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71. 发明授权

US5492627A Method for separating mercury from fluids using composite articles 失效
标题翻译：使用复合制品从流体中分离汞的方法
公开(公告)号：US5492627A
公开(公告)日：1996-02-20
申请号：US268286
申请日：1994-06-29
申请人： Donald F. Hagen , Wanda Bahmet , Louis C. Haddad , Robert E. Perkins
发明人： Donald F. Hagen , Wanda Bahmet , Louis C. Haddad , Robert E. Perkins
IPC分类号： B01D15/00 , B01D53/64 , B01J20/06 , B01J20/28 , B01D61/00
CPC分类号： B01J20/28028 , B01D15/00 , B01D53/64 , B01J20/103 , B01J20/28059 , B01J20/3234 , Y10S210/914
摘要： Composite articles are useful for separating mercury from fluids. The composite articles can be porous supports comprising an inert substrate having immobilized thereon finely divided gold optionally in combination with a tin salt coating. The porous support can be a particulate or porous fibrous webs. Alternatively, the composite articles can comprise a porous fibrous membrane having enmeshed therein the aforementioned porous supports which can be in particulate or fibrous forms. The method for separating elemental, ionic, or organic mercury in fluids comprises the step of contacting and passing a fluid containing mercury through a support comprising a porous, high surface area, inert substrate on which is immobilized finely divided elemental gold at a controlled rate for a time sufficient for the mercury to sorb to the elemental gold and to provide an immobilized gold-mercury amalgam on the support. If a tin salt also is immobilized on the inert substrate, mercury-tin salt can also be formed. In a further, and optional, step, elemental mercury can be removed from the support and optionally can be quantified.
摘要翻译：复合制品可用于从流体中分离汞。复合制品可以是多孔载体，其包括其上固定有细碎金的惰性基材，任选与锡盐涂层组合。多孔载体可以是颗粒或多孔纤维网。或者，复合制品可以包括多孔纤维膜，其中包含可以是颗粒或纤维形式的上述多孔载体。用于分离流体中的元素，离子或有机汞的方法包括使包含汞的流体通过包含多孔，高表面积的惰性基质的载体接触和通过的步骤，在其上以受控的速率将细分的元素金固定在其上足以使汞吸附到元素金上并在载体上提供固定的金汞汞合金。如果锡盐也固定在惰性基材上，也可以形成汞锡盐。在另外的和任选的步骤中，元素汞可以从支持物中除去并且可任选地被定量。

72. 发明授权

US5441635A Packing material for liquid chromatography 失效
标题翻译：液相色谱填充材料
公开(公告)号：US5441635A
公开(公告)日：1995-08-15
申请号：US29940
申请日：1993-03-10
申请人： Takeshi Ichitsuka , Tetsuro Ogawa , Masaya Sumita
发明人： Takeshi Ichitsuka , Tetsuro Ogawa , Masaya Sumita
IPC分类号： B01D15/08 , B01J20/04 , B01J20/32
CPC分类号： B01J20/28059 , B01D15/3847 , B01J20/048 , B01J20/28004 , B01J20/28019 , B01J20/28078 , B01J20/282 , B01J20/286 , B01J20/3021 , B01J20/3028 , B01J20/3064 , B01J20/3078 , B01J20/3092 , B01J20/3204 , B01J20/3208 , B01J20/3234 , B01J2220/54 , B01J2220/58
摘要： Column packing materials useful in applications such as liquid chromatography, as well as a process for producing such a packing material are described. A first aspect of the invention concerns a column packing material composed of a spherical substrate having a coating of a calcium phosphate based compound on the surface thereof.A second aspect of the invention concerns a packing material comprising porous calcium phosphate based granules having open pores with an average pore size of from 0.01 to 20 .mu.m, said granules being composed of crystalline particles with an average size of from 0.1 to 10 .mu.m.A third aspect of the invention concerns a spherical packing material for liquid chromatography comprising spherical particles of at least one material selected from the group consisting of Ca.sub.10 (PO.sub.4).sub.6 (OH).sub.2, Ca.sub.3 (PO.sub.4).sub.2, Ca.sub.2 P.sub.2 O.sub.7, Ca(PO.sub.3).sub.2, Ca.sub.10 (PO.sub.4).sub.6 F.sub.2 and Ca.sub.10 (PO.sub.4).sub.6 Cl.sub.2, said packing material having a dense structure with a porosity of no more than 5%.A fourth aspect of the invention concerns a packing for liquid chromatography comprising particles having at least on the surface thereof a fluoroapatite represented by formula (I):Ca.sub.10 (PO.sub.4).sub.6 (OH).sub.2-2x F.sub.2x (I)wherein x is a number of from about 0.1 to 1.
摘要翻译：描述了可用于诸如液相色谱法的应用的柱状填料，以及用于生产这种包装材料的方法。本发明的第一方面涉及一种柱状填充材料，其由在其表面上具有磷酸钙基化合物的涂层的球形基材构成。本发明的第二方面涉及一种包含多孔磷酸钙基颗粒的包装材料，其具有平均孔径为0.01至20μm的开放孔，所述颗粒由平均尺寸为0.1-10μm的结晶颗粒组成。本发明的第三方面涉及一种用于液相色谱的球形包装材料，其包括选自Ca10（PO4）6（OH）2，Ca3（PO4）2，Ca2P2O7，Ca（PO3） 2，Ca10（PO4）6F2和Ca10（PO4）6Cl2，所述包装材料具有孔隙率不超过5％的致密结构。本发明的第四方面涉及一种用于液相色谱的填料，其包括至少在其表面上具有由式（I）表示的氟磷灰石的颗粒：Ca10（PO4）6（OH）2-2xF2x（I），其中x是约0.1至1。

73. 发明授权

US5141634A High stability porous zirconium oxide spherules 失效
标题翻译：高稳定性多孔氧化锆球
公开(公告)号：US5141634A
公开(公告)日：1992-08-25
申请号：US654312
申请日：1991-02-12
申请人： Peter W. Carr , Eric F. Funkenbusch , Martin P. Rigney , Patrick L. Coleman , Douglas A. Hanggi , Wes A. Schafer
发明人： Peter W. Carr , Eric F. Funkenbusch , Martin P. Rigney , Patrick L. Coleman , Douglas A. Hanggi , Wes A. Schafer
IPC分类号： B01J20/06 , B01J20/32 , B01J39/12 , C01G25/02 , G01N30/52
CPC分类号： B01J20/287 , B01J20/06 , B01J20/3204 , B01J20/3234 , B01J20/3248 , B01J20/3282 , B01J39/12 , B82Y30/00 , C01G25/02 , B01J2220/54 , C01P2004/32 , C01P2004/61 , C01P2004/62 , C01P2004/64 , C01P2004/80 , C01P2006/12 , C01P2006/14 , C01P2006/16 , C01P2006/17 , G01N2030/525
摘要： The present invention provides a stable stationary phase for chromatography which comprises porous ZrO.sub.2 spherules coated with a cross-linked polymer coating wherein said coated spherules have a pore size from about 20-500 .ANG. and a particle diameter range of about 0.5-500 microns, and are stable in basic media to pHs of up to about 14.
摘要翻译：本发明提供了用于色谱的稳定的固定相，其包括涂覆有交联聚合物涂层的多孔ZrO 2球晶，其中所述涂覆的球体具有约20-500的孔径和约0.5-500微米的粒径范围，以及在碱性介质中稳定，pH值高达约14。

74. 发明授权

US4474853A Sorbent comprising spherical particles of activated carbon depositing non-crystalline compound of zirconium and process for preparing thereof 失效
标题翻译：吸附剂包括活性炭球形颗粒沉积锆的非结晶性化合物及其制备方法
公开(公告)号：US4474853A
公开(公告)日：1984-10-02
申请号：US543049
申请日：1983-10-18
申请人： Kazuhiro Watanabe
发明人： Kazuhiro Watanabe
IPC分类号： C02F1/28 , A61M1/36 , B01J20/06 , B01J20/20 , B32B9/00 , B05D7/00
CPC分类号： B01J20/3234 , B01J20/0211 , B01J20/06 , B01J20/20 , B01J20/3204 , B01J20/3236 , Y10T428/2982 , Y10T428/2991 , Y10T428/30
摘要： Disclosed herein are a sorbent comprising spherical particles of activated carbon formed from a pitch and/or a synthetic, organic high polymer, to which a non-crystalline compound of zirconium has been deposited in an amount of 1 to 10% by weight (calculated as ZrO.sub.2) to the weight thereof and a process for preparing the sorbent comprising the steps of impregnating the spherical particles of activated carbon with an aqueous solution of a water-soluble compound of zirconium and after treating the thus impregnated spherical particles of activated carbon with an alkali, thermally treating the thus treated spherical particles of activated carbon at a temperature of 400.degree. to 1000.degree. C.
摘要翻译：本文公开了一种吸附剂，其包含由沥青和/或合成的有机高分子形成的活性炭的球形颗粒，其中非晶态的锆化合物以1至10重量％的量沉积（计算为 ZrO 2）和其制备方法，包括以下步骤：用锆的水溶性化合物的水溶液浸渍活性炭的球形颗粒，并用碱处理如此浸渍的活性炭球形颗粒在400〜1000℃的温度下热处理这样处理的活性炭球形颗粒。

75. 发明授权

US3922392A Process for coating nonporous material with a porous silicon dioxide layer 失效
标题翻译：用多孔二氧化硅层涂覆无孔材料的方法
公开(公告)号：US3922392A
公开(公告)日：1975-11-25
申请号：US36411773
申请日：1973-05-25
申请人： MERCK PATENT GMBH
发明人： KOHLSCHUTTER HANS WOLFGANG , UNGER KLAUS , SCHICK-KALB JURGEN
IPC分类号： B01J20/281 , B01J20/10 , B05D7/00 , C03C17/25 , G01N30/88
CPC分类号： B01J20/3234 , B01J20/283 , B01J20/286 , B01J20/3204 , B01J20/3293 , B01J20/3295 , B05D7/00 , B05D2201/02 , B05D2202/25 , B05D2203/35 , B05D2518/12 , C03C17/25 , C03C2217/213 , C03C2218/111
摘要： Nonporous materials are coated with a porous silicon dioxide layer by coating the nonporous material with a polymeric alkoxysiloxane and then subjecting this coating to a hydrolytic polycondensation with an aqueous basic solution. The thusobtained product is then dried.
摘要翻译：通过用聚合物烷氧基硅氧烷涂覆无孔材料，然后使该涂层与碱性水溶液进行水解缩聚，将多孔材料涂覆多孔二氧化硅层。然后将由此获得的产物干燥。

76. 发明授权

US1570537A Absorbent material and process of making same 失效
标题翻译：吸收材料及其制造方法
公开(公告)号：US1570537A
公开(公告)日：1926-01-19
申请号：US70247424
申请日：1924-03-27
申请人： CELITE COMPANY
发明人： TEITSWORTH CLARK S
IPC分类号： B01J20/32
CPC分类号： B01J20/10 , B01J20/14 , B01J20/28047 , B01J20/3021 , B01J20/3078 , B01J20/3085 , B01J20/3204 , B01J20/3234 , B01J20/3236

77. 发明授权

US337026A Heney h 失效
公开(公告)号：US337026A
公开(公告)日：1886-03-02
申请号：US337026D
CPC分类号： B01D15/00 , B01J20/32 , B01J20/3204 , B01J20/3234 , Y10S210/917

78. 发明申请

US20180326399A1 CHROMATOGRAPHIC MATERIALS 审中-公开
公开(公告)号：US20180326399A1
公开(公告)日：2018-11-15
申请号：US15911630
申请日：2018-03-05
申请人： Waters Technologies Corporation
发明人： Kevin D. Wyndham , Michael F. Morris , Darryl W. Brousmiche , Jason F. Hill , Jacob N. Fairchild
IPC分类号： B01J20/283 , C07F7/18 , B01J20/28 , B01D15/30 , B01D15/32 , B01D15/40 , B01D53/02 , B01J20/22 , B01J20/32 , B01J20/30 , B01J20/289 , B01J20/288 , B01D15/26 , B01J20/282 , B01J20/285 , B01J20/284
CPC分类号： B01J20/283 , B01D15/26 , B01D15/30 , B01D15/305 , B01D15/322 , B01D15/40 , B01D53/025 , B01J20/22 , B01J20/28004 , B01J20/28016 , B01J20/28042 , B01J20/28057 , B01J20/28059 , B01J20/28061 , B01J20/28064 , B01J20/28066 , B01J20/28069 , B01J20/28071 , B01J20/28073 , B01J20/28076 , B01J20/28078 , B01J20/28083 , B01J20/28085 , B01J20/282 , B01J20/284 , B01J20/285 , B01J20/288 , B01J20/289 , B01J20/3085 , B01J20/32 , B01J20/3204 , B01J20/3206 , B01J20/3208 , B01J20/3234 , B01J20/3246 , B01J20/3285 , B01J20/3293 , B01J2220/54 , B01J2220/80 , C07F7/1804
摘要： In one aspect, the present invention provides a chromatographic stationary phase material for various different modes of chromatography represented by Formula 1: [X](W)a(Q)b(T)c (Formula 1). X can be a high purity chromatographic core composition having a surface comprising a silica core material, metal oxide core material, an inorganic-organic hybrid material or a group of block copolymers thereof. W can be absent and/or can include hydrogen and/or can include a hydroxyl on the surface of X. Q can be a functional group that minimizes retention variation over time (drift) under chromatographic conditions utilizing low water concentrations. T can include one or more hydrophilic, polar, ionizable, and/or charged functional groups that chromatographically interact with the analyte. Additionally, b and c can be positive numbers, with the ratio 0.05≤(b/c)≤100, and a≥0.

79. 发明申请

US20180250653A1 HYDROPHOBIC SORBENTS FOR CO2/H2O DISPLACEMENT DESORPTION APPLICATIONS 审中-公开
公开(公告)号：US20180250653A1
公开(公告)日：2018-09-06
申请号：US15910212
申请日：2018-03-02
申请人： ExxonMobil Research and Engineering Company , TDA Research, Inc.
发明人： Chuansheng Bai , Majosefina Cunningham , Patrick P. McCall , Hans Thomann , Jeannine Elizabeth Elliott , Vinh Nguyen
IPC分类号： B01J20/04 , B01J20/22 , B01J20/10 , B01J20/08 , B01J20/34 , B01J20/32 , B01J20/30 , B01D53/02
CPC分类号： B01J20/041 , B01D53/02 , B01D2253/104 , B01D2253/106 , B01D2253/1124 , B01D2253/20 , B01D2253/25 , B01D2257/504 , B01D2258/0283 , B01D2259/40086 , B01J20/08 , B01J20/103 , B01J20/22 , B01J20/3078 , B01J20/3204 , B01J20/3234 , B01J20/3433 , B01J20/3466
摘要： The disclosure generally relates to CCS sorbents, particularly for CO2/H2O displacement desorption process. The sorbent includes an aluminum oxide support and an alkali metal salt impregnated on the support, and a silicon modification of the sorbent to reduce water uptake by the sorbent and make it more hydrophobic. The silicon modification can be an organosilyl moiety added after the initial sorbent is complete, or a silica source added to the aluminum oxide structure, typically via impregnation. The sorbents demonstrate better H2O/CO2 ratios. Compositions and methods of making are disclosed.

80. 发明授权

US09765325B2 Fabrication of hierarchical silica nanomembranes and uses thereof for solid phase extraction of nucleic acids 有权
公开(公告)号：US09765325B2
公开(公告)日：2017-09-19
申请号：US14341957
申请日：2014-07-28
申请人： THE JOHNS HOPKINS UNIVERSITY
发明人： Tza-Huei Wang , Yi Zhang
IPC分类号： C12Q1/68 , G01N31/22 , G01N33/552 , C12N15/10 , C25D1/00 , B01D71/02 , B01D67/00 , B01J20/10 , B01J20/26 , B01J20/28 , B01J20/32 , C23C14/10 , C23C14/22 , C23C16/44 , C25D13/02 , C25D13/12 , C23C18/12 , B01D69/06
CPC分类号： C12N15/1006 , B01D67/0069 , B01D67/0072 , B01D67/0083 , B01D69/06 , B01D71/027 , B01J20/103 , B01J20/261 , B01J20/28035 , B01J20/321 , B01J20/3225 , B01J20/3234 , B01J20/3297 , C12Q1/6806 , C23C14/10 , C23C14/221 , C23C16/44 , C23C18/1212 , C25D1/006 , C25D13/02 , C25D13/12
摘要： The present invention provides a novel method to fabricate silica nanostructures on thin polymer films based on silica deposition and self-wrinkling induced by thermal shrinkage. These micro- and nano-scale structures have vastly enlarged the specific area of silica, thus the silica nanomembranes can be used for solid phase extraction of nucleic acids. The inventive silica nanomembranes are suitable for nucleic acid purification and isolation and demonstrated better performance than commercial particles in terms of DNA recovery yield and integrity. In addition, the silica nanomembranes have extremely high nucleic acid capacity due to its significantly enlarged specific surface area of silica. Methods of use and devices comprising the silica nanomembranes are also provided.

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