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71. 发明申请

US20140287908A1 AGGREGATED GRAPHENE OXIDE AND PREPARING METHOD THEREOF, AGGREGATED GRAPHENE AND PREPARING METHOD THEREOF, AND AGGREGATED AND NITROGEN-DOPED GRAPHENE AND PREPARING METHOD THEREOF 有权
标题翻译：聚集的石墨烯氧化物及其制备方法，聚集的石墨及其制备方法，以及聚集和氮化的石墨及其制备方法
公开(公告)号：US20140287908A1
公开(公告)日：2014-09-25
申请号：US14168284
申请日：2014-01-30
申请人： RESEARCH & BUSINESS FOUNDATION SUNGKYUNKWAN UNIVERSITY
发明人： Hyoyoung LEE , Yeo Heung YOON , Chul BAIK , Keun Sik LEE
IPC分类号： C01B31/04
CPC分类号： C01B31/0446 , C01B31/043 , C01B32/184 , C01B32/23 , C01B2204/32 , Y10T428/2982
摘要： Aggregated graphene oxide includes a range of specific surface area, and a method of preparing aggregated graphene oxide includes dispersing graphene oxide in an organic solvent and adding an anti-solvent. Aggregated graphene includes a range of specific surface area, and a method of preparing aggregated graphene includes dispersing graphene oxide in an organic solvent, adding an anti-solvent, and reducing the aggregated graphene oxide. Aggregated and nitrogen-doped includes a range of specific surface area, and a method of preparing aggregated and nitrogen-doped graphene includes dispersing graphene oxide in an organic solvent, adding an anti-solvent, and photo-reacting the aggregated graphene oxide.
摘要翻译：聚合石墨烯氧化物包括一定范围的比表面积，并且制备聚集的石墨烯氧化物的方法包括将氧化石墨烯分散在有机溶剂中并加入抗溶剂。聚集的石墨烯包括一定范围的比表面积，并且制备聚集的石墨烯的方法包括将氧化石墨烯分散在有机溶剂中，加入反溶剂和还原聚集的石墨烯氧化物。聚集和氮掺杂包括一定范围的比表面积，并且制备聚集和掺杂氮的石墨烯的方法包括将氧化石墨烯分散在有机溶剂中，加入抗溶剂，并对聚集的石墨烯氧化物进行光反应。

72. 发明申请

US20120201738A1 METHOD OF PRODUCING NANO-SIZE GRAPHENE-BASED MATERIAL AND AN EQUIPMENT FOR PRODUCING THE SAME 有权
标题翻译：生产基于纳米尺寸石墨的材料的方法及其生产设备
公开(公告)号：US20120201738A1
公开(公告)日：2012-08-09
申请号：US13389868
申请日：2009-08-11
申请人： Young Jin Kwon , Ja Woon Gu , Won Hyung Park , Cheol Min Shin , Byoung Kyu Ji , Doo Hyo Kwon
发明人： Young Jin Kwon , Ja Woon Gu , Won Hyung Park , Cheol Min Shin , Byoung Kyu Ji , Doo Hyo Kwon
IPC分类号： C01B31/00 , B01J8/08 , B01J8/18 , B82Y30/00 , B82Y40/00
CPC分类号： C01B31/043 , B01J6/004 , B01J19/0093 , B01J2219/0081 , B01J2219/00867 , B01J2219/00873 , B01J2219/00932 , B82Y30/00 , B82Y40/00 , C01B32/182 , C01B32/19 , C01B32/192 , C01B32/23 , C01B2204/04 , C01B2204/32 , Y10S977/734 , Y10S977/847
摘要： The present invention is directed to a method of producing nano-size graphene-based material and an equipment for producing the same. The present invention provides a method of producing graphitic oxide by forcing graphite sulfuric slurry and KMnO4 sulfuric solution into a lengthy micro-channel and by sustaining the mixture of the said graphite sulfuric slurry and the said KMnO4 sulfuric solution in the said micro-channel at predetermined temperatures, by putting the said aqua solution of hydrogen peroxide to the reaction mixture to terminate oxidation, and by washing and drying the reaction mixture. The present invention provides a method of producing nano-size graphene-based material by exfoliating graphitic oxide by thermal shock in a vertical fluidized furnace. According to the present invention, graphitic oxide can be produced massively without risks of explosion by forcing all reagents as liquid phase continuously into a lengthy micro-channel surrounded and thermally controlled strictly by heat exchangers. Nano-size graphene-based material derived by exfoliating thus produced graphitic oxide can be imported into compositions and composites for various uses since it has physical characteristics comparable to carbon nanotube and dispersibility superior to carbon nanotube via residual functional groups.
摘要翻译：本发明涉及一种生产纳米尺寸石墨烯材料的方法及其制造方法。本发明提供了一种通过将石墨硫酸浆料和KMnO 4硫酸溶液强制到长时间的微通道中并通过将预定的所述微通道中的所述石墨硫酸浆料和所述KMnO 4硫酸溶液的混合物维持在所述微通道中的方式来生产石英氧化物的方法通过将所述过氧化氢水溶液置于反应混合物中以终止氧化，并通过洗涤和干燥反应混合物来实现。本发明提供一种通过在垂直流化炉中通过热冲击剥离石墨氧化物来生产纳米级石墨烯材料的方法。根据本发明，通过将所有试剂作为液相连续进入严格由热交换器包围和热控制的长时间的微通道，可以大量生产石墨氧化物而没有爆炸的危险。通过剥离由此产生的石英氧化物衍生的纳米尺寸石墨烯材料可以被导入用于各种用途的组合物和复合材料中，因为其具有与碳纳米管相当的物理特性，并且通过残余官能团优于碳纳米管的分散性。

73. 发明授权

US08192870B2 Supercapacitor and battery electrode containing thermally exfoliated graphite oxide 有权
标题翻译：含有热剥离石墨氧化物的超级电容器和电池电极
公开(公告)号：US08192870B2
公开(公告)日：2012-06-05
申请号：US12208706
申请日：2008-09-11
申请人： Ilhan A. Aksay , Ted Chao-Hung Yeh , Dudley A. Saville , Joy Saville, legal representative
发明人： Ilhan A. Aksay , Ted Chao-Hung Yeh , Dudley A. Saville
IPC分类号： H01M4/48
CPC分类号： H05K1/095 , B82Y30/00 , B82Y40/00 , C01B31/0423 , C01B31/043 , C01B31/0476 , C01B32/192 , C01B32/225 , C01B32/23 , C01B2204/32 , H01G4/206 , H05K3/0091 , H05K3/10 , H05K2201/0323 , Y02E60/324 , Y02E60/325 , Y02E60/328 , Y10T428/13 , Y10T428/1341 , Y10T428/1379 , Y10T428/2982
摘要： A supercapacitor or battery electrode containing a modified graphite oxide material, which is a thermally exfoliated graphite oxide with a surface area of from about 300 m2/g to 2600 m2/g.
摘要翻译：包含改性氧化石墨材料的超级电容器或电池电极，其是表面积为约300m 2 / g至2600m 2 / g的热剥离石墨氧化物。

74. 发明授权

US08110524B2 Gas storage cylinder formed from a composition containing thermally exfoliated graphite 有权
标题翻译：由含有热剥离石墨的组合物形成的储气筒
公开(公告)号：US08110524B2
公开(公告)日：2012-02-07
申请号：US12194043
申请日：2008-08-19
申请人： Robert K. Prud'Homme , Ilhan A. Aksay
发明人： Robert K. Prud'Homme , Ilhan A. Aksay
IPC分类号： C01B31/04
CPC分类号： H05K1/095 , B82Y30/00 , B82Y40/00 , C01B31/0423 , C01B31/043 , C01B31/0476 , C01B32/192 , C01B32/225 , C01B32/23 , C01B2204/32 , H01G4/206 , H05K3/0091 , H05K3/10 , H05K2201/0323 , Y02E60/324 , Y02E60/325 , Y02E60/328 , Y10T428/13 , Y10T428/1341 , Y10T428/1379 , Y10T428/2982
摘要： A gas storage cylinder or gas storage cylinder liner, formed from a polymer composite, containing at least one polymer and a modified graphite oxide material, which is a thermally exfoliated graphite oxide with a surface area of from about 300 m2/g to 2600 m2/g.
摘要翻译：包含至少一种聚合物和改性氧化石墨材料的由聚合物复合材料形成的储气罐或气体存储缸套，其是表面积为约300m 2 / g至2600m 2 / m 2的热剥离石墨氧化物， G。

75. 发明授权

US08048950B2 Wire coating containing thermally exfoliated graphite oxide 有权
标题翻译：包含热剥离石墨氧化物的电线涂层
公开(公告)号：US08048950B2
公开(公告)日：2011-11-01
申请号：US12194007
申请日：2008-08-19
申请人： Robert K. Prud'homme , Ilhan A. Aksay , Douglas Adamson , Ahmed Abdala
发明人： Robert K. Prud'homme , Ilhan A. Aksay , Douglas Adamson , Ahmed Abdala
IPC分类号： C08K3/04
CPC分类号： H05K1/095 , B82Y30/00 , B82Y40/00 , C01B31/0423 , C01B31/043 , C01B31/0476 , C01B32/192 , C01B32/225 , C01B32/23 , C01B2204/32 , H01G4/206 , H05K3/0091 , H05K3/10 , H05K2201/0323 , Y02E60/324 , Y02E60/325 , Y02E60/328 , Y10T428/13 , Y10T428/1341 , Y10T428/1379 , Y10T428/2982
摘要： A wire coating containing a modified graphite oxide material, which is a thermally exfoliated graphite oxide with a surface area of from about 300 m2/g to 2600 m2/g.
摘要翻译：包含改性氧化石墨材料的线涂层，其是表面积为约300m 2 / g至2600m 2 / g的热剥离石墨氧化物。

76. 发明授权

US07658901B2 Thermally exfoliated graphite oxide 有权
标题翻译：热剥离石墨氧化物
公开(公告)号：US07658901B2
公开(公告)日：2010-02-09
申请号：US11249404
申请日：2005-10-14
申请人： Robert K. Prud'Homme , Ilhan A. Aksay , Douglas Adamson , Ahmed Abdala
发明人： Robert K. Prud'Homme , Ilhan A. Aksay , Douglas Adamson , Ahmed Abdala
IPC分类号： C01B31/04
CPC分类号： H05K1/095 , B82Y30/00 , B82Y40/00 , C01B31/0423 , C01B31/043 , C01B31/0476 , C01B32/192 , C01B32/225 , C01B32/23 , C01B2204/32 , H01G4/206 , H05K3/0091 , H05K3/10 , H05K2201/0323 , Y02E60/324 , Y02E60/325 , Y02E60/328 , Y10T428/13 , Y10T428/1341 , Y10T428/1379 , Y10T428/2982
摘要： A modified graphite oxide material contains a thermally exfoliated graphite oxide with a surface area of from about 300 m2/g to 2600 m2/g, wherein the thermally exfoliated graphite oxide displays no signature of the original graphite and/or graphite oxide, as determined by X-ray diffraction.
摘要翻译：改性氧化石墨材料含有表面积为约300m 2 / g至2600m 2 / g的热剥离石墨氧化物，其中热剥离的氧化石墨氧化物不显示原始石墨和/或氧化石墨的标志，如 X射线衍射。

77. 发明申请

US20090053437A1 GAS STORAGE CYLINDER FORMED FROM A COMPOSITION CONTAINING THERMALLY EXFOLIATED GRAPHITE 有权
标题翻译：由含有热变形石墨的组合物形成的气体储存气瓶
公开(公告)号：US20090053437A1
公开(公告)日：2009-02-26
申请号：US12194043
申请日：2008-08-19
申请人： Robert K. PRUD'HOMME , Ilhan A. AKSAY , Douglas ADAMSON , Ahmed ABDALA
发明人： Robert K. PRUD'HOMME , Ilhan A. AKSAY , Douglas ADAMSON , Ahmed ABDALA
IPC分类号： B32B1/08
CPC分类号： H05K1/095 , B82Y30/00 , B82Y40/00 , C01B31/0423 , C01B31/043 , C01B31/0476 , C01B32/192 , C01B32/225 , C01B32/23 , C01B2204/32 , H01G4/206 , H05K3/0091 , H05K3/10 , H05K2201/0323 , Y02E60/324 , Y02E60/325 , Y02E60/328 , Y10T428/13 , Y10T428/1341 , Y10T428/1379 , Y10T428/2982
摘要： A gas storage cylinder or gas storage cylinder liner, formed from a polymer composite, containing at least one polymer and a modified graphite oxide material, which is a thermally exfoliated graphite oxide with a surface area of from about 300 m2/g to 2600 m2/g.
摘要翻译：包含至少一种聚合物和改性氧化石墨材料的由聚合物复合材料形成的储气罐或气体存储缸套，其是表面积为约300m 2 / g至2600m 2 / m 2的热剥离石墨氧化物， G。

78. 发明申请

US20090053433A1 PACKAGING MATERIAL AND FLEXIBLE MEDICAL TUBING CONTAINING THERMALLY EXFOLIATED GRAPHITE OXIDE 有权
标题翻译：包装材料和灵活的医用管包含热膨胀的石墨氧化物
公开(公告)号：US20090053433A1
公开(公告)日：2009-02-26
申请号：US12194062
申请日：2008-08-19
申请人： Robert K. PRUD'HOMME , Ilhan A. AKSAY , Douglas ADAMSON , Ahmed ABDALA
发明人： Robert K. PRUD'HOMME , Ilhan A. AKSAY , Douglas ADAMSON , Ahmed ABDALA
IPC分类号： B32B1/08 , B32B9/00
CPC分类号： H05K1/095 , B82Y30/00 , B82Y40/00 , C01B31/0423 , C01B31/043 , C01B31/0476 , C01B32/192 , C01B32/225 , C01B32/23 , C01B2204/32 , H01G4/206 , H05K3/0091 , H05K3/10 , H05K2201/0323 , Y02E60/324 , Y02E60/325 , Y02E60/328 , Y10T428/13 , Y10T428/1341 , Y10T428/1379 , Y10T428/2982
摘要： A packaging material or flexible medical tubing containing a modified graphite oxide material, which is a thermally exfoliated graphite oxide with a surface area of from about 300 m2/g to 2600 m2/g.
摘要翻译：一种包含改性氧化石墨材料的包装材料或柔性医用管，其是表面积为约300m 2 / g至2600m 2 / g的热剥离石墨氧化物。

79. 发明授权

US4091083A Method for the production of graphite-hydrogensulfate 失效
标题翻译：生产石墨硫酸氢盐的方法
公开(公告)号：US4091083A
公开(公告)日：1978-05-23
申请号：US767775
申请日：1977-02-11
申请人： Alfred Hirschvogel , Friedrich Wagner
发明人： Alfred Hirschvogel , Friedrich Wagner
IPC分类号： C01B31/00 , C04B35/536 , C01B31/04
CPC分类号： C01B31/043 , C04B35/536
摘要： Production of graphite-hydrogensulfate by dispersing crystalline graphite particles in sulfuric acid, agitating the mixture, adding hydrogen peroxide to the agitated dispersion and continuing agitation until the graphite is converted to graphite-hydrogensulfate. Excess acid is separated and the residual acid in the solid product is removed by washing. The graphite-hydrogensulfate may be heated to transform it into expanded graphite. The method minimizes pollution of the atmosphere with noxious gases and also makes possible ready recovery of unused acid.
摘要翻译：通过将结晶石墨颗粒分散在硫酸中制备石墨硫酸氢盐，搅拌该混合物，向搅拌的分散体中加入过氧化氢，继续搅拌直到石墨转化为石墨 - 硫酸氢盐。分离过多的酸，并通过洗涤除去固体产物中的残留酸。可以加热石墨硫酸氢盐以将其转化成膨胀石墨。该方法可以减少有毒气体对大气的污染，也可以使未使用的酸回收。

80. 发明授权

US09844762B2 Nanoporous metal-carbon composite 有权
公开(公告)号：US09844762B2
公开(公告)日：2017-12-19
申请号：US14485474
申请日：2014-09-12
申请人： LAWRENCE LIVERMORE NATIONAL SECURITY, LLC
发明人： Marcus A. Worsley , Joe Satcher , Sergei Kucheyev , Supakit Charnvanichborikarn , Jeffrey Colvin , Thomas Felter , Sangil Kim , Matthew Merrill , Christine Orme
IPC分类号： A61L15/32 , B01J13/00 , C01B31/04 , C01B31/02
CPC分类号： B01J13/0091 , C01B31/022 , C01B31/0253 , C01B31/043 , C01B31/0438 , C01B31/0484 , C01B32/158 , C01B32/182 , C01B32/23 , C01P2006/10
摘要： Described here is a metal-carbon composite, comprising (a) a porous three-dimensional scaffold comprising one or more of carbon nanotubes, graphene and graphene oxide, and (b) metal nanoparticles disposed on said porous scaffold, wherein the metal-carbon composite has a density of 1 g/cm3 or less, and wherein the metal nanoparticles account for 1 wt. % or more of the metal-carbon composite. Also described are methods for making the metal-carbon composite.

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