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71. 发明授权

US08927788B2 Process to recover alcohol with reduced water from overhead of acid column 有权
标题翻译：从酸塔塔顶馏出水中还原水回收酒精的方法
公开(公告)号：US08927788B2
公开(公告)日：2015-01-06
申请号：US13457280
申请日：2012-04-26
申请人： David Lee , Adam Orosco , Claudio Ribeiro , R. Jay Warner , Robert Alan Deck , Emily Duff , Victor J. Johnston
发明人： David Lee , Adam Orosco , Claudio Ribeiro , R. Jay Warner , Robert Alan Deck , Emily Duff , Victor J. Johnston
IPC分类号： C07C29/149 , C07C29/80 , C07C27/04 , C07C51/12 , C07C67/08 , C07C67/54
CPC分类号： C07C29/149 , C07C29/76 , C07C29/80 , C07C29/84 , C07C51/12 , C07C67/08 , C07C67/54 , C10L1/02 , C10L2200/04 , C10L2290/543 , C10L2290/548 , C07C31/08 , C07C53/08 , C07C69/14
摘要： A process for recovering ethanol obtained from the hydrogenation of acetic acid. The crude ethanol product is separated in a column to produce a distillate stream comprising acetaldehyde and ethyl acetate and a residue stream comprising ethanol, acetic acid, ethyl acetate and water. The ethanol product is recovered from the residue stream.
摘要翻译：一种从乙酸氢化中回收乙醇的方法。将粗乙醇产物在柱中分离以产生包含乙醛和乙酸乙酯的馏出物流和包含乙醇，乙酸，乙酸乙酯和水的残余物流。从残余物流中回收乙醇产物。

72. 发明申请

US20140171671A1 CATALYTIC PROCESSES FOR PREPARING ESTOLIDE BASE OILS 有权
标题翻译：用于制备天花柱酰基油的催化方法
公开(公告)号：US20140171671A1
公开(公告)日：2014-06-19
申请号：US14095750
申请日：2013-12-03
申请人： BIOSYNTHETIC TECHNOLOGIES, LLC
发明人： Travis Thompson , Jakob BREDSGUARD , Jeremy Forest
IPC分类号： C07C67/465 , C07C67/48 , C07C67/54
CPC分类号： B05B1/326 , B05B1/1636 , B05B1/3026 , C07C57/02 , C07C67/465 , C07C67/48 , C07C67/54 , C07C69/34 , C07C69/604 , C07C69/675 , C10M105/34 , C10M105/36 , C10M107/32 , C10M2207/2825 , C10M2207/286 , C10M2209/1023 , C10N2220/022 , C10N2220/023 , C10N2220/024 , C10N2220/027 , C10N2220/028 , C10N2220/10 , C10N2230/02 , C10N2230/64 , C10N2240/04 , C11C3/00 , C11C3/003 , C11C3/08 , Y10T137/86549 , Y10T137/86863
摘要： Provided herein are processes for preparing estolides and estolide base oils from fatty acid reactants utilizing catalysts. Further provided herein are processes for preparing carboxylic esters from at least one carboxylic acid reactant and at least one olefin.
摘要翻译：本文提供了使用催化剂从脂肪酸反应物制备儿茶素和锭子基油的方法。本文还提供了由至少一种羧酸反应物和至少一种烯烃制备羧酸酯的方法。

73. 发明授权

US08562921B2 Ethyl acetate production 有权
标题翻译：乙酸乙酯生产
公开(公告)号：US08562921B2
公开(公告)日：2013-10-22
申请号：US13422743
申请日：2012-03-16
申请人： Sagar B. Gadewar
发明人： Sagar B. Gadewar
IPC分类号： B01J8/04 , B01D3/00 , C07C67/54
CPC分类号： C07C67/40 , B01D3/001 , B01D3/009 , Y02P20/127 , C07C69/14
摘要： A process for the production of high purity ethyl acetate from ethanol is described. The process involves reacting ethanol over a suitable catalyst in a reactive distillation column. The reactive distillation setup allows overcoming the reaction equilibrium for increased conversion of ethanol. Hydrogen is removed as the distillate and ethyl acetate is obtained as a bottoms product from the reactive distillation column. A feed of hydrogen at the bottom of the column and a suitable hydrogenation catalyst placed at the bottom of the column allows for a significant reduction of impurities such as butan-2-one and/or n-butyraldehyde in the ethyl acetate product. Adding side reactors to the reactive distillation column allows additional catalyst holdup for improved reactant conversion.
摘要翻译：描述了从乙醇生产高纯度乙酸乙酯的方法。该方法包括在反应性蒸馏塔中使合适的催化剂上的乙醇反应。反应蒸馏装置允许克服用于提高乙醇转化率的反应平衡。作为馏出物除去氢气，并从反应蒸馏塔作为塔底产物获得乙酸乙酯。在塔底部的氢气进料和位于塔底部的合适的氢化催化剂允许显着降低乙酸乙酯产物中杂质如丁-2-酮和/或正丁醛。将反应器加入反应蒸馏塔允许额外的催化剂保留以改善反应物转化率。

74. 发明授权

US08410307B2 Method for producing vinyl acetate 有权
标题翻译：乙酸乙烯酯的制造方法
公开(公告)号：US08410307B2
公开(公告)日：2013-04-02
申请号：US13574493
申请日：2011-01-14
申请人： Mehmet Guenaltay , Willibald Dafinger , Peter Holl
发明人： Mehmet Guenaltay , Willibald Dafinger , Peter Holl
IPC分类号： C07C67/54 , C07C67/05
CPC分类号： C07C67/055 , C07C67/54 , C07C69/01 , C07C69/15
摘要： A method for producing vinyl acetate in a heterogeneously catalyzed, continuous gas phase process by reacting ethylene with acetic acid and oxygen in a reactor and separating the product gas stream substantially comprising ethylene, vinyl acetate, acetic acid, water, carbon dioxide and inert gases.
摘要翻译：一种通过在反应器中使乙烯与乙酸和氧气反应而在不均匀催化的连续气相方法中生产乙酸乙烯酯的方法，并分离基本上包含乙烯，乙酸乙烯酯，乙酸，水，二氧化碳和惰性气体的产物气流。

75. 发明申请

US20120123147A1 KETOCARBOXYLIC ACIDS, METHODS OF MANUFACTURE AND USES THEREOF 有权
标题翻译：酮羧酸，其制备方法及其用途
公开(公告)号：US20120123147A1
公开(公告)日：2012-05-17
申请号：US13294751
申请日：2011-11-11
申请人： Brian D. MULLEN , Cora M. LEIBIG , Leo E. MANZER
发明人： Brian D. MULLEN , Cora M. LEIBIG , Leo E. MANZER
IPC分类号： C07C51/493 , C07C67/52 , C07C59/347 , C07C67/54 , C07C69/738 , C07C67/60 , C07C67/58
CPC分类号： C07C69/738 , C07C51/09 , C07C51/493 , C07C67/08 , C07C67/52 , C07C69/716 , Y02P20/582 , C07C59/185
摘要： Ketocarboxylic acids such as levulinic acid can be efficiently purified in high yield by esterification with a hydrocarbon polyol to the corresponding polyketocarboxylic ester, which can be readily purified, for example recrystallized. After purification, the ketocarboxylic ester can be hydrolyzed to provide pure ketocarboxylic acid, or a salt thereof, after removal of the esterifying hydrocarbon polyol, or used for other synthetic transformations. Advantageously, the polyketocarboxylic esters, ketocarboxylic acids, and salts thereof produced by this method are obtained in high purity.
摘要翻译：酮羧酸如乙酰丙酸可以通过用烃多元醇与相应的聚酮羧酸酯酯化而以高收率有效地纯化，其可以容易地纯化，例如重结晶。纯化后，在除去酯化烃多元醇之后，可以将酮羧酸酯水解以提供纯酮羧酸或其盐，或用于其它合成转化。有利地，以高纯度获得通过该方法制备的多酮羧酸酯，酮羧酸及其盐。

76. 发明申请

US20110021809A1 Method for Purification of Optically Active alpha-Fluorocarboxylic Acid Esters 有权
标题翻译：光活性α-氟羧酸酯的纯化方法
公开(公告)号：US20110021809A1
公开(公告)日：2011-01-27
申请号：US12673956
申请日：2008-08-05
申请人： Akihiro Ishii , Hideyuki Tsuruta , Yuzuru Morino , Mikihiro Takahashi
发明人： Akihiro Ishii , Hideyuki Tsuruta , Yuzuru Morino , Mikihiro Takahashi
IPC分类号： C07C67/54
CPC分类号： C07B53/00 , C07B57/00 , C07C67/307 , C07C67/54 , C07C69/63
摘要： Disclosed is a purification method of reducing and removing fluoride ions contained in an optically active α-fluorocarboxylic acid ester represented by formula [1] [in the formula, R1 represents a C1-6 alkyl group, R2 represents a C1-4 alkyl group, and * represents an asymmetric carbon], the purification method of the optically active α-fluorocarboxylic acid ester being characterized by that a distillation is conducted in the presence of an organic base. By this method, it is possible to greatly reduce the concentration of fluoride ion traces contained in the optically active α-fluorocarboxylic acid ester by a relatively easy operation. Of the organic base, a tertiary amine is preferable, and above all tri-n-butylamine is particularly preferable.
摘要翻译：公开了通式[1]表示的光学活性α-氟代羧酸酯中所含的氟离子的还原和除去净化方法[式中，R1表示C1-6烷基，R2表示C1-4烷基，和*表示不对称碳]，光学活性α-氟代羧酸酯的纯化方法的特征在于在有机碱的存在下进行蒸馏。通过该方法，可以通过相对容易的操作大大降低光学活性α-氟代羧酸酯中含有的氟离子痕迹的浓度。在有机碱中，优选叔胺，特别优选三正丁胺。

77. 发明授权

US07294240B2 Method for producing (meth)acrylic acid esters 有权
标题翻译：（甲基）丙烯酸酯的制造方法
公开(公告)号：US07294240B2
公开(公告)日：2007-11-13
申请号：US10479962
申请日：2002-05-28
申请人： Matthias Geisendoerfer , Gerhard Nestler , Juergen Schroeder , Hugues Vandenmersch
发明人： Matthias Geisendoerfer , Gerhard Nestler , Juergen Schroeder , Hugues Vandenmersch
IPC分类号： B01D3/34 , C07C213/06 , C07C213/10 , C07C51/44 , C07C67/54
CPC分类号： C07C213/06 , C07C213/10 , Y02P20/582 , Y10S203/20 , Y10S203/22 , Y10S203/90 , C07C219/08
摘要： Basic (meth)acrylates IV are prepared by transesterification of alkyl (meth)acrylates I in the presence of a catalyst and working-up of the reaction mixture by distillation, by a process in which a gas or gas mixture which is inert under the reaction conditions is passed through the reaction zone and/or heat exchanger.
摘要翻译：碱性（甲基）丙烯酸酯IV通过烷基（甲基）丙烯酸烷基酯I在催化剂存在下进行酯交换和通过蒸馏处理反应混合物，通过其中反应惰性气体或气体混合物条件通过反应区和/或热交换器。

79. 发明申请

US20050256332A1 Flourination of dicarbonyl compounds 失效
标题翻译：二羰基化合物的泛化
公开(公告)号：US20050256332A1
公开(公告)日：2005-11-17
申请号：US10505083
申请日：2003-02-19
申请人： John Moilliet
发明人： John Moilliet
IPC分类号： C07C67/307 , C07C20060101 , C07C45/63 , C07C49/167 , C07C51/363 , C07C67/54 , C07C69/003 , C07C69/66 , C07C69/716 , C07C253/30 , C07C25/39
CPC分类号： C07C67/307 , C07C69/716
摘要： The invention provides a method for the preparation of a dicarbonyl compound of formula (I) R1COCFR2COR3 wherein R1 is selected from alkyl, substituted alkyl, cycloalkyl, aryl, substituted aryl and acetoxy, R2 is selected from hydrogen, halogen, nitro, cyano, alkyl, substituted alkyl, cycloalkyl, acetoxy, aryl and substituted aryl, and R3 is selected from alkyl, substituted alkyl, oxyalkyl and substituted oxyalkyl, the method comprising treating a dicarbonyl compound of formula (II) R1COCHR2COR3 with elemental fluorine in a solvent which consists of methanol or aqueous methanol. The method provides an inexpensive and convenient synthetic route to 2-fluoro- and 2,2-difluoro-1,3-diketones and -1,3-ketoesters.
摘要翻译：本发明提供一种制备式（I）的二羰基化合物的方法，其中R 1，R 2，R c，选自烷基，取代的烷基，环烷基，芳基，取代的芳基和乙酰氧基，R 2选自氢，卤素，硝基，氰基，烷基，取代的烷基，环烷基，乙酰氧基，芳基和取代的芳基，R 3选自烷基，取代的烷基，烷氧基和取代的烷氧基，该方法包括处理式（II）的二羰基化合物R 1 COCHR 在由甲醇或甲醇水溶液组成的溶剂中，使用元素氟。该方法为2-氟-2,2-二氟-1,3-二酮和-1,3-酮酯提供了便宜且方便的合成途径。

80. 发明申请

US20050238554A1 Sulfur-bearing residue treatment system 有权
公开(公告)号：US20050238554A1
公开(公告)日：2005-10-27
申请号：US11156142
申请日：2005-06-17
申请人： Curtis Carlson , Michael DeCourcy , Jamie Juliette , Thomas Kaminski , Nicole Koegel , Nelson Quiros , Paul Schladenhauffen , Peter Schmeidler , Robert Maven , William Engle , Arthur Meisch
发明人： Curtis Carlson , Michael DeCourcy , Jamie Juliette , Thomas Kaminski , Nicole Koegel , Nelson Quiros , Paul Schladenhauffen , Peter Schmeidler , Robert Maven , William Engle , Arthur Meisch
IPC分类号： B01D3/16 , B01D1/00 , B01D3/06 , B01D3/32 , B01D3/38 , B01D5/00 , C02F1/20 , C07C51/48 , C07C67/54 , C07C67/62 , C07C69/54 , B01J10/00
CPC分类号： B01D5/0036 , B01D1/0017 , B01D1/0058 , B01D3/06 , B01D3/322 , B01D3/38 , C02F1/20 , C07C51/48 , Y10S159/26 , Y10S203/11 , C07C57/04
摘要： A sulfur-bearing residue treatment system is provided for the recovery of valuable organic components and the reduction of capital costs and operating costs. The treatment system involves the use of a stripping vessel in conjunction with a heating apparatus. All elements of the treatment system may be coupled together to form one integral piece of equipment.

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