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    • 76. 发明公开
    • PARTICLE DISPERSION AND PROCESS FOR FORMING A PARTICLE DISPERSION
    • US20230227674A1
    • 2023-07-20
    • US18070139
    • 2022-11-28
    • Friedrich-Alexander-Universität Erlangen-Nürnberg
    • Marcel REYNicolas VOGELSharanya NAIR
    • C09D7/65C09D7/62C09D7/20
    • C09D7/65C09D7/62C09D7/20
    • The present invention relates to a process for producing a particle dispersion comprising the steps of: a) providing a dispersion consisting of a solvent and solid core particles, b) providing a solution of a soluble, interfacially-active polymer having a molecular weight of more than 5 kDa, c) mixing said dispersion of solid core particles with said polymer solution, d) removing free polymer from the obtained mixture; wherein in step a) the solvent is selected from an organic solvent, a mixture of at least two organic solvents or a mixture of at least one organic solvent with water; wherein in step c), the amount of the soluble, interfacially-active polymer mixed with said dispersion of solid core particles exceeds the amount of polymer required to coat the surface of each of the solid core particles with a monolayer of the polymer; wherein step d) is repeated until the requirement described by the following formula is fulfilled:


      (STdisp−18 mN/m)/(STsolv−18 mN/m)>0.90,

      with STdisp being the surface tension of the modified particle dispersion in [mN/m] and STsolv being the surface tension of the pure solvent or solvent mixture in [mN/m]; and wherein the solvent or solvent mixture contained in the dispersion of solid core particles is miscible with the solvent or solvent mixture contained in the polymer solution. The present invention also relates to a particle dispersion exhibiting a homogenous drying pattern as well as a film made thereof and the use of the non-aqueous particle dispersion.