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81. 发明授权

US5089565A Process for the preparation of curable binder combinations, the combinations obtainable by this process and the use thereof 失效
标题翻译：制备可固化粘合剂组合的方法，本方法可获得的组合及其用途
公开(公告)号：US5089565A
公开(公告)日：1992-02-18
申请号：US358448
申请日：1989-05-30
申请人： Harald Blum , Christian Wamprecht , Josef Pedain , Michael Sonntag
发明人： Harald Blum , Christian Wamprecht , Josef Pedain , Michael Sonntag
IPC分类号： C08L35/00 , C08F20/02 , C08F22/06 , C08K5/35 , C09D133/02 , C09D135/00
CPC分类号： C09D135/00 , C08K5/35
摘要： A moisture-curing binder composition useful in paints and other coating compositions is prepared by mixing or mixing with spontaneous reaction in the absence of moistureA) 30 to 99 parts by weight of at least one compound containing at least two intramolecular carboxylic anhydride groups andB) 1 to 70 parts by weight of organic compounds having blocked amino groups, wherein B)comprises organic compounds containing hydrogen atoms which are reactive to acid anhydride groups and containing bicyclic amide acetal or bicyclic amide groups or both, wherein the ratios of the amounts of the individual components are chosen such that, by taking into account the addition reaction which occurs spontaneously between components A) and B) in the absence of moisture, in the resulting mixture 0.25 to 50 anhydride groups are present per bicyclic amide acetal and bicyclic amide aminal group.
摘要翻译：用于油漆和其他涂料组合物的湿固化粘合剂组合物通过在不存在水分的情况下与自发反应混合或混合制备A）30至99重量份的至少一种含有至少两个分子内羧酸酐基团的化合物和B ）1至70重量份具有封闭氨基的有机化合物，其中B）包含含有与酸酐基团反应并含有双环酰胺缩醛或双环酰胺基团或两者的氢原子的有机化合物，其中，选择各个组分使得通过考虑到在不存在水分的情况下在组分A）和B）之间自发发生的加成反应，在所得混合物中，每双酰胺缩醛和双环酰胺缩醛存在0.25至50个酸酐基团组。

82. 发明授权

US4980412A Aqueous solutions or dispersions of self-crosslinking binders, a process for their production and their use 失效
标题翻译：自交联粘合剂的水溶液或分散体，其生产方法及其用途
公开(公告)号：US4980412A
公开(公告)日：1990-12-25
申请号：US441751
申请日：1989-11-27
申请人： Harald Blum
发明人： Harald Blum
IPC分类号： C08L35/00 , C08F8/00 , C08F8/30 , C08F8/44 , C08K5/35
CPC分类号： C08K5/35 , C08F8/44 , C08F2810/20
摘要： Aqueous solutions or dispersions of self-crosslinking binders based on ionically modified polycarboxylic acid polyanhydrides, wherein the binders dissolved or dispersed in water have(a) a total content of lateral carboxylic acid ester, carboxylic acid thioester or carboxylic acid amide groups of up to 500 milliequivalents per 100 grams solids,(b) a content of chemically incorporated carboxylate groups of from 10 to 500 milliequivalents per 100 grams solids and(c) a content of ammonium groups of from 10 to 500 milliequivalents per 100 grams solids,are prepared which comprises a first reaction step wherein polyanhydrides (A) containing intramolecular carboxylic anhydride groups are at least partly reacted, with or without inert solvents, with blocked amines (B) which are activatible by water and which, in addition to blocked amino groups, contain at least one anhydride-reactive hydroxy, mercapto or amino group, in a molar ratio of anhydride groups to anhydride-reactive groups of 10:1 to 0.8:1 in an ester-, thioester- or amide-forming reaction accompanied by ring opening, and a second reaction step wherein the reaction mixture obtained from the first step is diluted with water and stirred at room temperature or higher until a stable aqueous solution or dispersion is formed.
摘要翻译：基于离子改性的多元羧酸聚酐的自交联粘合剂的水溶液或分散体，其中溶解或分散在水中的粘合剂具有（a）高达500的侧向羧酸酯，羧酸硫酯或羧酸酰胺基团的总含量每100克固体的毫当量，（b）每100克固体含有10-500毫当量的化学掺入的羧酸酯基团的含量，和（c）每100克固体含有10-500毫当量的铵基含量，其包含第一反应步骤，其中含有分子内羧酸酐基团的聚酐（A）至少部分地与（或不与惰性溶剂）反应，与被胺保护的封闭胺（B）部分反应，并且除封闭的氨基以外，还含有至少一个酸酐反应性羟基，巯基或氨基，酸酐基团与酸酐反应性基团的摩尔比为10:1 在连续开环的酯 - ，硫酯或酰胺形成反应中为0.8:1，第二反应步骤为将第一步得到的反应混合物用水稀释并在室温或更高温度下搅拌直到稳定的水溶液形成溶液或分散体。

83. 发明授权

US4975493A Process for the production of moisture-hardening binder compositions and their use 失效
标题翻译：湿固化粘合剂组合物的生产方法及其用途
公开(公告)号：US4975493A
公开(公告)日：1990-12-04
申请号：US223803
申请日：1988-07-25
申请人： Harald Blum , Josef Pedain , Christian Wamprecht , Michael Sonntag
发明人： Harald Blum , Josef Pedain , Christian Wamprecht , Michael Sonntag
IPC分类号： C08L23/00 , C08F8/32 , C08K5/35 , C09D133/04 , C09D135/00
CPC分类号： C08K5/35 , C08F8/32 , C09D135/00 , C08F2800/20
摘要： A moisture-hardening binder composition for lacquer of coating compositions is prepared by mixing(A) 50 to 97 parts by weight of copolymers of maleic anhydride with olefinically unsaturated monomers, said copolymers containing succinic anhydride units and having molecular weights Mw of 1,500 to 75,000 with(B) 3 to 50 parts by weight oxazolanes having a molecular weight Mw of 87 to 10,000,the quantitative ratios of (A) to (B) being such that the composition contains 0.25 to 10 anhydride groups for every oxazolane group,wherein component (A) consists essentially of copolymers of(a) 4.5 to 45 parts by weight of maleic anhydride,(b) 5 to 80 parts by weight of monomers of the formulae ##STR1## or both, and (c) 15 to 92 parts by weight of monomers of the formula ##STR2## wherein, R.sub.1 and R.sub.4 is each, independent of the other, an aliphatic or cycloaliphatic C.sub.1 -C.sub.12 hydrocarbon radical with or without oxygen, sulfur or nitrogen as a heteratom, R.sub.2 is hydrogen, methyl, ethyl, chlorine or fluorine,R.sub.3 is a C.sub.2 -C.sub.15 aliphatic hydrocarbon radical, a C.sub.5 -C.sub.10 cycloaliphatic hydrocarbon radical, a C.sub.7 -C.sub.18 araliphatic hydrocarbon radical, a C.sub.6 -C.sub.12 aromatic hydrocarbon radical, chlorine, fluorine, nitrile or a C.sub.2 -C.sub.18 hydrocarbon radical containing one or more heteroatoms selected from the group consisting of oxygen, sulfur and nitrogen in the form of ether, ester, amide, urethane, urea, thioester, oxirane, ketone, lactam or lactone groups.
摘要翻译：通过混合（A）50至97重量份的马来酸酐与烯属不饱和单体的共聚物，所述共聚物含有琥珀酸酐单元并具有1500至75,000的分子量Mw，制备用于涂料组合物漆的湿润硬化粘合剂组合物，（B）3〜50重量份的分子量Mw为87〜10,000的恶唑烷，（A）〜（B）的定量比为每个恶唑烷基组成含有0.25〜10个酸酐基，其中组分（ A）基本上由（a）4.5至45重量份马来酸酐的共聚物组成，（b）5-80重量份式（IMAGE）或两者的单体，和（c）15至92重量份具有下式的单体：其中，R 1和R 4各自独立地为具有或不具有氧，硫或氮作为杂原子的脂族或脂环族C 1 -C 12烃基，R 2为氢，甲基，乙基，氯或氟 ne，R 3是C 2 -C 15脂族烃基，C 5 -C 10脂环族烃基，C 7 -C 18芳脂族烃基，C 6 -C 12芳烃基，氯，氟，腈或含有一个的C 2 -C 18烃基或更多选自醚，酯，酰胺，氨基甲酸酯，脲，硫酯，环氧乙烷，酮，内酰胺或内酯基团的氧，硫和氮的杂原子。

84. 发明申请

US20120041145A1 AQUEOUS COATING SYSTEMS BASED ON PHYSICALLY DRYING URETHANE ACRYLATES 有权
标题翻译：基于物理干燥丙烯酸酯的水性涂料体系
公开(公告)号：US20120041145A1
公开(公告)日：2012-02-16
申请号：US13201074
申请日：2010-01-30
申请人： Stefan Sommer , Harald Blum , Jürgen Lippemeier , Miguel Fernandez
发明人： Stefan Sommer , Harald Blum , Jürgen Lippemeier , Miguel Fernandez
IPC分类号： C09D175/06 , C09J175/06
CPC分类号： C09D175/16 , C08F283/01 , C08G18/0823 , C08G18/10 , C08G18/4208 , C08G18/4213 , C08G18/4219 , C08G18/6659 , C08G18/672 , C08G18/724 , C08G18/758 , C08G18/792 , C08G2170/80 , C08G18/3228
摘要： The invention relates to radiation curable coating systems on the basis of aqueous polyurethane dispersions, to a method for the production thereof, to the use of the coating systems as paints and/or adhesives, and to objects and substrates provided with said paints and/or adhesives.
摘要翻译：本发明涉及基于水性聚氨酯分散体的可辐射固化涂料体系，其制备方法，涂料体系作为涂料和/或粘合剂的用途，以及提供有所述涂料和/或粘合剂。

85. 发明申请

US20110244228A1 CURABLE POLYURETHANE DISPERSIONS 审中-公开
标题翻译：可固化的聚氨酯分散体
公开(公告)号：US20110244228A1
公开(公告)日：2011-10-06
申请号：US13127924
申请日：2009-10-31
申请人： Harald Blum , Jörg Büchner , Wolfgang Henning
发明人： Harald Blum , Jörg Büchner , Wolfgang Henning
IPC分类号： C08L75/06 , C09J175/06 , C09J7/02
CPC分类号： C08G18/0823 , C08G18/12 , C08G18/348 , Y10T428/2848 , Y10T428/287 , Y10T428/2896 , C08G18/3821
摘要： The present invention relates to an aqueous polyurethane or polyurethane-urea dispersion comprising a polyurethane or a polyurethane polyurea dispersed therein, wherein the polyurethane or polyurethane polyurea comprises terminal carboxyl groups and lateral sulfonate and/or carboxylate groups.
摘要翻译：本发明涉及包含分散在其中的聚氨酯或聚氨酯聚脲的水性聚氨酯或聚氨酯 - 脲分散体，其中所述聚氨酯或聚氨酯聚脲包含末端羧基和侧向磺酸盐和/或羧酸酯基团。

86. 发明授权

US07902302B2 Hydroxy-functional polyester-polyurethane dispersions, methods of preparing the same, compositions containing such dispersions and uses therefor 失效
标题翻译：羟基官能聚酯 - 聚氨酯分散体，其制备方法，含有这种分散体的组合物及其用途
公开(公告)号：US07902302B2
公开(公告)日：2011-03-08
申请号：US12121926
申请日：2008-05-16
申请人： Harald Blum , Heino Müller
发明人： Harald Blum , Heino Müller
IPC分类号： C08L69/00
CPC分类号： C08G18/0823 , C08G18/345 , C08G18/6659 , C09D175/06
摘要： Hydroxy-functional polyester-polyurethane dispersions comprising a reaction product of: (a) at least one, at least difunctional polyol component; (b) at least one ionizable compound having at least one acid group and at least one functional group capable of reacting with isocyanate groups, the at least one functional group selected from the group consisting of mono-, di-, and trihydroxycarboxylic acids, hydroxysulfonic acids, aminosulfonic acids, and aminocarboxylic acids; (c) at least one acid anhydride; and (d) at least one, at least difunctional polyisocyanate component; methods for preparing such dispersions; compositions containing such dispersions; and uses thereof.
摘要翻译：羟基官能聚酯 - 聚氨酯分散体包含以下反应产物：（a）至少一种至少双官能的多元醇组分; （b）至少一种具有至少一个酸基团和至少一个能够与异氰酸酯基团反应的官能团的可离子化化合物，所述至少一种选自单 - ，二 - 和三羟基羧酸的官能团，羟基磺酸酸，氨基磺酸和氨基羧酸; （c）至少一种酸酐; 和（d）至少一种至少双官能的多异氰酸酯组分; 制备这种分散体的方法; 含有这种分散体的组合物; 及其用途。

87. 发明申请

US20110015291A1 PREPOLYMERS BASED ON DI- OR POLYISOCYANATES AND FORMAMIDE-TERMINATED LOW MOLECULAR WEIGHT COMPOUNDS, PROCESSES FOR PREPARING THE SAME AND USES THEREOF 有权
标题翻译：基于异二聚氰酸酯和甲醛封端的低分子量化合物的预聚物，其制备方法及其用途
公开(公告)号：US20110015291A1
公开(公告)日：2011-01-20
申请号：US12837536
申请日：2010-07-16
申请人： Harald Blum , Evelyn Peiffer , Marc Leimenstoll
发明人： Harald Blum , Evelyn Peiffer , Marc Leimenstoll
IPC分类号： C08G18/10 , C07C263/16
CPC分类号： C08G18/3825 , C08G18/10 , C08G18/5039 , C09D175/04 , C09J175/04
摘要： Prepolymers, which are accessible from formamides of low molecular weight di- or triamines (formamide-terminated low molecular weight compounds) and di- or polyisocyanates, of the general formula (II): X—[—N(CHO)—CO—NH—R1—NCO]n (II) wherein X represents a linear or branched aliphatic, cycloaliphatic, heterocyclic and/or aromatic structural unit having 2 to 40 carbon atoms, and which is optionally further substituted and/or optionally comprises one or more heteroatoms, wherein R1 represents an organic radical which may optionally contain one or more heteroatoms and which may further contain one or more additional free isocyanate groups and/or one or more urethane, biuret, carbodiimide, isocyanurate, allophanate, iminooxadiazinedione and/or uretdione structural units, and wherein n≧2; processes for making the same; compositions containing the same; and uses thereof
摘要翻译：通式（II）的低分子量二 - 或三胺（甲酰胺封端的低分子量化合物）和二异氰酸酯或多异氰酸酯的甲酰胺可以得到的预聚物：X - [ - N（CHO）-CO-NH -R1-NCO] n（II）其中X表示具有2至40个碳原子的直链或支链脂族，脂环族，杂环和/或芳族结构单元，并且其任选进一步被取代和/或任选地包含一个或多个杂原子，其中R1表示可以任选地含有一个或多个杂原子并且还可以含有一个或多个另外的游离异氰酸酯基团和/或一个或多个氨基甲酸酯，缩二脲，碳二亚胺，异氰脲酸酯，脲基甲酸酯，亚氨基恶二嗪二酮和/或脲二酮结构单元的有机基团，并且其中n≥2; 制作相同的过程; 含有它们的组合物; 及其用途

88. 发明申请

US20100210757A1 Aqueous Coating Systems Based On Physically Drying Urethane Acrylates 审中-公开
标题翻译：基于物理干燥聚氨酯丙烯酸酯的水性涂料体系
公开(公告)号：US20100210757A1
公开(公告)日：2010-08-19
申请号：US12704804
申请日：2010-02-12
申请人： Stefan Sommer , Harald Blum , Jürgen Lippemeier
发明人： Stefan Sommer , Harald Blum , Jürgen Lippemeier
IPC分类号： C09D175/04 , C08L75/04
CPC分类号： C09D175/16 , C08G18/0823 , C08G18/4211 , C08G18/4213 , C08G18/672 , C08G18/42
摘要： The invention relates to radiation-curable coating systems based on aqueous polyurethane dispersions, to a process for their production, to the use of the coating systems as lacquers and/or adhesives, and also to articles and substrates provided with these lacquers and/or adhesive.
摘要翻译：本发明涉及基于水性聚氨酯分散体的辐射固化涂料体系，其生产方法，涂料体系作为漆和/或粘合剂的使用，以及提供有这些漆和/或粘合剂的制品和基材。

89. 发明申请

US20090094886A1 LOW-VISCOSITY ESTER MIXTURES 审中-公开
标题翻译：低粘度酯混合物
公开(公告)号：US20090094886A1
公开(公告)日：2009-04-16
申请号：US12247459
申请日：2008-10-08
申请人： Burkhardt Koehler , Harald Blum , Sebastian Doerr
发明人： Burkhardt Koehler , Harald Blum , Sebastian Doerr
IPC分类号： C10L1/18
CPC分类号： C11C3/10 , C09D7/20 , C09D7/47 , C10L1/02 , C10L1/1817 , C10L1/19 , C10M105/34 , C10M105/38 , C10M2207/2815 , C10M2207/2835
摘要： The invention relates to the preparation of low-viscosity ester mixtures for transesterification of vegetable or animal fats or oils with monofunctional esters.
摘要翻译：本发明涉及用于将植物油或动物油脂与单官能酯酯交换的低粘度酯混合物的制备。

90. 发明申请

US20070129488A1 Preparation of a polyurethane dispersion with blocked isocyanate groups 有权
标题翻译：制备具有封端异氰酸酯基团的聚氨酯分散体
公开(公告)号：US20070129488A1
公开(公告)日：2007-06-07
申请号：US11604954
申请日：2006-11-28
申请人： Sebastian Dorr , Heino Muller , Harald Blum
发明人： Sebastian Dorr , Heino Muller , Harald Blum
IPC分类号： C08G18/08
CPC分类号： C08G18/0823 , C08G18/706 , C08G18/792 , C08G18/8048 , C08G18/8077 , C09D175/04
摘要： The present invention relates to the preparation of aqueous, cosolvent-free polyurethane dispersions with blocked isocyanate groups, to baking varnishes prepared from them, and to their use in coatings.
摘要翻译：本发明涉及制备具有封闭的异氰酸酯基团的无溶剂的无溶剂聚氨酯分散体，以烘烤由它们制备的清漆，以及它们在涂料中的用途。

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