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    • 84. 发明授权
    • Cold hearth refining
    • 冷炉精炼
    • US4961776A
    • 1990-10-09
    • US363160
    • 1989-06-08
    • Howard R. Harker
    • Howard R. Harker
    • B22D11/11C22B9/22C22B34/12
    • B22D11/11C22B34/1295C22B9/226C22B9/228
    • In the particular embodiments of the invention described in the specification, a hearth for melting and refining metal has a hearth bed with cooling pipes so that a skull of molten metal is formed and energy input devices are directionally controlled to permit the skull to form a barrier between a melting region where solid material is introduced into the hearth and a refining region where molten material is refined before being poured into a mold. In one embodiment, the barrier formed by the skull provides a dam with a narrow channel between the melting region and the refining region, and in another form, the barrier provided by the skull consists of spaced peninsulas extending from opposite sides of the hearth to provide a serpentine path between the melting region and the refining region.
    • 在本说明书中描述的本发明的特定实施例中,用于熔化和精炼金属的炉床具有带有冷却管的炉床,从而形成熔融金属的颅骨,并且能量输入装置被定向控制以允许颅骨形成屏障 在将固体材料引入炉床的熔融区域和熔融材料在被注入模具之前被精炼的精炼区域之间。 在一个实施例中,由颅骨形成的屏障提供了在熔化区域和精炼区域之间具有窄通道的坝,并且在另一种形式中,由颅骨提供的屏障由从炉膛的相对侧延伸的间隔开的半岛组成,以提供 在熔融区域和精炼区域之间的蛇形路径。
    • 85. 发明授权
    • Method of purifying refractory metal
    • 难熔金属的净化方法
    • US4749409A
    • 1988-06-07
    • US90914
    • 1987-08-31
    • Hiroshi Ishizuka
    • Hiroshi Ishizuka
    • C22B9/02C22B34/00C22B34/12C22B34/14
    • C22B34/14C22B34/00C22B34/1295C22B9/02C22B9/04Y02P10/234
    • A method of purifying refractory metal, comprising: providing a distillation space, said space comprising both a heatable portion and a condensation portion in communication with each other, and being closed but provided with gas inlet- and gas outlet openings, said degassing opening being located in the condensation portion, placing a mixed deposit of a refractory metal with magnesium metal and magnesium chloride in said heatable portion, heating said deposit under a subatmospheric pressure to temperatures high enough to cause evaporation of magnesium and magnesium chloride, degassing the space through the gas outlet opening, cooling magnesium and magnesium chloride to deposit in the condensation portion, starting introduction of an inert gas, through the gas inlet opening, at a timing where there is a steady, substantially decreased pressure of the thus forming vapor on the order of 10.sup.-2 Torr in the space, keeping supply of the inert gas while degassing through said openings, respectively, so that an increased but still subatmospheric pressure less than 1 Torr is maintained in the space.
    • 一种净化难熔金属的方法,包括:提供蒸馏空间,所述空间包括彼此连通的可加热部分和冷凝部分,并且被封闭,但设置有气体入口和气体出口,所述脱气开口位于 在冷凝部分中,将难熔金属与镁金属和氯化镁的混合沉积物放置在所述可加热部分中,将所述沉积物在低于大气压的压力下加热至高到足以引起镁和氯化镁蒸发的温度,使空气通过气体脱气 出口开口,冷却镁和氯化镁以沉积在冷凝部分中,在这样形成的蒸汽的压力稳定的基本上降低的时刻,通过气体入口开始引入惰性气体。 -2乇在空间中,保持惰性气体的供应,同时通过所述开口脱气 使得在该空间中保持小于1托的增加但仍然低于大气压的压力。