆有转印介质并且其原始基底为电极的石墨烯，电极被放置在电解质中，并且通过气泡的驱动力将石墨烯与原始基底分离，并且在电解过程中在石墨烯电极表面产生气体插层。然后，涂覆有转印介质的石墨烯与靶基材非破坏性地组合。去除转印介质以将石墨烯非破坏性地转印到目标衬底上。转印方法不会对石墨烯和原始基底造成损害或损失，并且可以重新使用原始基底。此外，该方法易于执行，工作快速，易于控制，无污染。

6. 发明授权

US11655529B2 Zr-based amorphous alloy and manufacturing method thereof 有权
公开(公告)号：US11655529B2
公开(公告)日：2023-05-23
申请号：US16500083
申请日：2018-04-20
申请人： INSTITUTE OF METAL RESEARCH, CHINESE ACADEMY OF SCIENCES , JIANGSU HAIJIN METALLIC GLASS TECHNOLOGY CO., LTD
发明人： Yi Li , Yinxiao Wang , Hongchuan Cai , Jinjiu Qiu
IPC分类号： C22C45/10 , C22C1/11
CPC分类号： C22C45/10 , C22C1/11
摘要： A Zr-based amorphous alloy and a manufacturing method thereof, wherein the Zr-based amorphous alloy includes a composition of (ZraHfbCucNidAle)100-XOx, wherein a, b, c, d, e, x are atomic percentages, and 49≤a≤55, 0.05≤b≤1, 31≤c≤38, 3≤d≤5, 7≤e≤10.5, and 0.05≤x≤0.5, wherein based on the volume of the alloy, the Zr-based amorphous alloy is cast into a rod-shaped sample having a diameter of 12-16 mm and a length of 60 mm, an amorphous content of 40%-95%, a strength of above 1800 MPa, and a fracture toughness of higher than 90 KPam1/2.

7. 发明授权

US11655512B2 Rare-earth microalloyed steel and control method 有权
公开(公告)号：US11655512B2
公开(公告)日：2023-05-23
申请号：US17641732
申请日：2019-09-29
申请人： INSTITUTE OF METAL RESEARCH CHINESE ACADEMY OF SCIENCES
发明人： Dianzhong Li , Yikun Luan , Pei Wang , Xiaoqiang Hu , Paixian Fu , Hongwei Liu , Lijun Xia , Chaoyun Yang , Hanghang Liu , Hang Liu , Yiyi Li
IPC分类号： C21C7/00 , C21C7/10 , C22C33/04 , C22C38/06 , C22C38/04 , C22C38/02 , C22C38/00
CPC分类号： C21C7/0006 , C21C7/10 , C22C33/04 , C22C38/001 , C22C38/002 , C22C38/005 , C22C38/02 , C22C38/04 , C22C38/06
摘要： Provided in the present application are a rare-earth microalloyed steel and a control process. The steel has a special microstructure, and the microstructure comprises a rare earth-rich nanocluster having a diameter of 1-50 nm. The nanocluster has the same crystal structure type as a matrix. The rare earth-rich nanocluster inhibits the segregation of the elements S, P and As on a grain boundary, and obviously improves the fatigue life of the steel. In addition, a rare-earth solid solution also directly affects a phase change dynamics process so that the diffusion-type phase change starting temperature in the steel changes at least to 2° C., and even changes to 40-60° C. in some kinds of steel, thereby greatly improving the mechanical properties thereof, and providing a foundation for the development of more kinds of high-performance steel.

8. 发明授权

US09945399B2 Liquid-driven nano-porous actuator and the application thereof 有权
公开(公告)号：US09945399B2
公开(公告)日：2018-04-17
申请号：US14764824
申请日：2014-09-26
申请人： INSTITUTE OF METAL RESEARCH CHINESE ACADEMY OF SCIENCES
发明人： Xinglong Ye , Lingzhi Liu , Haijun Jin
IPC分类号： B81B3/00 , F15B15/08
CPC分类号： F15B15/08 , B81B3/0032 , B81B2201/038 , Y10T29/49828
摘要： The present invention discloses a liquid-driven nano-porous actuator and the application thereof, and belongs to the field of nano material actuators. According to the present invention, by changing the content of the liquid in the nano-porous material, the interface between the surface liquid of the nano-porous material and air is exchanged between flat and curved states, so as to change the compressive stress acting on the nano-porous material from the surface tension of the liquid and change the elastic deformation of the nano-porous material, thus driving the nano-porous material to contract and expand in a reversible manner and further realizing driving performance. The actuator features simple and easy implementation and environmental-friendly effect without the need of external physical excitation signals (light, magnetic field, electricity or heat), complicated external excitation process, conversion of electric, magnetic, and light energy, chemical or electrochemical process, or toxic, harmful or corrosive chemical substances, and it is especially suitable for bio-robot, medical and aerospace fields.

9. 发明授权

US09896753B2 Bulk amorphous alloy Zr—Cu—Ni—Al—Ag—Y and methods of preparing and using the same 有权
公开(公告)号：US09896753B2
公开(公告)日：2018-02-20
申请号：US14806678
申请日：2015-07-23
申请人： Institute of Metal Research, Chinese Academy of Sciences , DongGuan Eontec Co., Ltd.
发明人： Huameng Fu , Haifeng Zhang , Zhengkun Li , Aimin Wang , Zhengwang Zhu , Hongwei Zhang , Hong Li , Yangde Li , Weirong Li , Tiezhuang Tang
IPC分类号： C22C45/10 , C22F1/18 , C22C1/00 , C22C1/03
CPC分类号： C22C45/10 , C22C1/002 , C22C1/03 , C22F1/186
摘要： A bulk amorphous alloy, including, based on atomic percentage amounts, between 41 and 63% of Zr, between 18 and 46% of Cu, between 1.5 and 12.5% of Ni, between 4 and 15% of Al, between 0.01 and 5% of Ag, and between 0.01 and 5% of Y.

10. 发明申请

US20160263655A1 HOT ISOSTATIC PRESSING PROCESS FOR SUPERALLOY POWDER 审中-公开
标题翻译：超级粉末热稳定压制工艺
公开(公告)号：US20160263655A1
公开(公告)日：2016-09-15
申请号：US15029900
申请日：2014-06-13
申请人： INSTITUTE OF METAL RESEARCH CHINESE ACADEMY OF SCIENCES
发明人： Litao CHANG , Yuyou CUI , Wenru SUN , Rui YANG
IPC分类号： B22F3/15 , C22C16/00 , B22F9/08 , C22C19/05 , B22F1/00 , B22F3/24
CPC分类号： B22F3/15 , B22F1/0003 , B22F1/0085 , B22F3/24 , B22F9/082 , B22F2009/0824 , B22F2998/10 , C22C1/0433 , C22C16/00 , C22C19/056 , C22F1/10 , B22F3/1216 , B22F2003/248
摘要： Hot isostatic press (HIP) process for superalloy powder, to form a superalloy member. A first step HIP temperature is higher than an initial melting temperature of low-melting-point alloy powder and more than 15° C. lower than a solidus of completely homogenized alloy. Pressure is ≧90 MPa, and time is 20 minutes≦t≧1 hour. Heating is stopped after the first step to cool material until temperature is below initial melting temperature of low-melting-point phase. There is temperature keeping for ≧2 hours, to ensure low-melting-point phase, formed during cooling after first step, is completely dissolved. Alloy is cooled after second step to room temperature as furnace pressure keeping continues. Formation of an original particle boundary is prevented or there is significantly reduced the number of precipitated phases on the original particle boundary in HIP procedure, to obtain compact alloy with microscopic structures as equiaxed crystals.
摘要翻译：热等静压（HIP）工艺为超合金粉末，形成超合金构件。第一步HIP温度高于低熔点合金粉末的初始熔融温度，比完全均质合金的固相线低15℃以上。压力≥90MPa，时间为20分钟≤t≥1小时。在第一步骤之后停止加热以冷却材料，直到低于低熔点相的初始熔融温度。保温≥2小时，确保第一步冷却后形成的低熔点相完全溶解。合金在第二步骤冷却至室温后，炉膛压力保持持续。避免了原始粒子界面的形成，或者在HIP程序中原始粒子边界处的析出相数明显减少，得到具有微观结构的紧密合金作为等轴晶体。

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