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81. 发明授权

US06746632B2 Morphology trapping and materials suitable for use therewith 失效
标题翻译：形态捕获和适合使用的材料
公开(公告)号：US06746632B2
公开(公告)日：2004-06-08
申请号：US10190208
申请日：2002-07-05
申请人： Michael R. Houston , Toshiaki Hino , David S. Soane
发明人： Michael R. Houston , Toshiaki Hino , David S. Soane
IPC分类号： B29D1100
CPC分类号： C08F287/00 , C08F265/04 , C08F291/00 , C08J3/28 , Y10S525/903 , Y10T428/31504 , Y10T428/31507 , Y10T428/31786 , Y10T428/31826 , Y10T428/31855
摘要： This invention is directed to a process for the rapid in-situ curing of polymerizable materials to provide macromolecular networks and articles of manufacture that are “morphology-trapped”; that is, they exhibit a fixed phase morphology and/or molecular orientation that is locked in by the curing step. The process includes the steps of mixing together a dead polymer, a reactive plasticizer and an initiator to give a polymerizable composition; further processing the mixture in order to achieve a desired phase morphology and/or molecular orientation of the polymeric constituents; shaping the polymerizable composition into a desired geometry; and exposing the polymerizable composition to a source of polymerizing energy, without mixing, to give a final product with the desired phase morphology and/or molecular orientation locked in place. The phase morphology and molecular orientation present just prior to cure of the polymerizable composition is subsequently trapped or locked in place by the curing step so that further changes in morphology are hindered or prevented.
摘要翻译：本发明涉及一种快速原位固化可聚合材料以提供“形态学被捕”的大分子网络和制品的方法。也就是说，它们表现出通过固化步骤锁定的固定相形态和/或分子取向。该方法包括将死聚合物，活性增塑剂和引发剂混合在一起以产生可聚合组合物的步骤; 进一步处理混合物以实现聚合物组分的期望相形态和/或分子取向; 将可聚合组合物成型为所需的几何形状; 并将可聚合组合物暴露于聚合能源，而不混合，得到具有所需相形态和/或分子取向锁定在适当位置的最终产物。在固化可聚合组合物之前存在的相态和分子取向随后通过固化步骤被捕获或锁定在适当位置，从而妨碍或防止形态的进一步变化。

82. 发明授权

US06570714B2 Precision composite article 失效
公开(公告)号：US06570714B2
公开(公告)日：2003-05-27
申请号：US10004455
申请日：2001-12-05
申请人： David S. Soane , Michael R. Houston , Toshiaki Hino
发明人： David S. Soane , Michael R. Houston , Toshiaki Hino
IPC分类号： G02B2500
CPC分类号： B32B27/00 , G02B1/04 , G02B1/041 , Y10T428/31616 , Y10T428/31645 , Y10T428/31855 , Y10T428/31909 , Y10T428/31935
摘要： The invention is directed to a method for making composite articles, including optical lenses, which includes the steps of obtaining a substrate; placing a semi-solid-like polymerizable composition in contact with at least one of the front or back surface of the substrate; compressing or heating the resulting semi-solid/substrate sandwich between two mold halves, where the mold contacting the semi-solid polymerizable material has a desired surface geometry; and exposing the semi-solid/substrate sandwich to a source of polymerizing energy. The resulting composite article has the desirable characteristics of the substrate but is also easily fabricated as a result of the semi-solid molding process. Also included within the present invention is a composite article comprising a substrate portion and at least one layer of a cured resin bonded to the substrate portion, the cured resin comprising an interpenetrating crosslinked polymer network of reactive plasticizer within a dead polymer. In one embodiment, the reactive plasticizer polymer network is further crosslinked to the dead polymer. The composite article exhibits dimensional stability and high-fidelity replication of an internal mold cavity.

83. 发明授权

US06413400B1 Polycarbonate electrophoretic devices 有权
标题翻译：聚碳酸酯电泳装置
公开(公告)号：US06413400B1
公开(公告)日：2002-07-02
申请号：US09479503
申请日：2000-01-07
申请人： David S. Soane , Zoya M. Soane
发明人： David S. Soane , Zoya M. Soane
IPC分类号： G01N2726
CPC分类号： B01D57/02 , B01F13/0059 , B01F13/0076 , B01J19/0093 , B01J2219/00853 , B01J2219/00912 , B82Y10/00 , B82Y40/00 , C07K1/26 , G01N27/44752 , G01N27/44773 , G03F7/0002
摘要： Devices and methods are disclosed for moving charged molecules through a medium by the application of a plurality of electrical fields of sufficient strength and applied for sufficient amounts of time so as to move the charged molecules through the medium. The devices although preferably small in size, preferably generate large numbers (100 or more) of electrical fields to a movement area which preferably contains a liquid buffered or gel medium. Mixtures of charged molecules are pulled through the gel by the force of the electrical fields. The fields are preferably activated simultaneously or sequentially one after another at various speeds to create complex force field distributions or moving field waves along the separation medium. Charged molecules capable of moving quickly through the gel will be moved along by the faster moving field waves and be separated from slower moving molecules. The fields can be activated by computer software and can be used to move molecules away from and toward each other to obtain rapid and complex chemical synthesis, sequencing or reaction protocols.
摘要翻译：公开的装置和方法用于通过施加足够强度的多个电场来移动带电分子通过介质，并施加足够的时间，以使带电分子移动通过介质。尽管尺寸优选小的装置优选地对于优选含有液体缓冲或凝胶介质的运动区域产生大量（100个或更多个）电场。带电分子的混合物被电场的力拉入凝胶。这些场优选地以各种速度一个接一个地同时或顺序地被激活，以产生沿着分离介质的复数的力场分布或移动的场波。能够快速移动通过凝胶的带电分子将沿着更快的移动场波移动并与较慢的移动分子分离。这些领域可以通过计算机软件激活，并且可以用于将分子移开和相互移动，以获得快速和复杂的化学合成，测序或反应方案。

84. 发明授权

US06387492B2 Hollow polymeric fibers 失效
标题翻译：中空聚合纤维
公开(公告)号：US06387492B2
公开(公告)日：2002-05-14
申请号：US09840317
申请日：2001-04-23
申请人： David S. Soane , Michael R. Houston
发明人： David S. Soane , Michael R. Houston
IPC分类号： D01F600
CPC分类号： D01D5/247 , C08J9/04 , C08J2201/03 , D01F1/08 , Y10T428/249921 , Y10T428/249962 , Y10T428/249971 , Y10T428/249972 , Y10T428/2913 , Y10T428/2927 , Y10T428/2935 , Y10T428/2975
摘要： The present invention is directed to thermo-expandable fibers and to the expanded hollow fibers or microtubes, microcellular foam or foamed composite material that results upon heating the expandable fibers. The thermo-expandable fiber of the present invention is characterized by having a polymeric wall surrounding one or more pockets or particles of blowing agent or propellant within the fiber. The polymeric wall may have reactive functional groups on its surface to give a fusible fiber. When the expandable fibers are heated, they expand to form hollow fibers or microtubes comprising polymeric shells surrounding one or more internal gaseous voids, and when the fibers are expanded while in contact with each other, a microcellular foam may be formed. The foam consists of a plurality of hollow fibers fused together, optionally aided by functional groups present on the surface of the heated fibers that act to crosslink the material. When expandable microspheres are mixed with a matrix, which can optionally react with functional groups on the fiber surface, and the resulting combination is heated, the fibers expand to give a foamed composite material in which the hollow fibers or microtubes may optionally be fused or chemically crosslinked to the matrix.
摘要翻译：本发明涉及热膨胀纤维和膨胀的中空纤维或微管，微孔泡沫或泡沫复合材料，其导致加热可膨胀纤维。本发明的热膨胀性纤维的特征在于，在纤维内具有包围发泡剂或推进剂的一个或多个口袋或颗粒的聚合物壁。聚合物壁在其表面上可以具有反应性官能团以得到可熔纤维。当可膨胀纤维被加热时，它们膨胀以形成包含围绕一个或多个内部气体空隙的聚合物壳的中空纤维或微管，并且当纤维在彼此接触时膨胀时，可以形成微孔泡沫。泡沫由多个融合在一起的中空纤维组成，任选由加热纤维表面上存在的用于交联材料的官能团辅助。当可膨胀微球与可以任选地与纤维表面上的官能团反应的基质混合，并且所得到的组合被加热时，纤维膨胀以产生泡沫复合材料，其中中空纤维或微管可以任选地熔融或化学与基质交联。

85. 发明授权

US06306272B1 Method and device for performing chemical reactions 有权
标题翻译：用于进行化学反应的方法和装置
公开(公告)号：US06306272B1
公开(公告)日：2001-10-23
申请号：US09172187
申请日：1998-10-13
申请人： David S. Soane , Zoya M. Soane
发明人： David S. Soane , Zoya M. Soane
IPC分类号： G01N2726
CPC分类号： B01D57/02 , B01F13/0059 , B01F13/0076 , B01J19/0093 , B01J2219/00853 , B01J2219/00912 , B82Y10/00 , B82Y40/00 , C07K1/26 , G01N27/44752 , G01N27/44773 , G03F7/0002
摘要： Devices and methods are disclosed for moving charged molecules through a medium by the application of a plurality of electrical fields of sufficient strength and applied for sufficient amounts of time so as to move the charged molecules through the medium. The devices although preferably small in size, preferably generate large numbers (100 or more) of electrical fields to a movement area which preferably contains a liquid buffered or gel medium. Mixtures of charged molecules are pulled through the gel by the force of the electrical fields. The fields are preferably activated simultaneously or sequentially one after another at various speeds to create complex force field distributions or moving field waves along the separation medium. Charged molecules capable of moving quickly through the gel will be moved along by the faster moving field waves and be separated from slower moving molecules. The fields can be activated by computer software and can be used to move molecules away from and toward each other to obtain rapid and complex chemical synthesis, sequencing or reaction protocols.
摘要翻译：公开的装置和方法用于通过施加足够强度的多个电场来移动带电分子通过介质，并施加足够的时间，以使带电分子移动通过介质。尽管尺寸优选小的装置优选地对于优选含有液体缓冲或凝胶介质的运动区域产生大量（100个或更多个）电场。带电分子的混合物被电场的力拉入凝胶。这些场优选地以各种速度一个接一个地同时或顺序地被激活，以产生沿着分离介质的复数的力场分布或移动的场波。能够快速移动通过凝胶的带电分子将沿着更快的移动场波移动并与较慢的移动分子分离。这些领域可以通过计算机软件激活，并且可以用于将分子移开和相互移动，以获得快速和复杂的化学合成，测序或反应方案。

86. 发明授权

US06176962B1 Methods for fabricating enclosed microchannel structures 失效
标题翻译：封闭微通道结构的制造方法
公开(公告)号：US06176962B1
公开(公告)日：2001-01-23
申请号：US08878437
申请日：1997-06-18
申请人： David S. Soane , Zoya M. Soane , Herbert H. Hooper , M. Goretty Alonso Amigo
发明人： David S. Soane , Zoya M. Soane , Herbert H. Hooper , M. Goretty Alonso Amigo
IPC分类号： B32B3100
CPC分类号： B01D57/02 , B01F13/0059 , B01F13/0076 , B01J19/0093 , B01L3/502707 , B01L2200/0689 , B01L2200/12 , B01L2300/0816 , B01L2300/0887 , B01L2400/0415 , B29C65/02 , B29C65/1403 , B29C65/1406 , B29C65/1412 , B29C65/1425 , B29C65/48 , B29C65/4815 , B29C65/483 , B29C65/4835 , B29C65/4845 , B29C65/485 , B29C65/4865 , B29C65/524 , B29C66/20 , B29C66/5346 , B29C66/54 , B29C66/71 , B29C66/73117 , B29L2031/756 , B29L2031/757 , B82Y10/00 , B82Y40/00 , C07K1/26 , G01N27/44704 , G01N27/44743 , G01N27/44752 , G01N27/44773 , G01N27/44791 , G03F7/0002 , B29K2083/00 , B29K2067/003 , B29K2033/12 , B29K2033/08 , B29K2023/06
摘要： Methods are provided for the fabrication of polymeric microchannel structures having enclosed microchannels of capillary dimension. The microchannel structures are constructed of a base plate and a cover, sealed together. Microchannel structures having walls of a plastic material are formed in a generally planar surface of at least the base plate. The cover has at least one generally planar surface, and the microchannel structures are enclosed by bonding the planar surfaces of the cover and the base plate together. In some embodiments the surfaces of the cover and base plate are both of plastic material, and are directly thermally bonded. In some embodiments a bonding material is applied to one of the surface prior to bringing the surfaces together. Suitable bonding materials are disclosed.
摘要翻译：提供了用于制造具有毛细管尺寸的封闭微通道的聚合物微通道结构的方法。微通道结构由基板和盖构成，密封在一起。具有塑料材料壁的微通道结构形成在至少基板的大致平坦的表面上。盖具有至少一个大致平坦的表面，并且通过将盖和基板的平面表面粘合在一起来封闭微通道结构。在一些实施例中，盖和基板的表面都是塑料材料，并且是直接热粘结的。在一些实施例中，在使表面在一起之前，将粘合材料施加到该表面之一。公开了合适的粘合材料。

87. 发明授权

US6093296A Method and device for moving molecules by the application of a plurality of electrical fields 失效
标题翻译：通过施加多个电场来移动分子的方法和装置
公开(公告)号：US6093296A
公开(公告)日：2000-07-25
申请号：US974372
申请日：1997-11-19
申请人： David S. Soane , Zoya M. Soane
发明人： David S. Soane , Zoya M. Soane
IPC分类号： B01D57/02 , B01F13/00 , B01J19/00 , C07K1/26 , G01N27/447 , G03F7/00 , G01N27/26
CPC分类号： B01D57/02 , B01F13/0076 , B01J19/0093 , B82Y10/00 , B82Y40/00 , C07K1/26 , G01N27/44752 , G01N27/44773 , G03F7/0002 , B01F13/0059 , B01J2219/00853 , B01J2219/00912
摘要： Devices and methods are disclosed for moving charged molecules through a medium by the application of a plurality of electrical fields of sufficient strength and applied for sufficient amounts of time so as to move the charged molecules through the medium. The devices although preferably small in size, preferably generate large numbers (100 or more) of electrical fields to a movement area which preferably contains a liquid buffered or gel medium. Mixtures of charged molecules are pulled through the gel by the force of the electrical fields. The fields are preferably activated simultaneously or sequentially one after another at various speeds to create complex force field distributions or moving field waves along the separation medium. Charged molecules capable of moving quickly through the gel will be moved along by the faster moving field waves and be separated from slower moving molecules. The fields can be activated by computer software and can be used to move molecules away from and toward each other to obtain rapid and complex chemical synthesis, sequencing or reaction protocols.
摘要翻译：公开的装置和方法用于通过施加足够强度的多个电场来移动带电分子通过介质，并施加足够的时间，以使带电分子移动通过介质。尽管尺寸优选小的装置优选地对于优选含有液体缓冲或凝胶介质的运动区域产生大量（100个或更多个）电场。带电分子的混合物被电场的力拉入凝胶。这些场优选地以各种速度一个接一个地同时或顺序地被激活，以产生沿着分离介质的复数的力场分布或移动的场波。能够快速移动通过凝胶的带电分子将沿着更快的移动场波移动并与较慢的移动分子分离。这些领域可以通过计算机软件激活，并且可以用于将分子移开和相互移动，以获得快速和复杂的化学合成，测序或反应方案。

88. 发明授权

US5750015A Method and device for moving molecules by the application of a plurality of electrical fields 失效
公开(公告)号：US5750015A
公开(公告)日：1998-05-12
申请号：US615642
申请日：1996-03-13
申请人： David S. Soane , Zoya M. Soane
发明人： David S. Soane , Zoya M. Soane
IPC分类号： B01D57/02 , B01F13/00 , B01J19/00 , C07K1/26 , G01N27/447 , G03F7/00 , G01N27/26
CPC分类号： B01D57/02 , B01F13/0076 , B01J19/0093 , B82Y10/00 , B82Y40/00 , C07K1/26 , G01N27/44752 , G01N27/44773 , G03F7/0002 , B01F13/0059 , B01J2219/00853 , B01J2219/00912
摘要： Devices and methods are disclosed for moving charged molecules through a medium by the application of a plurality of electrical fields of sufficient strength and applied for sufficient amounts of time so as to move the charged molecules through the medium. The devices although preferably small in size, preferably generate large numbers (100 or more) of electrical fields to a movement area which preferably contains a liquid buffered or gel medium. Mixtures of charged molecules are pulled through the gel by the force of the electrical fields. The fields are preferably activated simultaneously or sequentially one after another at various speeds to create complex force field distributions or moving field waves along the separation medium. Charged molecules capable of moving quickly through the gel will be moved along by the faster moving field waves and be separated from slower moving molecules. The fields can be activated by computer software and can be used to move molecules away from and toward each other to obtain rapid and complex chemical synthesis, sequencing or reaction protocols.

89. 发明授权

US5667735A Opthalmic mold coatings 失效
标题翻译： Opthalmic模具涂料
公开(公告)号：US5667735A
公开(公告)日：1997-09-16
申请号：US633220
申请日：1996-04-16
申请人： Young C. Bae , Thomas B. Ottoboni , Kwan Chan , Thai Minh Nguyen , Fredric J. Lim , David S. Soane
发明人： Young C. Bae , Thomas B. Ottoboni , Kwan Chan , Thai Minh Nguyen , Fredric J. Lim , David S. Soane
IPC分类号： B29D11/00
CPC分类号： B29D11/00432
摘要： A method is provided for applying a coating to an ophthalmic device by applying a coating to a face of the mold used to make the device and partially curing the coating, or, if the viscosity is sufficiently high, leaving the coating uncured. Then the liquid used to form the lens is poured into the mold and the liquid and coating are concurrently cured.
摘要翻译：提供了一种通过向用于制造该装置的模具的表面施加涂层并部分固化涂层而将涂层施加到眼科装置的方法，或者如果粘度足够高，则使涂层未固化。然后将用于形成透镜的液体倒入模具中，并且液体和涂层同时固化。

90. 发明授权

US5545367A Rapid prototype three dimensional stereolithography 失效
标题翻译：快速原型三维立体光刻
公开(公告)号：US5545367A
公开(公告)日：1996-08-13
申请号：US68692
申请日：1993-05-27
申请人： Young C. Bae , David S. Soane , Charles Crocker
发明人： Young C. Bae , David S. Soane , Charles Crocker
IPC分类号： B29C67/00 , B29C35/08 , B29C41/08
CPC分类号： B29C67/0066
摘要： Methods and apparatus are disclosed for the production of high precision large scale, micro and mini structures using three dimensional stereolithography. The objects formed using these methods have minimal stress between layers and low curl distortion. The objects also have low warpage because no post-cure treatment is necessary. The methods include the use of elevated pressure, elevated temperature, or sequential polymerization of polymer precursor fluid, or a combination of these, in the three dimensional stereolithographic process.
摘要翻译：公开了使用三维立体光刻技术生产高精度大规模，微型和微型结构的方法和装置。使用这些方法形成的物体在层之间具有最小的应力和低卷曲变形。这些物体也具有低翘曲，因为不需要后固化治疗。这些方法包括在三维立体光刻工艺中使用高压，高温或聚合物前体流体的顺序聚合，或它们的组合。

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