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1. 发明授权

US08287836B2 Method for preparing single walled carbon nanotubes 失效
标题翻译：制备单壁碳纳米管的方法
公开(公告)号：US08287836B2
公开(公告)日：2012-10-16
申请号：US11841952
申请日：2007-08-20
申请人： Xinjie Zhang , Jun Ma , Howard Tennent , Robert Hoch
发明人： Xinjie Zhang , Jun Ma , Howard Tennent , Robert Hoch
IPC分类号： D01F9/12 , B82B3/00
CPC分类号： B82Y40/00 , B01J23/881 , B01J23/882 , B82Y30/00 , C01B32/162 , C01B2202/02 , C01B2202/26 , C01B2202/30 , C01B2202/34 , Y10S977/843
摘要： Methods of preparing single walled carbon nanotubes are provided. Carbon containing gas is contacted with a supported metal catalyst under reaction conditions to yield at least 90% single walled carbon nanotubes and at least 1 gram single walled carbon nanotubes/gram metal catalyst. The support material may be calcined at temperatures between 150 and 600° C., and may have at least one oxidized planar surface. Reaction conditions include less than 10 atmospheres pressure and less than 800° C.
摘要翻译：提供制备单壁碳纳米管的方法。在反应条件下，将含碳气体与负载金属催化剂接触，得到至少90％的单壁碳纳米管和至少1克单壁碳纳米管/克金属催化剂。支撑材料可以在150℃和600℃之间的温度下煅烧，并且可以具有至少一个氧化的平面表面。反应条件包括小于10大气压和小于800℃

2. 发明申请

US20120153235A1 Electroconductive Carbon Fibril-Based Inks and Coatings 有权
标题翻译：基于导电碳纤维的油墨和涂料
公开(公告)号：US20120153235A1
公开(公告)日：2012-06-21
申请号：US13325560
申请日：2011-12-14
申请人： Jun MA , Alan B. FISCHER , Chunming NIU , Lein NGAW
发明人： Jun MA , Alan B. FISCHER , Chunming NIU , Lein NGAW
IPC分类号： H01B1/04 , B82Y30/00
CPC分类号： H01C17/06586 , C09D5/24 , C09D11/52 , H01B1/24 , H01C17/0652 , H01G11/24 , H01G11/38 , Y02E60/13 , Y10S977/742 , Y10T428/25 , Y10T428/29 , Y10T428/30
摘要： Provided are inks and coatings including carbon nanotubes.
摘要翻译：提供包括碳纳米管的油墨和涂层。

3. 发明授权

US07947247B2 Method for preparing single walled carbon nanotubes from a metal layer 失效
标题翻译：从金属层制备单壁碳纳米管的方法
公开(公告)号：US07947247B2
公开(公告)日：2011-05-24
申请号：US11693203
申请日：2007-03-29
申请人： Howard Tennent , Hai-feng Zhang , Jun Ma
发明人： Howard Tennent , Hai-feng Zhang , Jun Ma
IPC分类号： B82B3/00
CPC分类号： D01F9/127 , B82Y30/00 , B82Y40/00 , C01B32/152 , C01B32/16 , C01B32/162 , C01B2202/02 , C01B2202/08 , C01B2202/36 , Y10S423/12 , Y10S977/842 , Y10T428/2982 , Y10T428/30
摘要： Methods of preparing single walled carbon nanotubes are provided. An arrangement comprising one or more layers of fullerene in contact with one side of a metal layer and a solid carbon source in contact with the other side of metal layer is prepared. The fullerene/metal layer/solid carbon source arrangement is then heated to a temperature below where the fullerenes sublime. Alternatively, a non-solid carbon source may be used in place of a solid carbon source or the metal layer may simply be saturated with carbon atoms. A multiplicity of single walled carbon nanotubes are grown on the fullerene side of the metal layer, wherein at least 80% of the single walled carbon nanotubes in said multiplicity have a diameter within ±5% of a single walled carbon nanotube diameter D present in said multiplicity, said diameter D being in the range between 0.6-2.2 nm.
摘要翻译：提供制备单壁碳纳米管的方法。制备包括与金属层的一侧接触的一层或多层富勒烯和与金属层的另一侧接触的固体碳源的布置。然后将富勒烯/金属层/固体碳源装置加热至低于富勒烯升华的温度。或者，可以使用非固体碳源代替固体碳源，或者金属层可以简单地用碳原子饱和。在金属层的富勒烯侧生长多个单壁碳纳米管，其中所述多重性中的至少80％的单壁碳纳米管的直径在所述多层中存在的单壁碳纳米管直径D的±5％以内多重性，所述直径D在0.6-2.2nm之间的范围内。

4. 发明申请

US20110002838A1 METHOD FOR PREPARING SINGLE WALLED CARBON NANOTUBES FROM A METAL LAYER 失效
标题翻译：从金属层制备单壁碳纳米管的方法
公开(公告)号：US20110002838A1
公开(公告)日：2011-01-06
申请号：US11693203
申请日：2007-03-29
申请人： Howard Tennent , Hai-feng Zhang , Jun Ma
发明人： Howard Tennent , Hai-feng Zhang , Jun Ma
IPC分类号： D01F9/12 , B32B9/00 , C01B31/02
CPC分类号： D01F9/127 , B82Y30/00 , B82Y40/00 , C01B32/152 , C01B32/16 , C01B32/162 , C01B2202/02 , C01B2202/08 , C01B2202/36 , Y10S423/12 , Y10S977/842 , Y10T428/2982 , Y10T428/30
摘要： Methods of preparing single walled carbon nanotubes are provided. An arrangement comprising one or more layers of fullerene in contact with one side of a metal layer and a solid carbon source in contact with the other side of metal layer is prepared. The fullerene/metal layer/solid carbon source arrangement is then heated to a temperature below where the fullerenes sublime. Alternatively, a non-solid carbon source may be used in place of a solid carbon source or the metal layer may simply be saturated with carbon atoms. A multiplicity of single walled carbon nanotubes are grown on the fullerene side of the metal layer, wherein at least 80% of the single walled carbon nanotubes in said multiplicity have a diameter within ±5% of a single walled carbon nanotube diameter D present in said multiplicity, said diameter D being in the range between 0.6-2.2 nm.
摘要翻译：提供制备单壁碳纳米管的方法。制备包括与金属层的一侧接触的一层或多层富勒烯和与金属层的另一侧接触的固体碳源的布置。然后将富勒烯/金属层/固体碳源装置加热至低于富勒烯升华的温度。或者，可以使用非固体碳源代替固体碳源，或者金属层可以简单地用碳原子饱和。在金属层的富勒烯侧生长多个单壁碳纳米管，其中所述多重性中的至少80％的单壁碳纳米管的直径在所述多层中存在的单壁碳纳米管直径D的±5％以内多重性，所述直径D在0.6-2.2nm之间的范围内。

5. 发明申请

US20100221173A1 METHOD FOR PREPARING SINGLE WALLED CARBON NANOTUBES FROM A METAL LAYER 失效
标题翻译：从金属层制备单壁碳纳米管的方法
公开(公告)号：US20100221173A1
公开(公告)日：2010-09-02
申请号：US11909614
申请日：2006-03-29
申请人： Howard Tennent , Hai-feng Zhang , Jun Ma
发明人： Howard Tennent , Hai-feng Zhang , Jun Ma
IPC分类号： D01F9/12 , B01J19/00
CPC分类号： D01F9/127 , B82Y30/00 , B82Y40/00 , C01B32/152 , C01B32/16 , Y10T428/2982
摘要： Methods of preparing single walled carbon nanotubes are provided. An arrangement comprising one or more layers of fullerene in contact with one side of a metal layer and a solid carbon source in contact with the other side of metal layer is prepared. The fullerene/metal layer/solid carbon source arrangement is then heated to a temperature below where the fullerenes sublime. Single walled carbon nanotubes are grown on the fullerene side of the metal layer.
摘要翻译：提供制备单壁碳纳米管的方法。制备包括与金属层的一侧接触的一层或多层富勒烯和与金属层的另一侧接触的固体碳源的布置。然后将富勒烯/金属层/固体碳源装置加热至低于富勒烯升华的温度。单壁碳纳米管在金属层的富勒烯侧生长。

6. 发明授权

US07413723B2 Methods of oxidizing multiwalled carbon nanotubes 失效
标题翻译：氧化多壁碳纳米管的方法
公开(公告)号：US07413723B2
公开(公告)日：2008-08-19
申请号：US11271422
申请日：2005-11-09
申请人： Chunming Niu , David Moy , Asif Chishti , Robert Hoch
发明人： Chunming Niu , David Moy , Asif Chishti , Robert Hoch
IPC分类号： B82B3/00
CPC分类号： H01G11/36 , B82Y30/00 , B82Y40/00 , C01B32/158 , C01B32/162 , C01B32/168 , C01B32/174 , C01B2202/06 , C01B2202/10 , C01B2202/28 , C01B2202/34 , C01B2202/36 , C04B35/6265 , C04B35/83 , C04B2235/5252 , C04B2235/5264 , C04B2235/5288 , D01F11/12 , D01F11/122 , D01F11/123 , H01M4/583 , H01M4/96 , Y02E60/13 , Y02P20/544 , Y10S977/847 , Y10T428/292 , Y10T428/30
摘要： Methods of oxidizing multiwalled carbon nanotubes are provided. The multiwalled carbon nanotubes are oxidized by contacting the carbon nanotubes with gas-phase oxidizing agents such as CO2, O2, steam, N2O, NO, NO2, O3, and ClO2. Near critical and supercritical water can also be used as oxidizing agents. The multiwalled carbon nanotubes oxidized according to methods of the invention can be used to prepare rigid porous structures which can be utilized to form electrodes for fabrication of improved electrochemical capacitors.
摘要翻译：提供氧化多壁碳纳米管的方法。多壁碳纳米管通过使碳纳米管与气相氧化剂如CO 2，O 2，O 2，N 2，N 2， O，NO，NO 2，O 3和ClO 2。近临界和超临界水也可用作氧化剂。根据本发明的方法氧化的多壁碳纳米管可用于制备可用于形成用于制造改进的电化学电容器的电极的刚性多孔结构。

7. 发明申请

US20080102020A1 Methods of Oxidizing Multiwalled Carbon Nanotubes 失效
标题翻译：氧化多壁碳纳米管的方法
公开(公告)号：US20080102020A1
公开(公告)日：2008-05-01
申请号：US11841449
申请日：2007-08-20
申请人： Chunming Niu , David Moy , Asif Chishti , Robert Hoch
发明人： Chunming Niu , David Moy , Asif Chishti , Robert Hoch
IPC分类号： D01F9/12
CPC分类号： H01G11/36 , B82Y30/00 , B82Y40/00 , C01B32/158 , C01B32/162 , C01B32/168 , C01B32/174 , C01B2202/06 , C01B2202/10 , C01B2202/28 , C01B2202/34 , C01B2202/36 , C04B35/6265 , C04B35/83 , C04B2235/5252 , C04B2235/5264 , C04B2235/5288 , D01F11/12 , D01F11/122 , D01F11/123 , H01M4/583 , H01M4/96 , Y02E60/13 , Y02P20/544 , Y10S977/847 , Y10T428/292 , Y10T428/30
摘要： Methods of oxidizing multiwalled carbon nanotubes are provided. The multiwalled carbon nanotubes are oxidized by contacting the carbon nanotubes with gas-phase oxidizing agents such as CO2, O2, steam, N2O, NO, NO2, O3, and ClO2. Near critical and supercritical water can also be used as oxidizing agents. The multiwalled carbon nanotubes oxidized according to methods of the invention can be used to prepare rigid porous structures which can be utilized to form electrodes for fabrication of improved electrochemical capacitors.
摘要翻译：提供氧化多壁碳纳米管的方法。多壁碳纳米管通过使碳纳米管与气相氧化剂如CO 2，O 2，O 2，N 2，N 2， O，NO，NO 2，O 3和ClO 2。近临界和超临界水也可用作氧化剂。根据本发明的方法氧化的多壁碳纳米管可用于制备可用于形成用于制造改进的电化学电容器的电极的刚性多孔结构。

8. 发明申请

US20080036123A1 CONDUCTIVE THERMOSETS BY EXTRUSION 有权
标题翻译：导电热敏电阻
公开(公告)号：US20080036123A1
公开(公告)日：2008-02-14
申请号：US11841596
申请日：2007-08-20
申请人： Alan Fischer , Timothy Jozokos , James Leacock , Andrew Rich
发明人： Alan Fischer , Timothy Jozokos , James Leacock , Andrew Rich
IPC分类号： B28B1/00
CPC分类号： B82Y30/00 , C08K3/041 , C08K2201/011 , C08L63/00
摘要： Methods of preparing conductive thermoset precursors containing carbon nanotubes is provided. Also provided is a method of preparing conductive thermosets containing carbon nanotubes. The carbon nanotubes may in individual form or in the form of aggregates having a macromorpology resembling the shape of a cotton candy, bird nest, combed yarn or open net. Preferred multiwalled carbon nanotubes have diameters no greater than 1 micron and preferred single walled carbon nanotubes have diameters less than 5 nm. Carbon nanotubes may be adequately dispersed in a thermoset precursor by using a extrusion process generally reserved for thermoplastics. The thermoset precursor may be a precursor for epoxy, phenolic, polyimide, urethane, polyester, vinyl ester or silicone. A preferred thermoset precursor is a bisphenol A derivative.
摘要翻译：提供了制备含有碳纳米管的导热热固性前体的方法。还提供了制备含有碳纳米管的导电性热固性材料的方法。碳纳米管可以具有类似于棉花糖，鸟巢，精梳纱或开放网的形状的大体积学的单体形式或聚集体形式。优选的多壁碳纳米管的直径不大于1微米，优选的单壁碳纳米管的直径小于5nm。碳纳米管可以通过使用通常为热塑性塑料保留的挤出工艺而充分地分散在热固性前体中。热固性前体可以是环氧树脂，酚醛树脂，聚酰亚胺，聚氨酯，聚酯，乙烯酯或硅树脂的前体。优选的热固性前体是双酚A衍生物。

9. 发明申请

US20070238826A1 Conductive thermosets by extrusion 有权
标题翻译：导电热固性材料通过挤出
公开(公告)号：US20070238826A1
公开(公告)日：2007-10-11
申请号：US11218209
申请日：2005-08-31
申请人： Alan Fischer , Timothy Jozokos , James Leacock , Andrew Rich
发明人： Alan Fischer , Timothy Jozokos , James Leacock , Andrew Rich
IPC分类号： C08K3/04 , C08K3/00
CPC分类号： B82Y30/00 , C08K3/041 , C08K2201/011 , C08L63/00
摘要： Methods of preparing conductive thermoset precursors containing carbon nanotubes is provided. Also provided is a method of preparing conductive thermosets containing carbon nanotubes. The carbon nanotubes may in individual form or in the form of aggregates having a macromorpology resembling the shape of a cotton candy, bird nest, combed yarn or open net. Preferred multiwalled carbon nanotubes have diameters no greater than 1 micron and preferred single walled carbon nanotubes have diameters less than 5 nm. Carbon nanotubes may be adequately dispersed in a thermoset precursor by using a extrusion process generally reserved for thermoplastics. The thermoset precursor may be a precursor for epoxy, phenolic, polyimide, urethane, polyester, vinyl ester or silicone. A preferred thermoset precursor is a bisphenol A derivative.
摘要翻译：提供了制备含有碳纳米管的导热热固性前体的方法。还提供了制备含有碳纳米管的导电性热固性材料的方法。碳纳米管可以具有类似于棉花糖，鸟巢，精梳纱或开放网的形状的大体积学的单体形式或聚集体形式。优选的多壁碳纳米管的直径不大于1微米，优选的单壁碳纳米管的直径小于5nm。碳纳米管可以通过使用通常为热塑性塑料保留的挤出工艺而充分地分散在热固性前体中。热固性前体可以是环氧树脂，酚醛树脂，聚酰亚胺，聚氨酯，聚酯，乙烯酯或硅树脂的前体。优选的热固性前体是双酚A衍生物。

10. 发明申请

US20070179050A1 Methods of Making Carbide And Oxycarbide Containing Catalysts 失效
标题翻译：制备含有催化剂的硬质合金和含氧化碳的方法
公开(公告)号：US20070179050A1
公开(公告)日：2007-08-02
申请号：US11608359
申请日：2006-12-08
申请人： Jun Ma , David Moy
发明人： Jun Ma , David Moy
IPC分类号： B01J21/18
CPC分类号： B01J27/22 , B01J21/185 , B01J23/28 , B01J37/08 , B82Y30/00 , B82Y40/00 , C01B32/168 , C01B32/18 , C01B32/90 , Y10S977/742 , Y10S977/745 , Y10S977/748 , Y10S977/749 , Y10S977/788 , Y10S977/81 , Y10S977/811 , Y10S977/847
摘要： Methods for forming compositions including carbide-containing nanorods and/or oxycarbide-containing nanorods and/or carbon nanotubes bearing carbides and oxycarbides. Rigid porous structures including oxycarbide-containing nanorods and/or carbide containing nanorods and/or carbon nanotubes bearing modified carbides and oxycarbides and methods of making the same are also provided. The compositions and rigid porous structures of the invention can be used either as catalyst and/or catalyst supports in fluid phase catalytic chemical reactions. Processes for making supported catalyst for selected fluid phase catalytic reactions are also provided.
摘要翻译：用于形成包含含碳纳米棒和/或含碳氧化物的纳米棒和/或含有碳化物和碳氧化物的碳纳米管的组合物的方法。还提供了包括含有碳氧化物的纳米棒和/或包含纳米棒和/或含有改性碳化物和碳氧化物的碳纳米管的刚性多孔结构及其制备方法。本发明的组合物和刚性多孔结构可用作流化相催化化学反应中的催化剂和/或催化剂载体。还提供了用于制备选择的流化相催化反应的负载型催化剂的方法。

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