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    • 81. 发明授权
    • Method for measuring bonding force between substrate and carbon nanotube array formed thereon
    • 用于测量在其上形成的衬底和碳纳米管阵列之间的结合力的方法
    • US07559253B2
    • 2009-07-14
    • US11848186
    • 2007-08-30
    • Kai LiuKai-Li JiangShou-Shan Fan
    • Kai LiuKai-Li JiangShou-Shan Fan
    • G01N3/08
    • G01N19/04G01N2203/0286
    • A method for measuring a bonding force between a substrate (50) and a carbon nanotube array (40) formed thereon, wherein the carbon nanotube array includes a plurality of carbon nanotubes. A force gauge (1) including a cantilever (10), a flat-surface probe (20), a movement mechanism (60), and a force sensor (70) is provided. The probe is secured at one end of the cantilever. An adhesive layer (30) is formed on the flat surface of the probe. The probe is moved toward the substrate and is brought into bonding contact with the carbon nanotube array by the movement mechanism. The probe is pulled away from the substrate by the movement mechanism, causing the carbon nanotubes adhered thereto to separate from the substrate. The force at separation is detected by the force sensor, and that force can be converted into an average nanotube/substrate bonding force/strength.
    • 一种用于测量在其上形成的基板(50)和碳纳米管阵列(40)之间的结合力的方法,其中所述碳纳米管阵列包括多个碳纳米管。 提供了包括悬臂(10),平面表面探针(20),移动机构(60)和力传感器(70)的力量表(1)。 探头固定在悬臂的一端。 在探针的平坦表面上形成粘合剂层(30)。 探头朝向基板移动,并通过移动机构与碳纳米管阵列进行粘合接触。 通过移动机构将探针从基板拉出,使得粘附到其上的碳纳米管与基板分离。 分离时的力由力传感器检测,并且该力可以转换为平均纳米管/基底粘合力/强度。
    • 83. 发明申请
    • Apparatus and method for making carbon nanotube array
    • 制造碳纳米管阵列的装置和方法
    • US20060269669A1
    • 2006-11-30
    • US11371997
    • 2006-03-08
    • Kai-Li JiangKai LiuShou-Shan Fan
    • Kai-Li JiangKai LiuShou-Shan Fan
    • C23C16/00
    • C23C16/0281C23C16/26C23C16/448C30B25/02C30B29/02C30B29/605Y10S427/102
    • An apparatus for making an array of carbon nanotubes includes a reaction chamber with a gas inlet and a gas outlet; a quartz boat disposed in the reaction chamber; a substrate with a surface deposited with a film of first catalyst, the substrate being disposed in the quartz boat; and a second catalyst disposed in the quartz beside the substrate. A method for making an array of carbon nanotubes, comprising the steps of: (a) providing a substrate with a surface deposited with a film of first catalyst; (b) disposing a second catalyst beside the substrate to produce small amounts of hydrogen gas which flows to the first catalyst; (c) introducing a carrier gas and a carbon source gas flowing from the second catalyst to the first catalyst at a predetermined temperature; and (d) growing an array of carbon nanotubes extending from the substrate.
    • 制造碳纳米管阵列的装置包括具有气体入口和气体出口的反应室; 设置在反应室中的石英舟; 具有表面沉积有第一催化剂膜的基板,所述基板设置在所述石英舟中; 以及设置在基板旁边的石英中的第二催化剂。 一种制备碳纳米管阵列的方法,包括以下步骤:(a)向基材提供沉积有第一催化剂膜的表面; (b)在基板旁边设置第二催化剂以产生流过第一催化剂的少量氢气; (c)在预定温度下引入从第二催化剂流向第一催化剂的载气和碳源气体; 和(d)生长从衬底延伸的碳纳米管阵列。