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81. 发明申请

US20080295692A1 UV CROSS-LINKED POLYMER FUNCTIONALIZED MOLECULAR SIEVE/POLYMER MIXED MATRIX MEMBRANES FOR SULFUR REDUCTION 审中-公开
标题翻译： UV交联聚合物功能化分子筛/聚合物混合基体膜减少硫化
公开(公告)号：US20080295692A1
公开(公告)日：2008-12-04
申请号：US11757030
申请日：2007-06-01
申请人： Chunqing Liu , Jeffrey J. Chiou , Stephen T. Wilson
发明人： Chunqing Liu , Jeffrey J. Chiou , Stephen T. Wilson
IPC分类号： B01D46/00 , B29C71/04 , C08K3/30 , C08K3/32 , C08K3/34
CPC分类号： B01D69/125 , B01D53/228 , B01D67/0006 , B01D69/141 , B01D2323/345
摘要： The present invention discloses high performance UV cross-linked polymer functionalized molecular sieve/polymer mixed matrix membranes (MMMs), the method of making these membranes, and the use of such membranes for separations. These UV cross-linked MMMs were prepared by incorporating polyethersulfone functionalized molecular sieves such as AlPO-14 and UZM-25 into a continuous UV cross-linkable polymer matrix followed by UV cross-linking. The UV cross-linked MMMs in the form of symmetric dense film, asymmetric flat sheet membrane, or asymmetric hollow fiber membranes described in the current invention have good flexibility and high mechanical strength, and exhibit significantly enhanced selectivity and permeability over the polymer membranes made from the corresponding continuous polyimide polymer matrices for carbon dioxide/methane (CO2/CH4) and hydrogen/methane (H2/CH4) separations. The MMMs of the present invention are suitable for a variety of liquid, gas, and vapor separations such as deep desulfurization of gasoline and diesel fuels.
摘要翻译：本发明公开了高性能的紫外线交联聚合物官能化分子筛/聚合物混合基质膜（MMM），制备这些膜的方法以及使用这种膜进行分离。这些UV交联的MMM通过将聚醚砜官能化分子筛（例如AlPO-14和UZM-25）掺入连续的UV可交联聚合物基质中随后进行UV交联来制备。本发明所述的对称致密膜，不对称平板膜或不对称中空纤维膜形式的UV交联MMM具有良好的柔韧性和高的机械强度，并且显示出比由二氧化碳/甲烷（CO2 / CH4）和氢/甲烷（H2 / CH4）分离的相应的连续聚酰亚胺聚合物基质。本发明的MMM适合于各种液体，气体和蒸气分离，例如汽油和柴油的深度脱硫。

82. 发明申请

US20080142440A1 Liquid Separations Using High Performance Mixed Matrix Membranes 审中-公开
标题翻译：使用高性能混合基质膜的液体分离
公开(公告)号：US20080142440A1
公开(公告)日：2008-06-19
申请号：US11612402
申请日：2006-12-18
申请人： Chunqing Liu , Man-Wing Tang , Stephen T. Wilson , David A. Lesch
发明人： Chunqing Liu , Man-Wing Tang , Stephen T. Wilson , David A. Lesch
IPC分类号： B01D61/14 , B01D61/36
CPC分类号： B01D61/362 , B01D53/228 , B01D67/0079 , B01D69/141
摘要： The present invention discloses a novel method of making high performance mixed matrix membranes (MMMs) using stabilized concentrated suspensions of solvents, uniformly dispersed polymer stabilized molecular sieves, and at least two different types of polymers as the continuous blend polymer matrix. MMMs as dense films or asymmetric flat sheet or hollow fiber membranes fabricated by the method described in the current invention exhibit significantly enhanced permeation performance for separations over the polymer membranes made from the continuous blend polymer matrix. MMMs of the present invention are suitable for a wide range of gas, vapor, and liquid separations such as alcohol/water, CO2/CH4, H2/CH4, O2/N2, CO2/N2, olefin/paraffin, iso/normal paraffins, and other light gases separations.
摘要翻译：本发明公开了使用稳定的溶剂浓缩悬浮液，均匀分散的聚合物稳定化分子筛和至少两种不同类型的聚合物作为连续共混聚合物基质制备高性能混合基质膜（MMM）的新方法。通过本发明所述方法制造的致密膜或非对称平板或中空纤维膜的MMM显示出从由连续共混聚合物基质制成的聚合物膜上的分离显着增强的渗透性能。本发明的MMM适用于各种气体，蒸汽和液体分离，例如醇/水，CO 2 / CH 4，H 2 CH 2，N 2，N 2，CO 2，N 2，N 2，烯烃/石蜡，异/正链烷烃和其它轻质气体分离。

83. 发明授权

US07271259B1 Solid phase host compositions 有权
标题翻译：固相主体组合物
公开(公告)号：US07271259B1
公开(公告)日：2007-09-18
申请号：US10430702
申请日：2003-05-06
申请人： Joseph B. Lambert , Chunqing Liu
发明人： Joseph B. Lambert , Chunqing Liu
IPC分类号： C08B37/16
CPC分类号： C08B37/0012 , C08G77/48 , C08G77/50 , C08G77/52 , C08L83/06 , C08L83/14
摘要： A new family of silicon-based polymers has been prepared in which organic host components are bound covalently. The polymer is a polysilsesquioxane matrix comprising, for example, hosts such as cyclodextrins (CD) or calixarenes (CX).
摘要翻译：已经制备了新的硅基聚合物系列，其中有机主体组分共价键合。聚合物是包括例如主体如环糊精（CD）或杯芳烃（CX））的倍半硅氧烷基质。

84. 发明申请

US20070209505A1 High Flux Mixed Matrix Membranes for Separations 审中-公开
标题翻译：用于分离的高通量混合基质膜
公开(公告)号：US20070209505A1
公开(公告)日：2007-09-13
申请号：US11679142
申请日：2007-02-26
申请人： Chunqing Liu , Santi Kulprathipanja , Stephen T. Wilson
发明人： Chunqing Liu , Santi Kulprathipanja , Stephen T. Wilson
IPC分类号： B01D53/22
CPC分类号： B01D53/228 , B01D61/362 , B01D67/0079 , B01D69/141 , B01D69/147 , B01D71/028 , B01D71/72
摘要： The present invention discloses a new class of high flux mixed matrix membranes that are made by incorporating porous inorganic fillers (e.g. microporous and mesoporous molecular sieves, carbon molecular sieves, porous metal-organic frameworks) into a high flux high surface area microporous organic polymer matrix. These microporous organic polymers are referred to as “polymers of intrinsic microporosity” or PIMs. The high flux membranes are promising for a wide range of separations including liquid separations such as pervaporation of phenol/water and also gas separations in the petrochemical, refinery, and natural gas industries such as methane/carbon dioxide, olefin/paraffin and iso/normal paraffins separations.
摘要翻译：本发明公开了一种新型高通量混合基质膜，其通过将多孔无机填料（例如微孔和介孔分子筛，碳分子筛，多孔金属 - 有机骨架）并入高通量高表面积微孔有机聚合物基体。这些微孔有机聚合物被称为“内在微孔聚合物”或PIM。高通量膜对于广泛的分离是有希望的，包括液体分离，例如苯酚/水的渗透蒸发，以及在石化，炼油和天然气工业中的气体分离，例如甲烷/二氧化碳，烯烃/石蜡和异/正常石蜡分离。

85. 发明申请

US20050221087A1 Nanoporous chelating fibers 审中-公开
标题翻译：纳米多孔螯合纤维
公开(公告)号：US20050221087A1
公开(公告)日：2005-10-06
申请号：US11057698
申请日：2005-02-14
申请人： James Economy , Chunqing Liu
发明人： James Economy , Chunqing Liu
IPC分类号： B01J45/00 , B01J47/12 , C03C25/24 , D06L1/00 , D06M11/79 , D06M15/643
CPC分类号： B01J45/00 , B01J20/2808 , B01J47/127 , C03C25/24 , D06M11/79 , D06M15/643 , D06M2400/02 , Y10T428/2933
摘要： A composite includes substrate fibers, and an organosilica coating including a structure-directing template, on the substrate fibers. The composite may be formed by coating substrate fibers with an organosilica sol containing a structure-directing template, and curing the organosilica sol to form an organosilica coating. A nanoporous chelating fiber includes a substrate fiber and a nanoporous chelating coating, on the substrate fiber. Nanoporous chelating fibers may be formed by removing the structure-directing template from a composite to form a nanoporous chelating coating on the substrate fibers. Contaminants may be removed from a fluid by contacting nanoporous chelating fibers with a fluid containing at least one contaminant.
摘要翻译：复合材料包括基材纤维和包含结构导向模板的有机二氧化硅涂层。可以通过用含有结构导向模板的有机二氧化硅溶胶涂布基材纤维，并固化有机硅溶胶以形成有机二氧化硅涂层来形成复合材料。纳米多孔螯合纤维包括基材纤维和纳米多孔螯合涂层。可以通过从复合材料中除去结构导向模板以在基底纤维上形成纳米多孔螯合涂层来形成纳米多孔螯合纤维。通过使纳米多孔螯合纤维与含有至少一种污染物的流体接触，可以从流体中除去污染物。

86. 发明授权

US06423772B1 Organo-bridged ladderlike polysiloxane, tube-like organosilicon polymers, complexes thereof, and the method for producing the same 失效
标题翻译：有机桥状梯状聚硅氧烷，管状有机硅聚合物及其络合物及其制造方法
公开(公告)号：US06423772B1
公开(公告)日：2002-07-23
申请号：US09616338
申请日：2000-07-14
申请人： Rongben Zhang , Chunqing Liu , Ping Xie , Huadong Tang
发明人： Rongben Zhang , Chunqing Liu , Ping Xie , Huadong Tang
IPC分类号： G77
CPC分类号： C08G77/52 , C08G77/50
摘要： The present invention provides to an organo-bridged ladderlike polysiloxane having the following formula: and a tube-like organosilicon polymer, complexes thereof and the method for producing the same.
摘要翻译：本发明提供具有下式的有机桥状梯状聚硅氧烷和管状有机硅聚合物及其络合物及其制备方法。

87. 发明授权

US08912288B2 Separation process using a polyimide membrane 有权
标题翻译：使用聚酰亚胺膜的分离方法
公开(公告)号：US08912288B2
公开(公告)日：2014-12-16
申请号：US13278483
申请日：2011-10-21
申请人： Chunqing Liu , Travis C. Bowen , Emily G. Harbert , Raisa Minkov , Syed A. Faheem , Zara Osman
发明人： Chunqing Liu , Travis C. Bowen , Emily G. Harbert , Raisa Minkov , Syed A. Faheem , Zara Osman
IPC分类号： C08G69/08 , B01D71/64 , B01D53/22 , B01D61/02 , B01D61/36 , B01D67/00 , B01D69/08 , C02F1/44 , C07K1/14 , C07C7/144 , C07C17/38 , C10G31/11
CPC分类号： B01D71/64 , A61K9/70 , B01D53/228 , B01D61/025 , B01D61/362 , B01D67/0093 , B01D69/08 , B01D71/68 , B01D2323/30 , B01D2323/345 , C02F1/441 , C02F1/448 , C07C7/144 , C07C17/38 , C07K1/14 , C10G31/11 , C10G2300/1044 , Y02E50/17 , Y02P20/152 , Y02P20/51 , C07C9/04 , C07C11/06 , C07C11/09 , C07C11/02 , C07C19/04
摘要： The present invention discloses a new type of polyimide membrane with high permeances and high selectivities for gas separations and particularly for CO2/CH4 and H2/CH4 separations. The polyimide membranes have CO2 permeability of 50 Barrers or higher and single-gas selectivity for CO2/CH4 of 15 or higher at 50° C. under 791 kPa for CO2/CH4 separation. The polyimide membranes have UV cross-linkable functional groups and can be used for the preparation of UV cross-linked polyimide membranes having CO2 permeability of 20 Barrers or higher and single-gas selectivity for CO2/CH4 of 35 or higher at 50° C. under 791 kPa for CO2/CH4 separation.
摘要翻译：本发明公开了一种具有高渗透性和高选择性的新型聚酰亚胺膜，用于气体分离，特别是用于CO 2 / CH 4和H 2 / CH 4分离。聚酰亚胺膜具有50巴尔或更高的CO 2渗透性，对于CO 2 / CH 4分离，在791kPa下，在50℃，CO 2 / CH 4的单气体选择性为15或更高。聚酰亚胺膜具有UV可交联官能团，可用于制备二氧化碳透过率为20巴尔或更高的紫外线交联聚酰亚胺膜，在50℃下二氧化碳/氯化氢的单气选择性为35或更高。在791 kPa下CO2 / CH4分离。

88. 发明授权

US08816003B2 High plasticization-resistant cross-linked polymeric membranes for separations 有权
标题翻译：用于分离的高增塑抗性交联聚合物膜
公开(公告)号：US08816003B2
公开(公告)日：2014-08-26
申请号：US12145153
申请日：2008-06-24
申请人： Chunqing Liu , Stephen T. Wilson , David A. Lesch
发明人： Chunqing Liu , Stephen T. Wilson , David A. Lesch
IPC分类号： C08F12/22
CPC分类号： C08B15/10 , B01D53/228 , B01D67/0093 , B01D71/16 , B01D2323/30 , B01D2325/30 , C08G18/6484 , C08L71/02 , C08L81/06 , Y02P20/152
摘要： This invention involves a composition, a method of making, and an application of high plasticization-resistant chemically cross-linked polymeric membranes such as cross-linked cellulose acetate (CA) membrane. These cross-linked polymeric membranes with covalently interpolymer-chain-connected rigid networks showed no decrease in CO2/CH4 ideal selectivity under 690 kPa (100 psig) pure CO2 pressure and also no CO2 plasticization up to 3447 kPa (500 psig) pure CO2 pressure. By using the method of chemical cross-linking as described in this invention, the separation characteristics of the polymeric membranes can be decisively improved. These new cross-linked polymeric membranes can be used not only for gas separations such as CO2/CH4 and CO2/N2 separations, O2/N2 separation, olefin/paraffin separations (e.g. propylene/propane separation), iso/normal paraffins separations, but also for liquid separations such as pervaporation and desalination.
摘要翻译：本发明涉及一种组合物，制备方法，以及应用高耐增塑作用的化学交联聚合物膜，例如交联乙酸纤维素（CA）膜。这些具有共价互聚链连接的刚性网络的交联聚合物膜在690kPa（100psig）纯二氧化碳压力下没有显示CO 2 / CH 4理想选择性的降低，并且也没有CO2增塑达3447kPa（500psig）纯二氧化碳压力。通过使用如本发明所述的化学交联方法，可以确定地提高聚合物膜的分离特性。这些新的交联聚合物膜不仅可用于气体分离，如CO2 / CH4和CO2 / N2分离，O2 / N2分离，烯烃/石蜡分离（如丙烯/丙烷分离），异/正链烷烃分离，但还用于液体分离，例如渗透蒸发和脱盐。

89. 发明授权

US08710173B2 Blend polymer gas separation membrane 有权
标题翻译：混合聚合物气体分离膜
公开(公告)号：US08710173B2
公开(公告)日：2014-04-29
申请号：US13278545
申请日：2011-10-21
申请人： Chunqing Liu , Travis C. Bowen , Emily G. Harbert , Raisa Minkov , Syed A. Faheem , Zara Osman
发明人： Chunqing Liu , Travis C. Bowen , Emily G. Harbert , Raisa Minkov , Syed A. Faheem , Zara Osman
IPC分类号： C08G69/08
CPC分类号： C08G73/1071 , B01D53/226 , B01D53/227 , B01D53/228 , B01D71/64 , B01D71/68 , B01D2256/10 , B01D2256/12 , B01D2256/14 , B01D2256/16 , B01D2256/18 , B01D2256/245 , B01D2257/11 , B01D2257/304 , B01D2257/502 , B01D2257/504 , B01D2257/702 , B01D2257/708 , B01D2258/05 , B01D2258/06 , B01D2323/30 , B01D2323/345 , B01J20/267 , B01J20/28033 , B01J20/28038 , C08G73/1039 , C08G73/1067 , C08G73/1078 , C08L79/08 , Y02C10/10 , Y02P20/152
摘要： The present invention discloses a new type of polyimide membrane with high permeances and high selectivities for gas separations and particularly for CO2/CH4 and H2/CH4 separations. The polyimide membranes have CO2 permeability of 50 Barrers or higher and single-gas selectivity for CO2/CH4 of 15 or higher at 50° C. under 791 kPa for CO2/CH4 separation. The polyimide membranes have UV cross-linkable functional groups and can be used for the preparation of UV cross-linked polyimide membranes having CO2 permeability of 20 Barrers or higher and single-gas selectivity for CO2/CH4 of 35 or higher at 50° C. under 791 kPa for CO2/CH4 separation.
摘要翻译：本发明公开了一种具有高渗透性和高选择性的新型聚酰亚胺膜，用于气体分离，特别是用于CO 2 / CH 4和H 2 / CH 4分离。聚酰亚胺膜具有50巴尔或更高的CO 2渗透性，对于CO 2 / CH 4分离，在791kPa下，在50℃，CO 2 / CH 4的单气体选择性为15或更高。聚酰亚胺膜具有UV可交联官能团，可用于制备二氧化碳透过率为20巴尔或更高的紫外线交联聚酰亚胺膜，在50℃下二氧化碳/氯化氢的单气选择性为35或更高。在791 kPa下CO2 / CH4分离。

90. 发明授权

US08614288B2 Polyimide gas separation membranes 有权
标题翻译：聚酰亚胺气体分离膜
公开(公告)号：US08614288B2
公开(公告)日：2013-12-24
申请号：US13278388
申请日：2011-10-21
申请人： Chunqing Liu , Travis C. Bowen , Emily G. Harbert , Raisa Minkov , Syed A. Faheem , Zara Osman
发明人： Chunqing Liu , Travis C. Bowen , Emily G. Harbert , Raisa Minkov , Syed A. Faheem , Zara Osman
IPC分类号： C08G69/08
CPC分类号： C08G73/1042 , B01D53/228 , B01D61/362 , B01D67/0009 , B01D67/009 , B01D69/02 , B01D69/06 , B01D69/08 , B01D71/64 , B01D71/82 , B01D2323/30 , B01D2323/345 , B01D2325/20 , C08G73/1046 , C08G73/1064 , Y02P20/152
摘要： The present invention discloses a new type of polyimide membrane with high permeances and high selectivities for gas separations and particularly for CO2/CH4 and H2/CH4 separations. The polyimide membranes have CO2 permeability of 50 Barrers or higher and single-gas selectivity for CO2/CH4 of 15 or higher at 50° C. under 791 kPa for CO2/CH4 separation. The polyimide membranes have UV cross-linkable functional groups and can be used for the preparation of UV cross-linked polyimide membranes having CO2 permeability of 20 Barrers or higher and single-gas selectivity for CO2/CH4 of 35 or higher at 50° C. under 791 kPa for CO2/CH4 separation.
摘要翻译：本发明公开了一种具有高渗透性和高选择性的新型聚酰亚胺膜，用于气体分离，特别是用于CO 2 / CH 4和H 2 / CH 4分离。聚酰亚胺膜具有50巴尔或更高的CO 2渗透性，对于CO 2 / CH 4分离，在791kPa下，在50℃，CO 2 / CH 4的单气体选择性为15或更高。聚酰亚胺膜具有UV可交联官能团，可用于制备二氧化碳透过率为20巴尔或更高的紫外线交联聚酰亚胺膜，在50℃下二氧化碳/氯化氢的单气选择性为35或更高。在791 kPa下CO2 / CH4分离。

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