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81. 发明授权

US5843862A Process for manufacturing an absorbent composition 失效
标题翻译：制造吸收组合物的方法
公开(公告)号：US5843862A
公开(公告)日：1998-12-01
申请号：US736949
申请日：1996-10-25
申请人： Alakananda Bhattacharyya
发明人： Alakananda Bhattacharyya
IPC分类号： B01J20/04 , B01J20/06 , C01G31/00 , C10G25/00 , B01J20/10 , B01J20/00
CPC分类号： B01J20/06 , B01J20/041 , B01J20/28007 , B01J20/3078 , C01G31/006 , C10G25/003 , B01J2220/42 , C01P2002/22 , C01P2002/52 , C01P2002/72 , C01P2002/88 , C01P2006/12 , C01P2006/14 , C01P2006/16 , C01P2006/80 , C01P2006/82
摘要： A process for manufacturing a collapsed composition is described in which the manufactured composition is substantially composed of microcrystallites collectively of the formula: ##EQU1## where M.sup.2+ is a divalent metal, M.sup.3+ is a trivalent metal, and T is vanadium, tungsten, or molybdenum. The microcrystallites are so small as to be undetectable through conventional x-ray diffraction techniques, yet high resolution electron microscopy reveals that a substantial portion of the microcrystallites are composed of a solid solution having aluminum oxide molecularly dispersed in a divalent metal monoxide crystal structure. Another portion of the microcrystallites are constituted by a spinel phase. The collapsed composition is suitable as a sulfur oxide absorbent, having comparatively high capacity and comparatively fast absorption and desorption rates, and is also suitable as a nitrogen oxide reduction catalyst. The collapsed composition may be produced by heat treating a layered mixed hydroxide clay having interlayer anions in monometalate form. The reagents for the manufacturing process are relatively salt-free, as compared to reagents utilized in previous manufacturing processes.
摘要翻译：描述了制造塌陷组合物的方法，其中制造的组合物基本上由以下通式组成的微晶体：M2 + 2m Al2-p Mp3 + TrO7 + rxs其中M2 +是二价金属，M3 +是三价金属，T 是钒，钨或钼。微晶体很小，通过常规的x射线衍射技术是不可检测的，但是高分辨率电子显微镜显示，大部分微晶体由分子内分散在二价金属氧化物晶体结构中的氧化铝的固溶体构成。微晶的另一部分由尖晶石相构成。塌陷组合物适合作为硫氧化物吸收剂，具有相对较高的容量和相对较快的吸收和解吸速率，并且也适合作为氮氧化物还原催化剂。塌陷组合物可以通过以单金属盐形式对具有中间阴离子的层状混合氢氧化物粘土进行热处理来制备。与以前的制造方法中使用的试剂相比，制造方法的试剂相对不含盐。

82. 发明授权

US5767040A Catalyst prepared from nickel-containing hydrotalcite-like precursor compound 失效
标题翻译：由含镍水滑石前体化合物制备的催化剂
公开(公告)号：US5767040A
公开(公告)日：1998-06-16
申请号：US445699
申请日：1995-05-22
申请人： Alakananda Bhattacharyya , Wen-Dong Chang , Mark S. Kleefisch , Carl A. Udovich
发明人： Alakananda Bhattacharyya , Wen-Dong Chang , Mark S. Kleefisch , Carl A. Udovich
IPC分类号： B01J23/00 , B01J23/74 , B01J23/755 , B01J27/232 , B01J37/08 , C01B3/38 , C01B3/40 , C01G53/00 , B01J23/58
CPC分类号： B82Y30/00 , B01J23/005 , B01J23/007 , B01J23/755 , B01J27/232 , B01J37/08 , B01J37/088 , C01B3/386 , C01B3/40 , C01G53/00 , C01G53/006 , C01B2203/0233 , C01B2203/0238 , C01B2203/0261 , C01B2203/1041 , C01B2203/1052 , C01B2203/1064 , C01B2203/1076 , C01B2203/1082 , C01B2203/1088 , C01B2203/1241 , C01P2002/22 , C01P2002/32 , C01P2002/72 , C01P2002/77 , C01P2002/78 , C01P2004/04 , C01P2004/62 , C01P2004/64 , C01P2004/80 , Y02P20/142 , Y02P20/52
摘要： A method and nickel-containing catalyst are disclosed for preparing synthesis gas by the reforming of a hydrocarbyl compound using an oxygen-containing compound.
摘要翻译：公开了通过使用含氧化合物重整烃基化合物来制备合成气的方法和含镍催化剂。

83. 发明授权

US5426083A Absorbent and process for removing sulfur oxides from a gaseous mixture 失效
标题翻译：用于从气体混合物中除去硫氧化物的吸收剂和方法
公开(公告)号：US5426083A
公开(公告)日：1995-06-20
申请号：US252175
申请日：1994-06-01
申请人： Alakananda Bhattacharyya , Michael J. Foral , William J. Reagan
发明人： Alakananda Bhattacharyya , Michael J. Foral , William J. Reagan
IPC分类号： C01G49/00 , B01J20/04 , B01J20/06 , B01J20/08 , C01B13/14 , C01B17/04 , C01F7/00 , C01G31/00 , C01G37/00 , C01G39/00 , C01G41/00 , C01G51/00 , C10G11/02 , C10G11/18 , C10G25/00
CPC分类号： C10G25/003 , B01J20/041 , B01J20/06 , B01J20/08 , B01J20/28007 , B01J20/3078 , C01B13/14 , C01F7/005 , C01G31/006 , B01J2220/42 , C01P2002/22 , C01P2002/32 , C01P2002/52 , C01P2002/72 , C01P2002/88 , C01P2006/12 , C01P2006/14 , C01P2006/16 , C01P2006/80 , C01P2006/82
摘要： A collapsed composition is described which is substantially composed of microcrystallites collectively of the formula:M.sub.2m.sup.2+ Al.sub.2-p M.sub.p.sup.3+ T.sub.r O.sub.7+r.swhere M.sup.2+ is a divalent metal, M.sup.3+ is a trivalent metal, and T is vanadium, tungsten, or molybdenum.The microcrystallites are so small as to be undetectable through conventional x-ray diffraction techniques, yet high resolution electron microscopy reveals that a substantial portion of the microcrystallites are composed of a solid solution having aluminum oxide molecularly dispersed in a divalent metal monoxide crystal structure. Another portion of the microcrystallites are constituted by a spinel phase. The collapsed composition is suitable as a sulfur oxide absorbent, having comparatively high capacity and comparatively fast absorption and desorption rates. The collapsed composition may be produced by heat treating a layered mixed hydroxide clay having interlayer anions in monometalate form.A sulfur oxide separation process is also presented. The process can be operated cyclicly and integrated with any of several well-known fluidized bed catalytic cracking processes.
摘要翻译：描述了一种塌陷的组合物，其基本上由微晶体组成，其共同具有下式：M2m2 + Al2-pMp3 + TrO7 + r.s，其中M2 +是二价金属，M3 +是三价金属，T是钒，钨或钼。微晶体很小，通过常规的x射线衍射技术是不可检测的，但是高分辨率电子显微镜显示，大部分微晶体由分子内分散在二价金属氧化物晶体结构中的氧化铝的固溶体构成。微晶的另一部分由尖晶石相构成。塌陷组合物适合作为硫氧化物吸收剂，具有相对较高的容量和较快的吸收和解吸速率。塌陷组合物可以通过以单金属盐形式对具有中间阴离子的层状混合氢氧化物粘土进行热处理来制备。还提出了硫氧化物分离过程。该方法可以循环操作并与几种众所周知的流化床催化裂化方法中的任何一种结合。

84. 发明授权

US08933265B2 Process for oxidizing alkyl aromatic compounds 有权
公开(公告)号：US08933265B2
公开(公告)日：2015-01-13
申请号：US13155663
申请日：2011-06-08
申请人： Alakananda Bhattacharyya , Joel T. Walenga
发明人： Alakananda Bhattacharyya , Joel T. Walenga
IPC分类号： C07C51/16 , C07C51/265
CPC分类号： C07C51/265 , C07C51/42 , C07C63/06 , C07C63/16 , C07C63/26
摘要： A process and a mixture for oxidizing an alkyl-aromatic compound comprises forming a mixture comprising the alkyl-aromatic compound, a solvent, a bromine source, a catalyst, and ammonium acetate; and contacting the mixture with an oxidizing agent at oxidizing conditions to produce an oxidation product comprising at least one of an aromatic aldehyde, an aromatic alcohol, an aromatic ketone, and an aromatic carboxylic acid. The solvent comprises a carboxylic acid having from 1 to 7 carbon atoms; and the catalyst comprises at least one of cobalt, titanium, manganese, chromium, copper, nickel, vanadium, iron, molybdenum, tin, cerium, and zirconium.

85. 发明申请

US20120004450A1 PROCESS FOR PRODUCING TEREPHTHALIC ACID 有权
标题翻译：生产过敏性酸的方法
公开(公告)号：US20120004450A1
公开(公告)日：2012-01-05
申请号：US13155553
申请日：2011-06-08
申请人： Alakananda Bhattacharyya , Joseph A. Kocal , Joel T. Walenga , Nikolay Y. Adonin , Nina I. Kuznetsova , Bair S. Bal'zhinimaev
发明人： Alakananda Bhattacharyya , Joseph A. Kocal , Joel T. Walenga , Nikolay Y. Adonin , Nina I. Kuznetsova , Bair S. Bal'zhinimaev
IPC分类号： C07C51/265 , C07C51/16
CPC分类号： C07C51/265 , C07C51/42 , Y02P20/52 , Y02P20/542 , C07C63/26
摘要： A solid terephthalic acid composition and a process for producing terephthalic acid from para-xylene. The process comprises forming a mixture comprising the para-xylene, a solvent, a bromine source, and a catalyst; and oxidizing the para-xylene by contacting the mixture with an oxidizing agent at oxidizing conditions to produce a solid oxidation product comprising terephthalic acid, para-toluic acid, 4-carboxybenzaldehyde. The solvent comprises a carboxylic acid having from 1 to 7 carbon atoms and an dialkyl imidazolium ionic liquid; and the catalyst comprises at least one of cobalt, titanium, manganese, chromium, copper, nickel, vanadium, iron, molybdenum, tin, cerium, and zirconium. The solid terephthalic acid composition comprises, less than about 4,000 ppm-wt 4-carboxybenzaldehyde content, and more than about 2,000 ppm-wt a para-toluic acid.
摘要翻译：固体对苯二甲酸组合物和由对二甲苯生产对苯二甲酸的方法。该方法包括形成包含对二甲苯，溶剂，溴源和催化剂的混合物; 并通过在氧化条件下将氧化剂与氧化剂接触来氧化对二甲苯以产生包含对苯二甲酸，对甲苯甲酸，4-羧基苯甲醛的固体氧化产物。溶剂包括具有1至7个碳原子的羧酸和二烷基咪唑鎓离子液体; 催化剂包括钴，钛，锰，铬，铜，镍，钒，铁，钼，锡，铈和锆中的至少一种。固体对苯二甲酸组合物包含小于约4,000ppm重量的4-羧基苯甲醛含量和大于约2,000ppm重量的对甲苯甲酸。

86. 发明申请

US20120004448A1 PROCESS FOR OXIDIZING ALKYL AROMATIC COMPOUNDS 有权
标题翻译：用于氧化烷基芳族化合物的方法
公开(公告)号：US20120004448A1
公开(公告)日：2012-01-05
申请号：US13155663
申请日：2011-06-08
申请人： Alakananda Bhattacharyya , Joel T. Walenga
发明人： Alakananda Bhattacharyya , Joel T. Walenga
IPC分类号： C07C51/255
CPC分类号： C07C51/265 , C07C51/42 , C07C63/06 , C07C63/16 , C07C63/26
摘要： A process and a mixture for oxidizing an alkyl-aromatic compound comprises forming a mixture comprising the alkyl-aromatic compound, a solvent, a bromine source, a catalyst, and ammonium acetate; and contacting the mixture with an oxidizing agent at oxidizing conditions to produce an oxidation product comprising at least one of an aromatic aldehyde, an aromatic alcohol, an aromatic ketone, and an aromatic carboxylic acid. The solvent comprises a carboxylic acid having from 1 to 7 carbon atoms; and the catalyst comprises at least one of cobalt, titanium, manganese, chromium, copper, nickel, vanadium, iron, molybdenum, tin, cerium, and zirconium.
摘要翻译：用于氧化烷基 - 芳族化合物的方法和混合物包括形成包含烷基 - 芳族化合物，溶剂，溴源，催化剂和乙酸铵的混合物; 以及在氧化条件下使所述混合物与氧化剂接触以产生包含芳族醛，芳族醇，芳族酮和芳族羧酸中的至少一种的氧化产物。溶剂包括具有1至7个碳原子的羧酸; 催化剂包括钴，钛，锰，铬，铜，镍，钒，铁，钼，锡，铈和锆中的至少一种。

87. 发明申请

US20060004212A1 Catalysts for maleic acid hydrogenation to 1,4-butanediol 有权
标题翻译：用于马来酸氢化成1,4-丁二醇的催化剂
公开(公告)号：US20060004212A1
公开(公告)日：2006-01-05
申请号：US10883106
申请日：2004-07-01
申请人： Alakananda Bhattacharyya , Maynard Manila
发明人： Alakananda Bhattacharyya , Maynard Manila
IPC分类号： C07D37/04 , C07D37/33
CPC分类号： C07D315/00 , B01J21/063 , B01J21/18 , B01J23/40 , B01J23/44 , B01J23/6567 , B01J23/8986 , B01J35/002 , B01J37/0205 , C07C29/149 , C07C29/172 , C07D307/08 , C07C31/207
摘要： This invention relates to a process for catalytically hydrogenating a hydrogenatable precursor in contact with a hydrogen-containing gas and a hydrogenation catalyst comprising one or more active hydrogenation catalyst components on a support comprising titanium dioxide in the rutile crystalline phase to produce 1,4-butanediol and, optionally, gamma-butyrolactone and/or tetrahydrofuran.
摘要翻译：本发明涉及一种催化氢化与含氢气体接触的可氢化前体和在包含金红石结晶相中二氧化钛的载体上包含一种或多种活性氢化催化剂组分的氢化催化剂，以产生1,4-丁二醇和任选的γ-丁内酯和/或四氢呋喃。

88. 发明授权

US06953488B2 Preparing synthesis gas using hydrotalcite-derived nickel catalysts 失效
标题翻译：使用水滑石衍生的镍催化剂制备合成气
公开(公告)号：US06953488B2
公开(公告)日：2005-10-11
申请号：US10388154
申请日：2003-03-13
申请人： Alakananda Bhattacharyya , Wen-Dong Chang
发明人： Alakananda Bhattacharyya , Wen-Dong Chang
IPC分类号： B01J23/00 , B01J23/755 , B01J35/02 , B01J37/08 , C01B3/40 , C10G11/02 , C10G57/00 , C01B3/32
CPC分类号： C10G57/00 , B01J23/007 , C01B3/40 , C01B2203/1011 , C01B2203/1041 , C01B2203/1047 , C01B2203/1052 , C01B2203/1064 , C01B2203/1076 , C01B2203/1082 , Y02P20/52
摘要： There is provided a process for preparation of synthesis gas from feedstocks containing methane and/or higher hydrocarbons having from about 2 to about 12 carbon atoms by an initial catalytic treatment of feedstock to provide a methane-containing gaseous mixture substantially free of compounds having 2 or more carbon atoms, and reforming the gaseous mixture at elevated temperatures using nickel-containing catalytic materials that are unusually active under mild conditions of conversion and resistant to deactivation. The process consists fundamentally in converting the higher hydrocarbon compounds to form the methane-containing gaseous mixture in an initial conversion zone containing a catalyst while controlling temperatures within the initial conversion zone to temperatures in a range downward from about 500° C. to about 300° C., and reforming the methane-containing gaseous mixture in a subsequent zone to form synthesis gas.
摘要翻译：提供了一种通过原料的初始催化处理从含有甲烷和/或具有约2至约12个碳原子的甲烷和/或高级烃的原料制备合成气的方法，以提供基本上不含化合物的含甲烷的气体混合物，其具有2或更多的碳原子，并且在升高的温度下使用在温和的转化条件下具有异常活性且耐失活的含镍催化材料重整气态混合物。该方法基本上是在含有催化剂的初始转化区中转化高级烃化合物形成含甲烷的气态混合物，同时将初始转化区内的温度控制在约500℃至约300℃的范围内的温度并在随后的区域中重整含甲烷气体混合物以形成合成气。

89. 发明授权

US6137001A Process for preparing aromatic carboxylic acids with efficient treatments of gaseous effluent 失效
标题翻译：通过有效处理气态流出物制备芳香族羧酸的方法
公开(公告)号：US6137001A
公开(公告)日：2000-10-24
申请号：US245214
申请日：1999-02-05
申请人： Jeffrey L. Broeker , Frank G. Belmonte , Thomas M. Bartos , Alakananda Bhattacharyya , Anne M. Karachewski , Bruce I. Rosen , Kenneth J. Abrams
发明人： Jeffrey L. Broeker , Frank G. Belmonte , Thomas M. Bartos , Alakananda Bhattacharyya , Anne M. Karachewski , Bruce I. Rosen , Kenneth J. Abrams
IPC分类号： C01B7/09 , C07C29/124 , C07C51/265 , C07C51/15
CPC分类号： C07C29/124 , C01B7/093 , C07C51/265 , Y02P20/131
摘要： Processes are disclosed for recovery of hydrogen bromide from one or more alkyl bromide compounds by hydrolyzing the alkyl bromide compounds to hydrogen bromide and corresponding alcohols, and simultaneously separating at least the alcoholic products of hydrolysis from aliphatic monocarboxylic acid solvent component. Also disclosed are process for preparing aromatic carboxylic acids by the exothermic, liquid-phase oxidation of an aromatic feedstock compound wherein the energy produced by the exothermic oxidation is efficiently recovered, and uses of water produced during the preparation of aromatic carboxylic acids are efficiently integrated into the process.
摘要翻译：公开了通过将烷基溴化合物水解成溴化氢和相应的醇，同时将至少水解的醇产物与脂族一元羧酸溶剂组分分离，从一种或多种烷基溴化合物中回收溴化氢的方法。还公开了通过芳族原料化合物的放热，液相氧化制备芳族羧酸的方法，其中通过放热氧化产生的能量被有效地回收，并且在制备芳族羧酸期间产生的水的使用被有效地整合到的过程。

90. 发明授权

US5980840A Autothermic reactor and process using oxygen ion--conducting dense ceramic membrane 失效
标题翻译：自热反应器和工艺采用氧离子导电致密陶瓷膜
公开(公告)号：US5980840A
公开(公告)日：1999-11-09
申请号：US845310
申请日：1997-04-25
申请人： Mark S. Kleefisch , Carl A. Udovich , Alakananda Bhattacharyya , Thaddeus P. Kobylinski
发明人： Mark S. Kleefisch , Carl A. Udovich , Alakananda Bhattacharyya , Thaddeus P. Kobylinski
IPC分类号： B01D53/22 , B01D53/88 , B01D71/02 , B01J8/00 , B01J19/24 , C01B3/38 , C01B3/40 , C01G49/00 , C01G51/00 , C04B35/00 , B01J8/02 , C10J1/28 , F28D21/00
CPC分类号： C01B3/382 , B01D53/885 , B01J19/2475 , B01J8/009 , C01B3/40 , B01J2219/00117 , B01J2219/00135 , B01J2219/00164 , B01J2219/00166 , C01B2203/1052 , C01B2203/1082 , C01B2203/142 , C01B2203/82
摘要： The present invention relates to devices for conducting, simultaneously, exothermic and endothermic chemical conversions with transfer of heat therebetween. More particularly, this invention relates to autothermic modules using oxygen ion-conducting dense ceramic membranes to separate, selectively, oxygen from an oxygen-containing gas and supply it directly to partial combustion of gaseous organic compounds. Processes using autothermic modules in accordance with this invention are, advantageously, used for production of synthesis gas comprising carbon monoxide and molecular hydrogen which synthesis gas is substantially free of deleterious and/or inert gaseous diluents such as nitrogen. In particular, for conversions, within the integral autothermic module, of natural gas or other forms of gaseous lower alkanes to synthesis gas by means of partial combustion followed by reforming.
摘要翻译：本发明涉及用于同时传导放热和吸热化学转化的装置，其间传递热量。更具体地说，本发明涉及使用氧离子传导致密陶瓷膜从含氧气体中选择性分离氧并将其直接供应到气态有机化合物的部分燃烧的自热模块。使用根据本发明的自热模块的方法有利地用于生产包含一氧化碳和分子氢的合成气，该合成气基本上不含有害和/或惰性的气态稀释剂如氮气。特别地，在整体自热模块内，通过部分燃烧，随后重整，将天然气或其它形式的气态低级烷烃转化成合成气。

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