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81. 发明授权

US4940570A Beryllium-aluminum-phosphorus-oxide molecular sieve compositions 失效
标题翻译：铍 - 铝 - 氧化磷分子筛组合物
公开(公告)号：US4940570A
公开(公告)日：1990-07-10
申请号：US835293
申请日：1986-03-03
申请人： Edith M. Flanigen , Brent M. Lok , Robert L. Patton , Stephen T. Wilson
发明人： Edith M. Flanigen , Brent M. Lok , Robert L. Patton , Stephen T. Wilson
IPC分类号： B01J29/84 , C01B25/45 , C01B37/06 , C07C2/12 , C07C2/54 , C07C5/02 , C07C5/22 , C07C5/27 , C07C5/41
CPC分类号： C07C5/41 , B01J29/84 , C01B37/06 , C07C2/12 , C07C2/54 , C07C5/02 , C07C5/224 , C07C5/2716 , C07C2527/173 , C07C2529/84
摘要： Molecular sieve compositions having three-dimensional microporous framework structures of BeO.sub.2, AlO.sub.2 and PO.sub.2 tetrahedral oxide units are disclosed. These molecular sieves have an empirical chemical composition on an anhydrous basis expressed by the formula:mR:(Be.sub.x Al.sub.y P.sub.z)O.sub.2wherein "R" represents at least one organic templating agent present in the intracrystalline pore system; "m" represents the molar amount of "R" present per mole of (Be.sub.x Al.sub.y P.sub.z)O.sub.2 ; and "x", "y" and "z" represent the mole fractions of beryllium, aluminum and phosphorus, respectively, present as tetrahedral oxides. Their use as adsorbents, catalysts, etc. is also disclosed.
摘要翻译：公开了具有BeO 2，AlO 2和PO 2四面体氧化物单元的三维微孔骨架结构的分子筛组合物。这些分子筛具有由下式表示的无水基础上的经验化学组成：mR：（BexAlyPz）O 2，其中“R”表示存在于晶体内孔系统中的至少一种有机模板剂; “m”表示每摩尔（BexAlyPz）O 2存在的“R”摩尔量; 和“x”，“y”和“z”分别表示作为四面体氧化物存在的铍，铝和磷的摩尔分数。还公开了它们作为吸附剂，催化剂等的用途。

82. 发明授权

US4861743A Process for the production of molecular sieves 失效
标题翻译：生产分子筛的方法
公开(公告)号：US4861743A
公开(公告)日：1989-08-29
申请号：US126192
申请日：1987-11-25
申请人： William H. Flank , Stephen T. Wilson , Julio C. Marte , Edith M. Flanigen
发明人： William H. Flank , Stephen T. Wilson , Julio C. Marte , Edith M. Flanigen
IPC分类号： B01J27/16 , B01J29/03 , B01J29/84 , C01B37/04 , C01B37/06 , C01B37/08
CPC分类号： C01B37/08 , B01J29/84 , C01B37/04 , C01B37/06 , B01J2229/64
摘要： Non-zeolitic molecular sieves are prepared by contacting a body of alumina or silica-alumina (optionally containing reactive sources of phosphorus pentoxide and/or other elements desired in the non-zeolitic molecular sieve) with a liquid reaction mixture containing a reactive source of phosphorus pentoxide (and optionally reactive sources of silica and/or other elements desired in the non-zeolitic molecular sieve), and an organic templating agent, thereby causing the body to react with the liquid reaction mixture and to form crystals of the non-zeolitic molecular sieve within the body.

83. 发明授权

US4853197A Crystalline metal aluminophosphates 失效
标题翻译：结晶金属铝磷酸盐
公开(公告)号：US4853197A
公开(公告)日：1989-08-01
申请号：US58032
申请日：1987-06-04
申请人： Stephen T. Wilson , William C. Mercer
发明人： Stephen T. Wilson , William C. Mercer
IPC分类号： C01B25/45 , B01J29/83 , B01J29/85 , C01B37/06
CPC分类号： B01J29/85 , C01B39/00
摘要： Crystalline microporous metal aluminophosphates wherein the metal is at least one of Co, Mg, Mn, Fe and Zn are provided having the -43, and -50 structures.

84. 发明授权

US4759919A Chromium-aluminum-phosphorus-oxide molecular sieve compositions 失效
标题翻译：铬 - 铝 - 氧化磷分子筛组成
公开(公告)号：US4759919A
公开(公告)日：1988-07-26
申请号：US830756
申请日：1986-02-19
申请人： Edith M. Flanigen , Brent M. T. Lok , Robert L. Patton , Stephen T. Wilson
发明人： Edith M. Flanigen , Brent M. T. Lok , Robert L. Patton , Stephen T. Wilson
IPC分类号： B01J29/84 , C01B25/45 , C01B25/00
CPC分类号： B01J29/84 , C01B39/00 , C07C2527/173 , C07C2529/84
摘要： Molecular sieve compositions having three-dimensional microporous framework structures of CrO.sub.2, AlO.sub.2 and PO.sub.2 tetrahedral oxide units are disclosed. These molecular sieves have an empirical chemical composition on an anhydrous basis expressed by the formula:mR:(Cr.sub.x Al.sub.y P.sub.z)O.sub.2wherein "R" represents at least one organic templating agent present in the intracrystalline pore system; "m" represents the molar amount of "R" present per mole of (Cr.sub.x Al.sub.y P.sub.z)O.sub.2 ; and "x", "y" and "z" represent the mole fractions of chromium, aluminum and phosphorus, respectively, present as tetrahedral oxides. Their use as adsorbents, catalysts, etc. is also disclosed.
摘要翻译：公开了具有CrO 2，AlO 2和PO 2四面体氧化物单元的三维微孔骨架结构的分子筛组合物。这些分子筛具有无水基础上的经验化学组成，由下式表示：mR：（CrxAlyPz）O 2其中“R”表示存在于晶体内孔系统中的至少一种有机模板剂; “m”表示每摩尔（CrxAlyPz）O 2存在的“R”摩尔量; 和“x”，“y”和“z”分别表示作为四面体氧化物存在的铬，铝和磷的摩尔分数。还公开了它们作为吸附剂，催化剂等的用途。

85. 发明授权

US4310440A Crystalline metallophosphate compositions 失效
标题翻译：结晶金属磷酸盐组合物
公开(公告)号：US4310440A
公开(公告)日：1982-01-12
申请号：US166333
申请日：1980-07-07
申请人： Stephen T. Wilson , Brent M. Lok , Edith M. Flanigen
发明人： Stephen T. Wilson , Brent M. Lok , Edith M. Flanigen
IPC分类号： B01D53/28 , B01J20/02 , B01J20/08 , B01J29/04 , B01J29/83 , B01J29/84 , C01B25/36 , C01B37/04 , C07B61/00 , C07C1/00 , C07C2/54 , C07C2/66 , C07C4/18 , C07C5/02 , C07C5/22 , C07C5/27 , C07C5/41 , C07C6/12 , C07C15/08 , C07C67/00 , C10G11/02 , C10G35/06 , C10G45/04 , C10G47/02 , B01J27/14 , B01J31/02 , C01B15/16
CPC分类号： C07C5/224 , B01J20/0292 , B01J29/84 , C01B37/04 , C07C2/54 , C07C5/02 , C07C5/2716 , C07C2529/83 , Y10S502/51 , Y10S502/511
摘要： A novel family of crystalline, microporous aluminophosphate compositions is synthesized by hydrothermal crystallization at elevated temperatures of aluminophosphate gels containing a molecular structure-forming template. The family comprises a number of distinct species, each with a unique crystal structure. Calcination removes volatile extraneous matter from the intracrystalline void space and yields microporous crystalline adsorbents with uniform pores, the dimensions of which vary, among the individual species, from about 3A to 10A in diameter. The compositions represent a new class of adsorbents of the molecular sieve type, and also exhibit properties somewhat analogous to zeolitic molecular sieves which render them useful as catalysts or catalyst bases in chemical reactions such as hydrocarbon conversions.
摘要翻译：通过在含有分子结构形成模板的磷酸铝凝胶的升高温度下水热结晶合成了一系列结晶的微孔磷酸铝组合物。家庭包括许多不同的物种，每个都有独特的晶体结构。焙烧从晶体间隙空间中除去挥发性的外来物质，并产生具有均匀孔隙的微孔结晶吸附剂，其尺寸在各个物种之间变化，直径为约3A至10A。该组合物代表了一类新型的分子筛型吸附剂，并且还表现出与沸石分子筛有些类似的特性，使得它们可用作化学反应如烃转化中的催化剂或催化剂。

86. 发明授权

US08816003B2 High plasticization-resistant cross-linked polymeric membranes for separations 有权
标题翻译：用于分离的高增塑抗性交联聚合物膜
公开(公告)号：US08816003B2
公开(公告)日：2014-08-26
申请号：US12145153
申请日：2008-06-24
申请人： Chunqing Liu , Stephen T. Wilson , David A. Lesch
发明人： Chunqing Liu , Stephen T. Wilson , David A. Lesch
IPC分类号： C08F12/22
CPC分类号： C08B15/10 , B01D53/228 , B01D67/0093 , B01D71/16 , B01D2323/30 , B01D2325/30 , C08G18/6484 , C08L71/02 , C08L81/06 , Y02P20/152
摘要： This invention involves a composition, a method of making, and an application of high plasticization-resistant chemically cross-linked polymeric membranes such as cross-linked cellulose acetate (CA) membrane. These cross-linked polymeric membranes with covalently interpolymer-chain-connected rigid networks showed no decrease in CO2/CH4 ideal selectivity under 690 kPa (100 psig) pure CO2 pressure and also no CO2 plasticization up to 3447 kPa (500 psig) pure CO2 pressure. By using the method of chemical cross-linking as described in this invention, the separation characteristics of the polymeric membranes can be decisively improved. These new cross-linked polymeric membranes can be used not only for gas separations such as CO2/CH4 and CO2/N2 separations, O2/N2 separation, olefin/paraffin separations (e.g. propylene/propane separation), iso/normal paraffins separations, but also for liquid separations such as pervaporation and desalination.
摘要翻译：本发明涉及一种组合物，制备方法，以及应用高耐增塑作用的化学交联聚合物膜，例如交联乙酸纤维素（CA）膜。这些具有共价互聚链连接的刚性网络的交联聚合物膜在690kPa（100psig）纯二氧化碳压力下没有显示CO 2 / CH 4理想选择性的降低，并且也没有CO2增塑达3447kPa（500psig）纯二氧化碳压力。通过使用如本发明所述的化学交联方法，可以确定地提高聚合物膜的分离特性。这些新的交联聚合物膜不仅可用于气体分离，如CO2 / CH4和CO2 / N2分离，O2 / N2分离，烯烃/石蜡分离（如丙烯/丙烷分离），异/正链烷烃分离，但还用于液体分离，例如渗透蒸发和脱盐。

87. 发明授权

US08540800B2 Microporous UZM-5 inorganic zeolite membranes for gas, vapor, and liquid separations 失效
标题翻译：用于气体，蒸汽和液体分离的微孔UZM-5无机沸石膜
公开(公告)号：US08540800B2
公开(公告)日：2013-09-24
申请号：US13052720
申请日：2011-03-21
申请人： Chunqing Liu , Jaime G. Moscoso , Stephen T. Wilson
发明人： Chunqing Liu , Jaime G. Moscoso , Stephen T. Wilson
IPC分类号： B01D53/22 , B01D71/02
CPC分类号： B01D71/028 , B01D53/228 , B01D67/0048 , B01D67/0051 , B01D67/0088 , B01D69/10 , B01D2323/14 , B01J20/186 , B01J20/28007 , B01J20/28035 , B01J20/3057 , B01J20/3078 , B01J20/3085 , B01J20/3238 , B01J20/3272 , B82Y30/00
摘要： The present invention discloses microporous UZM-5 zeolite membranes, methods for making the same, and methods of separating gases, vapors, and liquids using the same. The small-pore microporous UZM-5 zeolite membrane is prepared by two different methods, including in-situ crystallization of one or more layers of UZM-5 zeolite crystals on a porous membrane support, and a seeding method by in-situ crystallization of a continuous second layer of UZM-5 zeolite crystals on a seed layer of UZM-5 zeolite crystals supported on a porous membrane support. The membranes in the form of disks, tubes, or hollow fibers have superior thermal and chemical stability, good erosion resistance, high CO2 plasticization resistance, and significantly improved selectivity over polymer membranes for gas, vapor, and liquid separations.
摘要翻译：本发明公开了微孔UZM-5沸石膜，其制造方法，以及使用其分离气体，蒸汽和液体的方法。小孔微孔UZM-5沸石膜通过两种不同的方法制备，包括在多孔膜载体上的一层或多层UZM-5沸石晶体的原位结晶，以及通过原位结晶的接种方法在支撑在多孔膜载体上的UZM-5沸石晶种的种子层上连续的第二层UZM-5沸石晶体。圆盘，管或中空纤维形式的膜具有优异的热稳定性和化学稳定性，良好的抗侵蚀性，高的二氧化碳抗塑化性，并且对于气体，蒸汽和液体分离，在聚合物膜上显着提高了选择性。

88. 发明申请

US20120240763A1 MICROPOROUS UZM-5 INORGANIC ZEOLITE MEMBRANES FOR GAS, VAPOR, AND LIQUID SEPARATIONS 失效
标题翻译：用于气体，蒸气和液体分离的微波UZM-5无机沸石膜
公开(公告)号：US20120240763A1
公开(公告)日：2012-09-27
申请号：US13052720
申请日：2011-03-21
申请人： Chunqing Liu , Jaime G. Moscoso , Stephen T. Wilson
发明人： Chunqing Liu , Jaime G. Moscoso , Stephen T. Wilson
IPC分类号： B01D53/22 , B01J20/32
CPC分类号： B01D71/028 , B01D53/228 , B01D67/0048 , B01D67/0051 , B01D67/0088 , B01D69/10 , B01D2323/14 , B01J20/186 , B01J20/28007 , B01J20/28035 , B01J20/3057 , B01J20/3078 , B01J20/3085 , B01J20/3238 , B01J20/3272 , B82Y30/00
摘要： The present invention discloses microporous UZM-5 zeolite membranes, methods for making the same, and methods of separating gases, vapors, and liquids using the same. The small-pore microporous UZM-5 zeolite membrane is prepared by two different methods, including in-situ crystallization of one or more layers of UZM-5 zeolite crystals on a porous membrane support, and a seeding method by in-situ crystallization of a continuous second layer of UZM-5 zeolite crystals on a seed layer of UZM-5 zeolite crystals supported on a porous membrane support. The membranes in the form of disks, tubes, or hollow fibers have superior thermal and chemical stability, good erosion resistance, high CO2 plasticization resistance, and significantly improved selectivity over polymer membranes for gas, vapor, and liquid separations.
摘要翻译：本发明公开了微孔UZM-5沸石膜，其制造方法，以及使用其分离气体，蒸汽和液体的方法。小孔微孔UZM-5沸石膜通过两种不同的方法制备，包括在多孔膜载体上的一层或多层UZM-5沸石晶体的原位结晶，以及通过原位结晶的接种方法在支撑在多孔膜载体上的UZM-5沸石晶种的种子层上连续的第二层UZM-5沸石晶体。圆盘，管或中空纤维形式的膜具有优异的热稳定性和化学稳定性，良好的抗侵蚀性，高的二氧化碳抗塑化性，并且对于气体，蒸汽和液体分离，在聚合物膜上显着提高了选择性。

89. 发明授权

US08083833B2 Flexible template-directed microporous partially pyrolyzed polymeric membranes 有权
标题翻译：灵活的模板定向微孔部分热解聚合物膜
公开(公告)号：US08083833B2
公开(公告)日：2011-12-27
申请号：US11679160
申请日：2007-02-26
申请人： Chunqing Liu , David A. Lesch , Stephen T. Wilson
发明人： Chunqing Liu , David A. Lesch , Stephen T. Wilson
IPC分类号： B01D53/22
CPC分类号： B01D53/228 , B01D67/003 , B01D71/64 , B01D2323/08 , B01D2323/24 , Y02C10/10
摘要： This invention describes a new concept of flexible template-directed microporous partially pyrolyzed polymeric membranes which have greatly improved performance in separation of gas pairs compared to their precursor polymeric membranes. Organic hosts, such as crown ethers, cyclodextrins (CDs), calixarenes (CXs), and spherands, or polymeric additives, such as poly(ethylene glycol) (PEG) and polyvinylpyrrolidone (PVP) were used as the micropore-forming templates. Micropore-forming template/polymer blend membranes comprising organic micropore-forming templates embedded in a polymer matrix were prepared by dissolving the organic micropore-forming templates in the polymer solution followed by solution-casting and solvent evaporation or solvent exchange. Low-temperature selectively pyrolyzing micropore-forming templates in the micropore-forming template/polymer blend membranes at a nitrogen flow resulted in the formation of flexible microporous partially pyrolyzed polymeric membranes.
摘要翻译：本发明描述了柔性模板定向的微孔部分热解的聚合物膜的新概念，其与其前体聚合物膜相比具有大大改进气体对分离的性能。使用有机主体，例如冠醚，环糊精（CDs），杯芳烃（CXs）和花粉，或聚合物添加剂如聚（乙二醇）（PEG）和聚乙烯吡咯烷酮（PVP））作为微孔形成模板。通过将有机微孔形成模板溶解在聚合物溶液中，然后进行溶液流延和溶剂蒸发或溶剂交换来制备包含嵌入聚合物基质中的有机微孔形成模板的微孔形成模板/聚合物共混膜。在微孔形成模板/聚合物共混膜中的氮气流下的低温选择性热解微孔形成模板导致柔性微孔部分热解聚合物膜的形成。

90. 发明授权

US07806962B2 Cross-linkable and cross-linked mixed matrix membranes and methods of making the same 有权
标题翻译：可交联和交联的混合基质膜及其制备方法
公开(公告)号：US07806962B2
公开(公告)日：2010-10-05
申请号：US12193897
申请日：2008-08-19
申请人： Chunqing Liu , Jeffrey J. Chiou , Stephen T. Wilson
发明人： Chunqing Liu , Jeffrey J. Chiou , Stephen T. Wilson
IPC分类号： B01D53/22
CPC分类号： B01D53/228 , B01D67/0004 , B01D67/009 , B01D69/02 , B01D69/141 , B01D71/64 , B01D2323/30 , B01D2323/345 , Y02C10/10 , Y02C20/20 , Y10S55/05
摘要： The present invention is for novel high performance cross-linkable and cross-linked mixed matrix membranes and the use of such membranes for separations such as for CO2/CH4, H2/CH4 and propylene/propane separations. More specifically, the invention involves the preparation of cross-linkable and cross-linked mixed matrix membranes (MMMs). The cross-linkable MMMs were prepared by incorporating microporous molecular sieves or soluble high surface area microporous polymers (PIMs) as dispersed microporous fillers into a continuous cross-linkable polymer matrix. The cross-linked MMMs were prepared by UV-cross-linking the cross-linkable MMMs containing cross-linkable polymer matrix such as BP-55 polyimide. Pure gas permeation test results demonstrated that both types of MMMs exhibited higher performance for CO2/CH4 and H2/CH4 separations than those of the corresponding cross-linkable and cross-linked pure polymer matrices.
摘要翻译：本发明是用于新型高性能可交联和交联的混合基质膜，以及这种膜用于分离的用途，例如用于CO 2 / CH 4，H 2 / CH 4和丙烯/丙烷分离。更具体地，本发明涉及可交联和交联的混合基质膜（MMM）的制备。通过将微孔分子筛或可溶性高表面积微孔聚合物（PIM）作为分散的微孔填料掺入连续可交联的聚合物基质中来制备可交联的MMM。交联的MMM通过UV-交联含有可交联聚合物基质如BP-55聚酰亚胺的可交联MMM制备。纯气体渗透测试结果表明，两种类型的MMM对于CO 2 / CH 4和H 2 / CH 4分离显示出比相应的可交联和交联纯聚合物基质更高的性能。

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