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71. 发明申请

US20120202006A1 ZEOLITE COMPOSITIONS AND METHODS FOR TAILORING ZEOLITE CRYSTAL HABITS WITH GROWTH MODIFIERS 审中-公开
标题翻译：沸石组合物和使用生长改性剂调配沸石晶体的方法
公开(公告)号：US20120202006A1
公开(公告)日：2012-08-09
申请号：US13366206
申请日：2012-02-03
申请人： Jeffrey D. Rimer
发明人： Jeffrey D. Rimer
IPC分类号： B32B3/10 , C30B7/14
CPC分类号： C01B39/40 , C01B37/02 , C01B37/08 , C01B39/265 , C01B39/32 , C01B39/445 , C01B39/54 , Y10T428/24273
摘要： Embodiments of the invention generally provide compositions of crystalline zeolite materials with tailored crystal habits and the methods for forming such crystalline zeolite materials. The methods for forming the crystalline zeolite materials include binding one or more zeolite growth modifiers (ZGMs) to the surface of a zeolite crystal, which results in the modification of crystal growth rates along different crystallographic directions, leading to the formation of zeolites having a tailored crystal habit. The improved properties enabled by the tailored crystal habit include a minimized crystal thickness, a shortened internal diffusion pathlength, and a greater step density as compared to a zeolite having the native crystal habit prepared by traditional processes. The tailored crystal habit provides the crystalline zeolite materials with an aspect ratio of about 4 or greater and crystal surfaces having a step density of about 25 steps/μm2 or greater.
摘要翻译：本发明的实施方案通常提供具有定制的晶体习惯的结晶沸石材料的组合物和形成这种结晶沸石材料的方法。形成结晶沸石材料的方法包括将一种或多种沸石生长改性剂（ZGM）结合到沸石晶体的表面，这导致沿着不同的晶体方向改变晶体生长速率，导致形成具有定制的沸石水晶习惯与通过传统方法制备的具有天然结晶习性的沸石相比，通过定制的晶体习性实现的改进的性质包括最小化的晶体厚度，缩短的内部扩散路径长度和更大的阶梯密度。定制的晶体习性提供了具有约4或更大的纵横比的结晶沸石材料和具有约25步/μm2或更大的阶梯密度的晶体表面。

72. 发明申请

US20110247548A1 Method For Fabricating Of ZnO Particle And Method For Fabricating Of ZnO Rod 审中-公开
标题翻译： ZnO颗粒的制造方法和ZnO棒的制造方法
公开(公告)号：US20110247548A1
公开(公告)日：2011-10-13
申请号：US13085072
申请日：2011-04-12
申请人： Gun-Young JUNG , Ki-Seok KIM
发明人： Gun-Young JUNG , Ki-Seok KIM
IPC分类号： C30B7/14 , C30B19/00
CPC分类号： C30B29/605 , C30B7/04 , C30B29/16
摘要： Disclosed herein are a method for preparing zinc oxide (ZnO) nanoparticles and a method for preparing ZnO nanorods. The method for preparing ZnO nanoparticles may include: preparing a growth solution containing a zinc salt, a precipitator, and a growth inhibitor; and applying heat to the growth solution to prepare ZnO nanoparticles. Moreover, the method for preparing ZnO nanorods may include: forming a ZnO seed layer on a substrate; forming a pattern layer including a plurality of holes on the ZnO seed layer; preparing a growth solution containing a zinc salt, a precipitator, and a growth inhibitor; and immersing the substrate including the pattern layer in the growth solution such that ZnO nanorods are grown in the holes.
摘要翻译：本文公开了一种制备氧化锌（ZnO）纳米颗粒的方法和一种制备ZnO纳米棒的方法。制备ZnO纳米颗粒的方法可包括：制备含锌盐，沉淀剂和生长抑制剂的生长溶液; 并向生长溶液施加热量以制备ZnO纳米颗粒。此外，制备ZnO纳米棒的方法可以包括：在衬底上形成ZnO种子层; 在所述ZnO种子层上形成包括多个孔的图案层; 制备含有锌盐，沉淀剂和生长抑制剂的生长溶液; 将含有图案层的基板浸渍在生长溶液中，使ZnO纳米棒在孔中生长。

73. 发明授权

US07811381B2 Antisolvent crystallization in porous hollow fiber devices and methods of use thereof 有权
标题翻译：多孔中空纤维装置中的抗溶剂结晶及其使用方法
公开(公告)号：US07811381B2
公开(公告)日：2010-10-12
申请号：US11811557
申请日：2007-06-11
申请人： Kamalesh K. Sirkar , Dimitrios Zarkadas
发明人： Kamalesh K. Sirkar , Dimitrios Zarkadas
IPC分类号： C30B7/14
CPC分类号： C13K1/10 , B01D63/02 , B01D69/082 , B01D2323/225
摘要： Antisolvent crystallization systems and methods are provided that employ porous hollow fiber membranes. The porous hollow fiber membrane includes a plurality of porous hollow fibers positioned within a shell, each porous hollow fiber defining a lumen side and shell side. A crystallizing solution is introduced to one side of the hollow fibers and an antisolvent is introduced to the other side of the fibers, in either cocurrent or countercurrent flow. One of the antisolvent and the crystallizing solution permeates in part through the porous hollow fiber membrane to the other side and crystals are formed thereby. Permeation of the antisolvent or the crystallizing solution establishes advantageous radial mixing that facilitates crystal formation of a desired size distribution. Downstream mixing, e.g., a completely stirred tank or a static mixer, may be employed to further improve crystallization operations.
摘要翻译：提供了使用多孔中空纤维膜的抗溶剂结晶体系和方法。多孔中空纤维膜包括位于壳内的多个多孔中空纤维，每个多孔中空纤维限定内腔侧和外壳侧。将结晶溶液引入中空纤维的一侧，并将反溶剂以并流或逆流流入纤维的另一侧。反溶剂和结晶溶液中的一种通过多孔中空纤维膜渗透到另一侧，由此形成晶体。反溶剂或结晶溶液的渗透产生有利的径向混合，其有利于所需尺寸分布的晶体形成。可以使用下游混合，例如完全搅拌的罐或静态混合器，以进一步改善结晶操作。

74. 发明授权

US07704321B2 Polycrystalline material having a plurality of single crystal particles 失效
标题翻译：具有多个单晶粒子的多晶材料
公开(公告)号：US07704321B2
公开(公告)日：2010-04-27
申请号：US11062273
申请日：2005-02-18
申请人： Richard Riman , Larry McCandlish , Xiangyuan Liu
发明人： Richard Riman , Larry McCandlish , Xiangyuan Liu
IPC分类号： C30B7/14
CPC分类号： C01G23/003 , C01G25/006 , C01P2002/60 , C01P2004/03 , C01P2004/20 , C01P2004/30 , C01P2004/60
摘要： Polycrystalline materials of macroscopic size exhibiting Single-Crystal-Like properties are formed from a plurality of Single-Crystal Particles, having Self-Aligning morphologies and optionally bonded together and aligned along at least one, and up to three, crystallographic directions.
摘要翻译：具有单晶样性质的宏观尺寸的多晶材料由具有自对准形态并可任选地结合在一起并沿着至少一个晶体学方向和至多三个结晶方向排列的多个单晶体颗粒形成。

75. 发明授权

US07195670B2 High throughput screening of crystallization of materials 有权
标题翻译：高通量筛选材料结晶
公开(公告)号：US07195670B2
公开(公告)日：2007-03-27
申请号：US10117978
申请日：2002-04-05
申请人： Carl L. Hansen , Stephen R. Quake , James M. Berger
发明人： Carl L. Hansen , Stephen R. Quake , James M. Berger
IPC分类号： C30B7/14
CPC分类号： C30B7/08 , B01J2219/00274 , B01L3/06 , B01L3/502707 , B01L3/50273 , B01L3/502738 , B01L3/502761 , B01L7/54 , B01L9/527 , B01L2200/025 , B01L2200/027 , B01L2200/0605 , B01L2200/0642 , B01L2200/10 , B01L2300/0681 , B01L2300/0816 , B01L2300/0861 , B01L2300/0864 , B01L2300/0887 , B01L2300/123 , B01L2300/14 , B01L2300/18 , B01L2300/1827 , B01L2400/0481 , B01L2400/049 , B01L2400/0638 , B01L2400/0655 , B01L2400/0688 , C12Q1/6874 , C30B7/14 , F04B43/043 , F16K99/0001 , F16K99/0015 , F16K99/0026 , F16K99/0034 , F16K99/0059 , F16K2099/0074 , F16K2099/0078 , F16K2099/008 , F16K2099/0084 , F16K2099/0094 , Y10T117/1004 , Y10T117/1008 , Y10T137/0318 , Y10T137/0396 , C12Q2535/125
摘要： High throughput screening of crystallization of a target material is accomplished by simultaneously introducing a solution of the target material into a plurality of chambers of a microfabricated fluidic device. The microfabricated fluidic device is then manipulated to vary the solution condition in the chambers, thereby simultaneously providing a large number of crystallization environments. Control over changed solution conditions may result from a variety of techniques, including but not limited to metering volumes of crystallizing agent into the chamber by volume exclusion, by entrapment of volumes of crystallizing agent determined by the dimensions of the microfabricated structure, or by cross-channel injection of sample and crystallizing agent into an array of junctions defined by intersecting orthogonal flow channels.
摘要翻译：目标材料的结晶化的高通量筛选是通过将目标材料的溶液同时引入微细加工的流体装置的多个室来实现的。然后对微制造的流体装置进行操作以改变室中的溶液状态，从而同时提供大量的结晶环境。改变的溶液条件的控制可以由各种技术产生，包括但不限于通过体积排阻将结晶剂计量到室中的体积，通过捕获通过微结构结构的尺寸确定的结晶剂的体积，将样品和结晶剂通道注入由相交的正交流动通道限定的连接阵列。

76. 发明申请

US20050120946A1 Synthesis of colloidal PbS nanocrystals with size tunable NIR emission 失效
标题翻译：具有大小可调谐近红外发射的胶体PbS纳米晶体的合成
公开(公告)号：US20050120946A1
公开(公告)日：2005-06-09
申请号：US10727821
申请日：2003-12-04
申请人： Margaret Hines , Gregory Scholes
发明人： Margaret Hines , Gregory Scholes
IPC分类号： C30B7/14 , C30B29/46 , C30B29/60 , C30B7/00 , C30B21/02 , C30B28/06
CPC分类号： B82Y30/00 , B82Y10/00 , C30B7/00 , C30B7/14 , C30B29/46 , C30B29/605
摘要： The present invention discloses a method for synthesis of narrowly dipsersed colloidal PbS nanocrystals that offer size-tunable near-infrared emission. The stability and processibility of these near-infrared emitting quantum dots makes them ideal materials for device applications. The use of cost-effective and non-pyrophoric precursors as well as the success of larger scale reactions means the present invention provides a method for the industrial scale production of PbS nanocrystals.
摘要翻译：本发明公开了一种合成狭窄倾斜胶体PbS纳米晶体的方法，其提供尺寸可调的近红外发射。这些近红外发射量子点的稳定性和加工性使其成为器件应用的理想材料。使用成本效益和非发火前体以及大规模反应的成功意味着本发明提供了一种用于工业规模生产PbS纳米晶体的方法。

77. 发明授权

US5454344A System for polymer crystallization 失效
标题翻译：聚合物结晶体系
公开(公告)号：US5454344A
公开(公告)日：1995-10-03
申请号：US340594
申请日：1994-11-16
申请人： Ilya Pikus , Greg J. Kimball , Masayuki Inoue
发明人： Ilya Pikus , Greg J. Kimball , Masayuki Inoue
IPC分类号： B29B13/02 , B01F7/00 , B01F15/06 , B01J19/18 , B29B13/06 , C08G63/80 , C30B7/14
CPC分类号： B01J19/18 , B01F15/068 , B29B13/065 , B29B7/44 , B29B7/82 , C08G63/80 , B01F7/0045 , B01J2219/00085 , B01J2219/00155 , B01J2219/00166 , B01J2219/00182 , B01J2219/182 , B29K2067/00 , Y10T117/1016 , Y10T117/1024
摘要： A system for crystallization of polymers involving the use of a stationary housing with a rotor mounted for rotation within the housing. The rotor supports a plurality of spaced apart hollow discs and heated fluid is delivered to the interior of the discs. The polymer material to be treated is fed into the housing for heat exchange contact with the exterior surfaces of the discs. The rotation of the discs in addition serves as the propelling force for the material along the length of the housing at which point the material is discharged. The speed of rotation of the rotor is controlled to influence agitation and conveying of material in the housing to thereby control the crystallization reaction. A holdup mechanism which operates independently of the speed control is located adjacent the discharge location to contribute to the fixing of the residence time. The material inlet operation, discharge operation and residence control are such that the ratio of crystallized to uncrystallized material is maintained within desired limits, typically at about 4 to 1. The method and apparatus provides various other operating parameters and structural features which maximize the efficiency of the crystallization reaction.
摘要翻译：一种用于结晶聚合物的系统，涉及使用具有安装在壳体内旋转的转子的固定壳体。转子支撑多个间隔开的中空盘，并且加热的流体被输送到盘的内部。要处理的聚合物材料被供给到壳体中以与盘的外表面进行热交换接触。此外，盘的旋转作为沿着壳体的长度的材料的推进力，在该点材料被排出。控制转子的旋转速度以影响壳体中材料的搅拌和输送，从而控制结晶反应。独立于速度控制运行的保持机构位于排放位置附近以有助于固定停留时间。材料入口操作，排放操作和停留控制使得结晶化与未结晶材料的比例保持在期望的限度内，通常为约4:1。该方法和设备提供了各种其它操作参数和结构特征，其使效率最大化结晶反应。

78. 发明授权

US5281405A Optically useful compositions and a sol-gel process for their production 失效
标题翻译：光学上有用的组合物和其生产的溶胶 - 凝胶法
公开(公告)号：US5281405A
公开(公告)日：1994-01-25
申请号：US838589
申请日：1992-02-19
申请人： Mark A. Harmer
发明人： Mark A. Harmer
IPC分类号： C30B7/14 , C01B25/45 , C30B5/00 , C30B29/22 , G02B6/13 , G02F1/355 , C01B25/26 , C01G23/00 , C01G28/02 , C03C3/00
CPC分类号： G02B6/13 , C01B25/45 , C01B25/451 , C30B29/10 , C30B29/14 , C30B5/00 , G02F1/3553
摘要： A sol-gel process is disclosed for preparing MTiOXO.sub.4 when M is K, Rb, Tl and/or NH.sub.4 and X is P and/or As which involves dissolving suitable compounds of M, Ti and X in stoichiometic amounts in a suitable organic liquid, and then producing crystalline MTiOXO.sub.4 using procedures including hydrolysis, condensation, solidification and pyrolysis. Bulk material and films (e.g., films of KTP on a single crystal silicon substrate) may be produced. Compositions comprising films of said MTiOXO.sub.4 produced by this process are disclosed.
摘要翻译：公开了当M为K，Rb，T1和/或NH4且X为P时制备MTiOXO4的溶胶 - 凝胶法和/或As，其涉及以合适的有机液体中化学计量的M，Ti和X的合适化合物溶解，然后使用包括水解，缩合，固化和热解的方法制备结晶MTiOXO4。可以制造块状材料和膜（例如，单晶硅衬底上的KTP的膜）。公开了包含通过该方法生产的所述MTiOXO4的膜的组合物。

79. 发明授权

US4833233A Human serum albumin crystals and method of preparation 失效
标题翻译：人血清白蛋白晶体及其制备方法
公开(公告)号：US4833233A
公开(公告)日：1989-05-23
申请号：US87281
申请日：1987-08-20
申请人： Daniel C. Carter
发明人： Daniel C. Carter
IPC分类号： C30B7/14 , C07K1/14 , C07K14/435 , C07K14/76 , C07K14/765 , C30B7/00 , C30B29/58
CPC分类号： C07K14/765 , C30B29/58 , C30B7/00 , Y10T428/30 , Y10T428/31536 , Y10T428/31768
摘要： HSA crystals are provided in the form of tetragonal plates having the space groups P42.sub.1 2, the crystals being grown to sizes in excess of 0.5 mm in two dimensions and a thickness of 0.1 mm. Growth of the crystals is carried out by a hanging drop method wherein a precipitant solution containing PEG and a phosphate buffer is mixed with an HSA solution, and a droplet of mixed solution is suspended over a well of precipitant solution. Crystals grow to the desired size in 3 to 7 days. Concentration of reagents, pH and other parameters are controlled within prescribed limits. The resulting crystals exhibit a size and quality such as to allow performance of x-ray diffraction studies and enable the conduct of drug binding studies as well as genetic engineering studies.

80. 发明授权

US4489133A Two-dimensional crystallization technique 失效
标题翻译：二维结晶技术
公开(公告)号：US4489133A
公开(公告)日：1984-12-18
申请号：US442066
申请日：1982-11-16
申请人： Roger D. Kornberg
发明人： Roger D. Kornberg
IPC分类号： G01N33/50 , A61K9/127 , B05D1/18 , B05D1/20 , C07K1/00 , C07K16/00 , C30B7/00 , C30B7/14 , C30B29/54 , G01N33/543 , B32B9/00
CPC分类号： C30B7/14 , A61K9/127 , A61K9/1274 , B05D1/185 , B82Y30/00 , B82Y40/00 , C30B29/54 , C30B7/00 , B05D1/202 , Y10T428/30 , Y10T428/31536 , Y10T428/31768
摘要： Methods and compositions involving two-dimensional ordering of organic polar solvent soluble organic macromolecules. Lipid monolayer forming molecules are bound covalently or non-covalently to organic macromolecules soluble in polar solvents, whereby the macromolecules are allowed to become oriented in two-dimensions to form an ordered, low free energy, including crystalline, layer of macromolecules. The macromolecules may then be further combined with other moieties to create additional layers, to be cross-linked or otherwise modified, and/or separated from the lipid monolayer. The resulting ordered layers can be used for a variety of purposes, in crystallographic techniques for structure determination and structural relationship determinations, in optics, as polymers, films, and the like.
摘要翻译：涉及有机极性溶剂可溶性有机大分子二维排序的方法和组成。脂质单层形成分子与可溶于极性溶剂的有机大分子共价或非共价结合，从而允许大分子二维取向以形成有序的低自由能，包括结晶的大分子层。然后可以将大分子与其它部分进一步组合以产生要与脂质单层交联或以其它方式修饰和/或分离的另外的层。所得到的有序层可以用于各种目的，在用于结构确定和结构关系确定的晶体学技术中，在光学中，作为聚合物，膜等。

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